Information card for entry 8102462

Structure parameters

• Chemical name: Crystal structure of {tetra[bis(diphenylphosphino) methane dioxide-O,O']dysprosium(III) trifluoromethanesulfonate-N,N'-dimethylformamide(1:2)}, [Dy(dppmo~2~)~4~](OTf)~3~.2DMF
• Formula: C109 H102 Dy F9 N2 O19 P8 S3
• Calculated formula: C109 H102 Dy F9 N2 O19 P8 S3
• Title of publication: Crystal structure of tetra[bis(diphenylphosphino)methane dioxide-O,O']dysprosium(III) tri(trifluoromethanesulfonate) — N,N'-dimethylformamide (1:2), [Dy(C25H22P2O2)4][CF3SO3]3 · 2C3H7NO
• Authors of publication: Qiong-Hua Jin; Jie-Qiang Wu; Yuan-Yuan Zhang; Cun-Lin Zhang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2009
• Journal volume: 224
• Journal issue: 3
• Pages of publication: 428
• a: 15.8588 ± 0.0013 Å
• b: 18.6305 ± 0.0017 Å
• c: 20.687 ± 0.002 Å
• α: 88.076 ± 0.002°
• β: 83.988 ± 0.001°
• γ: 65.575 ± 0.001°
• Cell volume: 5534.2 ± 0.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0912
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.135
• Weighted residual factors for all reflections included in the refinement: 0.1675
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No