Information card for entry 8107307

Structure parameters

• Formula: C48 H32 N4 O8 Pb2
• Calculated formula: C48 H32 N4 O8 Pb2
• Title of publication: The crystal structure of tetrakis(6-phenylpyridine-2-carboxylate-κ 2 N,O)-bis(μ2-6-phenylpyridine-2-carboxylate-κ 2 O:O′)-bis(μ2-6-phenylpyridine-2-carboxylate-κ 3N,O:O)tetralead(II) C48H32N4O8Pb2
• Authors of publication: Li-Hua, Wang; Hao-Wen, Tai; Qiu-Shi, Li; Yu-Pei, Xia; Xi-Shi, Tai
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2022
• Journal volume: 237
• Journal issue: 6
• Pages of publication: 1113 - 1116
• a: 9.2712 ± 0.0008 Å
• b: 14.5959 ± 0.0013 Å
• c: 16.6178 ± 0.0013 Å
• α: 76.089 ± 0.007°
• β: 77.068 ± 0.007°
• γ: 74.717 ± 0.007°
• Cell volume: 2074.5 ± 0.3 ų
• Cell temperature: 249.99 ± 0.1 K
• Ambient diffraction temperature: 249.99 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1536
• Weighted residual factors for all reflections included in the refinement: 0.1783
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No