#------------------------------------------------------------------------------
#$Date: 2025-08-18 16:20:24 +0200 (Mon 18 de Aug de 2025) $
#$Revision: 301776 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/28/1512872.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1512872
loop_
_publ_author_name
'Harri Sopo'
'Ari Väisänen'
'Reijo Sillanpää'
_publ_section_title
;
 Uranyl ion complexes with long chain aminoalcoholbis(phenolate)
 [O,N,O,O′] donor ligands
;
_journal_issue                   1
_journal_name_full               Polyhedron
_journal_page_first              184
_journal_page_last               196
_journal_paper_doi               10.1016/j.poly.2006.08.006
_journal_volume                  26
_journal_year                    2007
_chemical_formula_moiety         'C46 H64 N2 O8 U, 2(C2 H3 N)'
_chemical_formula_sum            'C50 H70 N4 O8 U'
_chemical_formula_weight         1093.13
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.197(2)
_cell_angle_beta                 108.741(2)
_cell_angle_gamma                93.142(2)
_cell_formula_units_Z            1
_cell_length_a                   9.1043(3)
_cell_length_b                   10.9246(4)
_cell_length_c                   13.0396(4)
_cell_measurement_reflns_used    4253
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      25.682
_cell_measurement_theta_min      0.407
_cell_volume                     1222.62(7)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor 1997)'
_computing_data_collection       'Collect (Nonius BV, 1997-2000)'
_computing_data_reduction
;
HKL Denzo and Scalepack (Otwinowski & Minor 1997)
;
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device       '95mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'CCD rotation images, thick slices'
_diffrn_radiation_monochromator  'horizonally mounted graphite crystal'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0532
_diffrn_reflns_av_sigmaI/netI    0.0472
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            13707
_diffrn_reflns_theta_full        25.57
_diffrn_reflns_theta_max         25.57
_diffrn_reflns_theta_min         2.37
_diffrn_source                   'Enraf Nonius FR590'
_exptl_absorpt_coefficient_mu    3.374
_exptl_absorpt_correction_T_max  0.7780
_exptl_absorpt_correction_T_min  0.3664
_exptl_absorpt_correction_type   refdelf
_exptl_absorpt_process_details
;
Sheldrick, G.M. (anon) SHELX97 Release 97-2 (1998)
I/sigma threshold for reflections     =   5.000
Delta(U)/lambda**2                    =   0.000
Highest even order spherical harmonic =       6
Highest odd  order spherical harmonic =       3
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.485
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             554
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.393
_refine_diff_density_min         -1.079
_refine_diff_density_rms         0.109
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.081
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     297
_refine_ls_number_reflns         4541
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.081
_refine_ls_R_factor_all          0.0283
_refine_ls_R_factor_gt           0.0274
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0237P)²+1.2606P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0609
_refine_ls_wR_factor_ref         0.0614
_reflns_number_gt                4522
_reflns_number_total             4541
_reflns_threshold_expression     >2s(I)
_cod_data_source_file            2007-184_RS.txt
_cod_data_source_block           so18a=3
_cod_database_code               1512872
#BEGIN Tags that were not found in dictionaries:
_exptl_absorpt_rmerge_before     0.0548
_exptl_absorpt_rmerge_after      0.0364
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
U U 0.5000 0.5000 0.0000 0.01704(7) Uani 1 2 d S
O1 O 0.3774(3) 0.4459(3) 0.0744(2) 0.0353(6) Uani 1 1 d .
O3 O 0.6972(3) 0.3997(2) 0.1032(2) 0.0284(6) Uani 1 1 d .
O2 O 0.6005(3) 0.6513(2) 0.1328(2) 0.0348(6) Uani 1 1 d .
O4 O 1.4167(5) 0.4734(3) 0.6676(3) 0.0585(9) Uani 1 1 d .
H4 H 1.428(6) 0.445(5) 0.740(5) 0.070 Uiso 1 1 d .
N8 N 0.9172(3) 0.5962(3) 0.1979(2) 0.0193(6) Uani 1 1 d .
H8 H 0.826(5) 0.568(3) 0.179(3) 0.023 Uiso 1 1 d .
C1 C 0.6527(4) 0.7569(3) 0.1931(3) 0.0229(7) Uani 1 1 d .
C2 C 0.5543(4) 0.8250(3) 0.2331(3) 0.0259(8) Uani 1 1 d .
C3 C 0.6158(5) 0.9338(3) 0.2976(3) 0.0323(9) Uani 1 1 d .
H3 H 0.5488 0.9807 0.3240 0.039 Uiso 1 1 calc R
C4 C 0.7718(5) 0.9767(3) 0.3249(3) 0.0355(9) Uani 1 1 d .
C5 C 0.8687(4) 0.9058(3) 0.2866(3) 0.0300(8) Uani 1 1 d .
H5 H 0.9762 0.9314 0.3062 0.036 Uiso 1 1 calc R
C6 C 0.8109(4) 0.7987(3) 0.2204(3) 0.0222(7) Uani 1 1 d .
