Information card for entry 8102264

Structure parameters

• Chemical name: [cinnamato-[tris(1-methylbenzimidazol-2-ylmethyl)amine]-zinc(II)] perchlorate dimethylformamide solvate methanol (1:1:2:0.5)
• Formula: C42.5 H50 Cl N9 O8.5 Zn
• Calculated formula: C42.5 H49.5 Cl N9 O8.5 Zn
• Title of publication: Crystal structure of [cinnamato-[tris(1-methylbenzimidazol-2-ylmethyl)- amine]-zinc(II)] perchlorate - dimethylformamide - methanol (1:1:2:0.5), [Zn(C27H27N7)(C9H7O2)](ClO4) · 2(CH3)2NCHO · 0.5CH3OH
• Authors of publication: Hui-Lu Wu; Rui-Rui Yun; Jing-Kun Yuan; Jian Ding; Yong-Qiang Tian
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2008
• Journal volume: 223
• Journal issue: 2
• Pages of publication: 152
• a: 33.2012 ± 0.0011 Å
• b: 15.3991 ± 0.0004 Å
• c: 22.3422 ± 0.0007 Å
• α: 90°
• β: 128.686 ± 0.001°
• γ: 90°
• Cell volume: 8916.5 ± 0.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1612
• Weighted residual factors for all reflections included in the refinement: 0.1702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No