Information card for entry 8102189

Structure parameters

• Common name: tris(1,10-phenanthroline-5,6-dione)-nickel diperchlorate
• Chemical name: tris(1,10-phenanthroline-5,6-dione)nickel(II) diperchlorate
• Formula: C36 H18 Cl2 N6 Ni O14
• Calculated formula: C36 H18 Cl2 N6 Ni O14
• Title of publication: Crystal structure of tris(1,10-phenanthroline-5,6-dione)nickel(II) diperchlorate, [Ni(C~12~H~6~N~2~O~2~)~3~][ClO~4~]~2~
• Authors of publication: Li, Ren-Tao; Jiang, Wen-Jun; Li, Xiao-Xiang; Cai, Tie-Jun; Deng, Qian; Peng, Zhen-Shan; Huang, Ming-Zhong
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2007
• Journal volume: 222
• Journal issue: 4
• Pages of publication: 395 - 397
• a: 10.5035 ± 0.0009 Å
• b: 17.8918 ± 0.0015 Å
• c: 18.7366 ± 0.0015 Å
• α: 90°
• β: 93.383 ± 0.001°
• γ: 90°
• Cell volume: 3515 ± 0.5 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1087
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1389
• Weighted residual factors for all reflections included in the refinement: 0.1682
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No