Information card for entry 8103194

Structure parameters

• Formula: C38 H33 Cl2 N P2 Pd
• Calculated formula: C38 H33 Cl2 N P2 Pd
• Title of publication: Crystal structure of bis(triphenylphospine-?P)-dichloropalladium(II) — acetonitrile (1:1), [PdCl2(C18H15P)2] • CH3CN
• Authors of publication: Li-Na Cui; Zhong-Feng Li; Jin Wen; Yu-Han Jiang; Qiong-Hua Jin; Hui-Li Gong
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2011
• Journal volume: 226
• Journal issue: 4
• Pages of publication: 591
• a: 12.056 ± 0.0011 Å
• b: 14.3931 ± 0.0013 Å
• c: 20.0019 ± 0.0019 Å
• α: 90°
• β: 92.372 ± 0.001°
• γ: 90°
• Cell volume: 3467.8 ± 0.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.103
• Residual factor for significantly intense reflections: 0.0689
• Weighted residual factors for significantly intense reflections: 0.1527
• Weighted residual factors for all reflections included in the refinement: 0.1812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No