Information card for entry 8104931

Structure parameters

• Formula: C52 H40 Cl4 N4 O16 Pb2
• Calculated formula: C52 H40 Cl4 N4 O16 Pb2
• Title of publication: Crystal structure of diaqua-bis(μ2-5-chloro-salicylato-κ3 O,O′:O′)-bis(5-chloro-salicylato-κ2 O,O′)-bis(1,10-phenanthroline-κ2 N,N′) dilead(II) – water (1/2), C52H36C14N4O14Pb2·2(H2O)
• Authors of publication: Tang, Zhiwei; Wen, Decai
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2021
• Journal volume: 236
• Journal issue: 1
• Pages of publication: 235 - 237
• a: 9.1186 ± 0.0004 Å
• b: 12.8031 ± 0.0006 Å
• c: 13.0111 ± 0.0006 Å
• α: 63.504 ± 0.004°
• β: 79.4 ± 0.004°
• γ: 77.198 ± 0.004°
• Cell volume: 1319.34 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0523
• Weighted residual factors for all reflections included in the refinement: 0.0554
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No