Information card for entry 8101661

Structure parameters

• Formula: C32 H32 Br2 Cl2 Ni O2 P2
• Calculated formula: C32 H32 Br2 Cl2 Ni O2 P2
• Title of publication: Crystal structure of dibromo[(-)-2,2-dimethyl-4,5-bis(diphenylphoshinomethyl)- 1,3-dioxolane-<i>P</i>,<i>P</i>'] nickel-dichloromethane (1/1), C~31~H~32~Br~2~NiO~2~P~2~ · CH~2~Cl~2~
• Authors of publication: Frenzen, Gerlinde; Pilz, Astrid; Frauenrath, Herbert; Reim, Stefan
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 1998
• Journal volume: 213
• Journal issue: 4
• Pages of publication: 775 - 776
• a: 10.735 ± 0.001 Å
• b: 17.56 ± 0.003 Å
• c: 17.685 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3333.7 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0687
• Weighted residual factors for significantly intense reflections: 0.1734
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No