Information card for entry 8106167

Structure parameters

• Formula: C25 H23 Br2 Cl N3 Na Ni O9
• Calculated formula: C25 H23 Br2 Cl N3 Na Ni O9
• Title of publication: Crystal structure of (dimethylformamide-κO)(perchlorato-κ2 O,O′){μ2-6,6′-((1,2-phenylenebis(azanylylidene))bis(methanylylidene))bis(4-bromo-2-methoxyphenolate)-κ8 N,N′,O:O,O′:O′,O′′,O′′′}sodium(I)nickel(II), C25H23Br2ClN3NaNiO9
• Authors of publication: Meng, Qingguo; Yue, Chen; Yu, Jiangkun; Liu, Qingyun; Lu, Jitao
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2018
• Journal volume: 233
• Journal issue: 3
• Pages of publication: 409 - 411
• a: 15.595 ± 0.004 Å
• b: 10.993 ± 0.003 Å
• c: 18.66 ± 0.005 Å
• α: 90°
• β: 114.536 ± 0.004°
• γ: 90°
• Cell volume: 2910.1 ± 1.3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0865
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0842
• Weighted residual factors for all reflections included in the refinement: 0.0998
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No