C7 C 0.9128(4) 0.7288(3) 0.1718(3) 0.0239(7) Uani 1 1 d .
H7A H 1.0198 0.7688 0.1993 0.029 Uiso 1 1 calc R
H7B H 0.8744 0.7324 0.0920 0.029 Uiso 1 1 calc R
C9 C 0.9885(4) 0.5243(3) 0.1267(3) 0.0220(7) Uani 1 1 d .
H9A H 0.9411 0.5451 0.0507 0.026 Uiso 1 1 calc R
H9B H 1.1011 0.5496 0.1492 0.026 Uiso 1 1 calc R
C10 C 0.9678(4) 0.3879(3) 0.1309(3) 0.0202(7) Uani 1 1 d .
C11 C 1.0940(4) 0.3161(3) 0.1406(3) 0.0258(8) Uani 1 1 d .
H11 H 1.1948 0.3554 0.1543 0.031 Uiso 1 1 calc R
C12 C 1.0742(5) 0.1889(4) 0.1307(3) 0.0330(9) Uani 1 1 d .
C13 C 0.9255(5) 0.1343(4) 0.1137(3) 0.0364(9) Uani 1 1 d .
H13 H 0.9110 0.0471 0.1082 0.044 Uiso 1 1 calc R
C14 C 0.7969(4) 0.2023(3) 0.1046(3) 0.0310(8) Uani 1 1 d .
C15 C 0.8182(4) 0.3307(3) 0.1119(3) 0.0235(7) Uani 1 1 d .
C16 C 0.9789(4) 0.5762(3) 0.3163(3) 0.0212(7) Uani 1 1 d .
H16A H 0.9647 0.4874 0.3252 0.025 Uiso 1 1 calc R
H16B H 0.9166 0.6201 0.3542 0.025 Uiso 1 1 calc R
C17 C 1.1491(4) 0.6190(4) 0.3704(3) 0.0272(8) Uani 1 1 d .
H17A H 1.1644 0.7084 0.3641 0.033 Uiso 1 1 calc R
H17B H 1.2128 0.5759 0.3332 0.033 Uiso 1 1 calc R
C18 C 1.2019(4) 0.5930(4) 0.4902(3) 0.0273(8) Uani 1 1 d .
H18A H 1.1392 0.6378 0.5272 0.033 Uiso 1 1 calc R
H18B H 1.1829 0.5040 0.4960 0.033 Uiso 1 1 calc R
C19 C 1.3735(4) 0.6316(4) 0.5471(3) 0.0326(9) Uani 1 1 d .
H19A H 1.4356 0.5897 0.5077 0.039 Uiso 1 1 calc R
H19B H 1.3913 0.7213 0.5436 0.039 Uiso 1 1 calc R
C20 C 1.4301(5) 0.6019(4) 0.6643(3) 0.0424(10) Uani 1 1 d .
H20A H 1.5400 0.6339 0.6989 0.051 Uiso 1 1 calc R
H20B H 1.3669 0.6407 0.7044 0.051 Uiso 1 1 calc R
C21 C 0.3849(4) 0.7799(4) 0.2065(4) 0.0370(9) Uani 1 1 d .
H21A H 0.3781 0.6962 0.2290 0.056 Uiso 1 1 calc R
H21B H 0.3321 0.7798 0.1281 0.056 Uiso 1 1 calc R
H21C H 0.3350 0.8344 0.2453 0.056 Uiso 1 1 calc R
C22 C 0.8341(6) 1.0977(4) 0.3907(4) 0.0541(13) Uani 1 1 d .
H22A H 0.9397 1.0902 0.4399 0.081 Uiso 1 1 calc R
H22B H 0.7666 1.1195 0.4331 0.081 Uiso 1 1 calc R
H22C H 0.8365 1.1620 0.3416 0.081 Uiso 1 1 calc R
C23 C 1.2094(6) 0.1121(5) 0.1360(4) 0.0517(12) Uani 1 1 d .
H23A H 1.2448 0.1259 0.0738 0.078 Uiso 1 1 calc R
H23B H 1.1762 0.0249 0.1341 0.078 Uiso 1 1 calc R
H23C H 1.2948 0.1358 0.2036 0.078 Uiso 1 1 calc R
C24 C 0.6369(5) 0.1404(4) 0.0848(4) 0.0428(11) Uani 1 1 d .
H24A H 0.5961 0.1700 0.1419 0.064 Uiso 1 1 calc R
H24B H 0.6432 0.0512 0.0858 0.064 Uiso 1 1 calc R
H24C H 0.5673 0.1598 0.0140 0.064 Uiso 1 1 calc R
N1 N 1.2889(7) 0.0146(7) 0.4028(5) 0.0925(18) Uani 1 1 d .
C25 C 1.2749(6) 0.1135(7) 0.4327(5) 0.0689(16) Uani 1 1 d .
C26 C 1.2512(8) 0.2366(6) 0.4684(6) 0.0828(19) Uani 1 1 d .
