Information card for entry 8102328

Structure parameters

• Formula: C47 H49 Li N2 O2 Si2
• Calculated formula: C47 H49 Li N2 O2 Si2
• Title of publication: Crystal structure of b-diketiminatodibenzophenonatolithium, [Me3SiNC(Ph)CHC(Ph)NSiMe3](Ph2CO)2Li
• Authors of publication: Hong-Bo Tong; Dian-Sheng Liu
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2008
• Journal volume: 223
• Journal issue: 4
• Pages of publication: 419
• a: 18.525 ± 0.004 Å
• b: 18.391 ± 0.004 Å
• c: 12.54 ± 0.003 Å
• α: 90°
• β: 95.107 ± 0.004°
• γ: 90°
• Cell volume: 4255.3 ± 1.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.131
• Residual factor for significantly intense reflections: 0.0727
• Weighted residual factors for significantly intense reflections: 0.0951
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No