Information card for entry 8106037

Structure parameters

• Formula: C38 H34 Cl2 N4 Ni2 O12
• Calculated formula: C38 H34 Cl2 N4 Ni2 O12
• Title of publication: Crystal structure of diaqua-bis(N,N-dimethylformamide-κ1 O)-bis{3-((5-chloro-2-oxidobenzylidene)amino)-2-oxo-2H-chromen-4-olato-κ4 N,O,O′:O′}dinickel(II), C38H34Ni2Cl2N4O12
• Authors of publication: Li, Jing; Jia, Hao-Ran; Guo, Jian-Qiang; Sun, Yin-Xia
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2018
• Journal volume: 233
• Journal issue: 1
• Pages of publication: 41 - 43
• a: 17.867 ± 0.003 Å
• b: 9.17 ± 0.006 Å
• c: 24.651 ± 0.005 Å
• α: 90°
• β: 110.837 ± 0.002°
• γ: 90°
• Cell volume: 3775 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0392
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.1023
• Weighted residual factors for all reflections included in the refinement: 0.1078
• Goodness-of-fit parameter for all reflections included in the refinement: 0.929
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No