Information card for entry 8102111

Structure parameters

• Chemical name: μ-oxo-bis[σ-1,2-bis(trimethylsilyl)vinylhafnocene] benzene solvate
• Formula: C42 H64 Hf2 O Si4
• Calculated formula: C42 H64 Hf2 O Si4
• Title of publication: Crystal structure of μ-oxo-bis(σ-1,2-bis(trimethylsilyl) vinylhafnocene) benzene solvate, [C~2~H{Si(CH~3~)~3~}~2~Hf(C~5~H~5~) ~2~]~2~O · C~6~H~6~
• Authors of publication: Spannenberg, Anke; Beweries, Torsten; Bach, Marc A.; Rosenthal, Uwe
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2007
• Journal volume: 222
• Journal issue: 3
• Pages of publication: 187 - 188
• a: 11.442 ± 0.001 Å
• b: 9.7998 ± 0.0006 Å
• c: 19.8266 ± 0.0016 Å
• α: 90°
• β: 95.229 ± 0.007°
• γ: 90°
• Cell volume: 2213.9 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0231
• Residual factor for significantly intense reflections: 0.0173
• Weighted residual factors for significantly intense reflections: 0.0362
• Weighted residual factors for all reflections included in the refinement: 0.037
• Goodness-of-fit parameter for all reflections included in the refinement: 0.959
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No