Information card for entry 8106573

Structure parameters

• Formula: C22 H32 N2 Ni O6
• Calculated formula: C22 H32 N2 Ni O6
• Title of publication: Crystal structure of bis(2-(2-hydroxymethyl)pyridine-κ2 N,O)-bis(pivalato-κO)nickel(II), C22H32N2NiO6
• Authors of publication: Yuhua, Guo; Youzhu, Yu; Weiyun, Shi; Aimin, Wei; Fengli, Wang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2017
• Journal volume: 232
• Journal issue: 3
• Pages of publication: 471 - 472
• a: 12.7943 ± 0.0007 Å
• b: 11.7513 ± 0.0006 Å
• c: 16.7322 ± 0.0009 Å
• α: 90°
• β: 96.337 ± 0.002°
• γ: 90°
• Cell volume: 2500.3 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.03
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for significantly intense reflections: 0.0795
• Weighted residual factors for all reflections included in the refinement: 0.0816
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No