Information card for entry 8101411

Structure parameters

• Formula: C44 H34 Cl2 F3 O2 P2 Re S
• Calculated formula: C44 H34 Cl2 F3 O2 P2 Re S
• Title of publication: Crystal structure of dichloro[4,4,4-trifluoro-1-(2'-thienyl)butane-1,3- dionato]-bis(triphenylphosphine)rhenium(III), [Re(C~44~H~34~Cl~2~F~3~O~2~P~2~S)]
• Authors of publication: Sawusch, S.; Schilde, U.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 1999
• Journal volume: 214
• Journal issue: 1
• Pages of publication: 81 - 82
• a: 13.098 ± 0.002 Å
• b: 23.673 ± 0.003 Å
• c: 13.289 ± 0.002 Å
• α: 90°
• β: 90.15 ± 0.014°
• γ: 90°
• Cell volume: 4120.5 ± 1.1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0347
• Weighted residual factors for significantly intense reflections: 0.09
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No