Information card for entry 8102365

Structure parameters

• Formula: C28 H26 Cl3 Cu N O4 P2
• Calculated formula: C28 H26 Cl3 Cu N O4 P2
• Title of publication: Crystal structure of catena-bis[μ-bis(diphenylphosphino)methane]-(μ-pyrazine)-diperchloratodicopper(I)] - dichloromethane (1:1), [Cu2(Ph2PCH2PPh2)2(ClO4)2(C4H4N2)] · CH2Cl2
• Authors of publication: Qiong-Hua Jin; Li-Min Chen; Ke-Yi Hu; Pei-Zhou Li; Cun-Lin Zhang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2009
• Journal volume: 224
• Journal issue: 1
• Pages of publication: 159
• a: 11.1129 ± 0.0011 Å
• b: 21.52 ± 0.002 Å
• c: 12.8719 ± 0.0013 Å
• α: 90°
• β: 98.46 ± 0.002°
• γ: 90°
• Cell volume: 3044.8 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1304
• Residual factor for significantly intense reflections: 0.0791
• Weighted residual factors for significantly intense reflections: 0.1372
• Weighted residual factors for all reflections included in the refinement: 0.1555
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No