Information card for entry 8101932

Structure parameters

• Chemical name: bis(2-hydroxy-2,2-bis(pyridin-2-yl)acetato)nickel(II) methanol monosolvate
• Formula: C25 H22 N4 Ni O7
• Calculated formula: C25 H18 N4 Ni O7
• Title of publication: Crystal structure of bis(2-hydroxy-2,2-bis(pyridin-2-yl)acetato)nickel (II) methanol solvate, Ni[(C~5~H~4~N)~2~C(OH)COO]~2~·CH~3~OH
• Authors of publication: Tang, L.; Li, J.; Li, D.-S.; Zhou, C.-H.; Wang, J.-J.; Wang, J.-W.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2006
• Journal volume: 221
• Journal issue: 1
• Pages of publication: 85 - 86
• a: 8.4623 ± 0.0019 Å
• b: 8.5144 ± 0.0019 Å
• c: 10.467 ± 0.002 Å
• α: 79.823 ± 0.004°
• β: 74.813 ± 0.004°
• γ: 76.791 ± 0.004°
• Cell volume: 703.1 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0505
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.1407
• Weighted residual factors for all reflections included in the refinement: 0.1443
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No