Information card for entry 8102310

Structure parameters

• Formula: C208 H168 N48 O36 Zn8
• Calculated formula: C208 H168 N48 O36 Zn8
• Title of publication: Crystal structure of bis(pyridine-2-carboxaldehyde-2-hydroxybenzoyl hydrazone)zinc(II) semihydrate, Zn(C13H10N3O2)2 · 0.5 H2O
• Authors of publication: Xinsheng Wan; Caoyuan Niu; Xianfu Zheng; Chunhong Kou
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2008
• Journal volume: 223
• Journal issue: 3
• Pages of publication: 279
• a: 18.19 ± 0.012 Å
• b: 24.61 ± 0.016 Å
• c: 11.519 ± 0.011 Å
• α: 90°
• β: 103.595 ± 0.018°
• γ: 90°
• Cell volume: 5012 ± 7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1141
• Residual factor for significantly intense reflections: 0.0595
• Weighted residual factors for significantly intense reflections: 0.1634
• Weighted residual factors for all reflections included in the refinement: 0.1973
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No