Information card for entry 8105651

Structure parameters

• Formula: C20 H24 N6 Ni O6
• Calculated formula: C20 H24 N6 Ni O6
• Title of publication: Crystal structure of bis[2-(((3-aminopropyl)imino)methyl)-4-nitro-phenolato-κ3 N,N′,O]nickel(II), C20H24N6NiO6
• Authors of publication: Wang, Li; Yu, Meng; Liu, Ling-Zhi; Ma, Jin-Xia; Dong, Wen-Kui
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2019
• Journal volume: 234
• Journal issue: 3
• Pages of publication: 377 - 378
• a: 5.3944 ± 0.0006 Å
• b: 10.1144 ± 0.0012 Å
• c: 10.9297 ± 0.0012 Å
• α: 65.236 ± 0.003°
• β: 81.959 ± 0.003°
• γ: 79.882 ± 0.003°
• Cell volume: 531.61 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0285
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0636
• Weighted residual factors for all reflections included in the refinement: 0.0649
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No