Information card for entry 8105015

Structure parameters

• Chemical name: tetra-(1,10-phenanthroline-N,N') octa-(azido-N) tetra-zinc(II)
• Formula: C48 H32 N32 Zn4
• Calculated formula: C48 H32 N32 Zn4
• Title of publication: Crystal structure of hexakis(μ2-azido-κ2N:N)-diazido-κ1N-tetrakis(phenanthroline-κ2N,N′)tetrazinc(II), C48H32N32Zn4
• Authors of publication: Feng, Yu-Quan; Zhong, Zhi-Guo; Yue, Zi-Long
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2019
• Journal volume: 235
• Journal issue: 1
• Pages of publication: 57 - 58
• a: 9.9928 ± 0.0014 Å
• b: 10.1374 ± 0.0014 Å
• c: 14.2362 ± 0.0019 Å
• α: 71.71 ± 0.002°
• β: 76.166 ± 0.002°
• γ: 71.086 ± 0.002°
• Cell volume: 1280.1 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0795
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0249
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No