Information card for entry 8101788

Structure parameters

• Formula: C18 H49 Cl4 I N6 Ni3 O
• Calculated formula: C18 H49 Cl4 I N6 Ni3 O
• Title of publication: Crystal structure of μ~3~-chloro- μ~3~-hydroxo-tris (μ-chloro)tris(tetramethylethylenediamine)trinickel(II) iodide, [Ni~3~(C~6~H~16~N~2~)~3~Cl~4~(OH)]I
• Authors of publication: Miyamoto, K.; Koizumi, R.; Horn, E.; Fukuda, Y.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2006
• Journal volume: 221
• Journal issue: 2
• Pages of publication: 123 - 125
• a: 33.562 ± 0.007 Å
• b: 12.22 ± 0.002 Å
• c: 18.849 ± 0.004 Å
• α: 90°
• β: 117.7 ± 0.03°
• γ: 90°
• Cell volume: 6845 ± 3 ų
• Cell temperature: 273.2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for all reflections included in the refinement: 0.0655
• Goodness-of-fit parameter for all reflections included in the refinement: 0.182
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No