Information card for entry 8101776

Structure parameters

• Chemical name: tetrachloro-bis(pyrazole)tungsten dimethoxyethane solvate
• Formula: C10 H18 Cl4 N4 O2 W
• Calculated formula: C10 H18 Cl4 N4 O2 W
• Title of publication: Crystal structure of tetrachloro-bis(pyrazole)tungsten(IV) dimethoxyethane solvate, WCl~4~(C~3~H~4~N~2~)~2~ · (CH~3~OCH~2~)~2~
• Authors of publication: R. D. Ernst; B. G. Harvey; A. M. Arif
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2005
• Journal volume: 220
• Journal issue: 2
• Pages of publication: 281 - 282
• a: 13.9659 ± 0.0003 Å
• b: 8.2642 ± 0.0002 Å
• c: 15.8814 ± 0.0003 Å
• α: 90°
• β: 101.184 ± 0.0012°
• γ: 90°
• Cell volume: 1798.18 ± 0.07 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0881
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No