Information card for entry 8101475

Structure parameters

• Formula: C70 H108 Cl2 N20 Ni9 O40
• Calculated formula: C70 H70 Cl2 N20 Ni9 O40
• Title of publication: Crystal structure of hexaaquadi(μ3-hydroxo)tetra(μ2-hydroxo) tetrakis-(μ3-{1-[2-(6-methylpyridyl)]ethanone oximato})hexakis (μ2-{1-[2-(6-methylpyridyl)]ethanone oximato)nonanickel(II) perchlorate hydrate, [Ni9(C7H7N2O)10(OH)6(H2O)6](ClO4)2 · 10H2O
• Authors of publication: Pajunen, A.; Mutikainen, I.; Saarinen, H.; Orama, M.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 1999
• Journal volume: 214
• Journal issue: 2
• Pages of publication: 217 - 220
• a: 15.92 ± 0.007 Å
• b: 16.673 ± 0.008 Å
• c: 20.583 ± 0.01 Å
• α: 77.8 ± 0.06°
• β: 81 ± 0.06°
• γ: 72.6 ± 0.04°
• Cell volume: 5070 ± 4 ų
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.1084
• Weighted residual factors for significantly intense reflections: 0.2626
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No