H26A H 1.2322 0.2890 0.4075 0.124 Uiso 1 1 calc R
H26B H 1.3440 0.2703 0.5275 0.124 Uiso 1 1 calc R
H26C H 1.1612 0.2338 0.4942 0.124 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 U O1 180.00(17) . 2_665
O1 U O3 90.48(11) . .
O1 U O3 89.52(11) 2_665 .
O1 U O3 89.52(11) . 2_665
O1 U O3 90.48(11) 2_665 2_665
O3 U O3 180.0 . 2_665
O1 U O2 91.64(12) . 2_665
O1 U O2 88.36(12) 2_665 2_665
O3 U O2 97.28(9) . 2_665
O3 U O2 82.72(9) 2_665 2_665
O1 U O2 88.36(12) . .
O1 U O2 91.64(12) 2_665 .
O3 U O2 82.72(9) . .
O3 U O2 97.28(9) 2_665 .
O2 U O2 180.00(12) 2_665 .
C15 O3 U 149.8(2) . .
C1 O2 U 167.2(2) . .
C20 O4 H4 115(3) . .
C16 N8 C9 115.4(3) . .
C16 N8 C7 115.1(3) . .
C9 N8 C7 110.2(3) . .
C16 N8 H8 104(3) . .
C9 N8 H8 104(3) . .
C7 N8 H8 106(3) . .
O2 C1 C2 121.0(3) . .
O2 C1 C6 119.6(3) . .
C2 C1 C6 119.4(3) . .
C3 C2 C1 118.6(3) . .
C3 C2 C21 121.4(3) . .
C1 C2 C21 120.0(3) . .
C4 C3 C2 122.7(3) . .
C4 C3 H3 118.7 . .
C2 C3 H3 118.7 . .
C5 C4 C3 117.8(3) . .
C5 C4 C22 120.5(4) . .
C3 C4 C22 121.7(4) . .
C6 C5 C4 121.1(3) . .
C6 C5 H5 119.5 . .
C4 C5 H5 119.5 . .
C5 C6 C1 120.4(3) . .
C5 C6 C7 120.7(3) . .
C1 C6 C7 118.8(3) . .
C6 C7 N8 112.7(3) . .
C6 C7 H7A 109.0 . .
N8 C7 H7A 109.0 . .
C6 C7 H7B 109.0 . .
N8 C7 H7B 109.0 . .
H7A C7 H7B 107.8 . .
C10 C9 N8 113.5(3) . .
C10 C9 H9A 108.9 . .
N8 C9 H9A 108.9 . .
C10 C9 H9B 108.9 . .
N8 C9 H9B 108.9 . .
H9A C9 H9B 107.7 . .
C11 C10 C15 119.9(3) . .
C11 C10 C9 119.9(3) . .
C15 C10 C9 119.8(3) . .
C12 C11 C10 121.2(3) . .
C12 C11 H11 119.4 . .
C10 C11 H11 119.4 . .
C11 C12 C13 117.9(3) . .
C11 C12 C23 120.9(4) . .
C13 C12 C23 121.3(4) . .
C12 C13 C14 122.8(4) . .
C12 C13 H13 118.6 . .
C14 C13 H13 118.6 . .
C13 C14 C15 118.5(3) . .
C13 C14 C24 121.5(4) . .
C15 C14 C24 119.9(3) . .
O3 C15 C14 120.5(3) . .
O3 C15 C10 119.9(3) . .
C14 C15 C10 119.6(3) . .
N8 C16 C17 114.3(3) . .
N8 C16 H16A 108.7 . .
C17 C16 H16A 108.7 . .
N8 C16 H16B 108.7 . .
C17 C16 H16B 108.7 . .
H16A C16 H16B 107.6 . .
C16 C17 C18 110.5(3) . .
C16 C17 H17A 109.6 . .
C18 C17 H17A 109.6 . .
C16 C17 H17B 109.6 . .
C18 C17 H17B 109.6 . .
H17A C17 H17B 108.1 . .
C19 C18 C17 112.3(3) . .
C19 C18 H18A 109.2 . .
C17 C18 H18A 109.2 . .
C19 C18 H18B 109.2 . .
C17 C18 H18B 109.2 . .
H18A C18 H18B 107.9 . .
C20 C19 C18 113.2(3) . .
C20 C19 H19A 108.9 . .
C18 C19 H19A 108.9 . .
C20 C19 H19B 108.9 . .
C18 C19 H19B 108.9 . .
H19A C19 H19B 107.7 . .
O4 C20 C19 108.4(3) . .
O4 C20 H20A 110.0 . .
C19 C20 H20A 110.0 . .
O4 C20 H20B 110.0 . .
C19 C20 H20B 110.0 . .
H20A C20 H20B 108.4 . .
C2 C21 H21A 109.5 . .
C2 C21 H21B 109.5 . .
H21A C21 H21B 109.5 . .
C2 C21 H21C 109.5 . .
H21A C21 H21C 109.5 . .
H21B C21 H21C 109.5 . .
C4 C22 H22A 109.5 . .
C4 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C4 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C12 C23 H23A 109.5 . .
C12 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
C12 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
C14 C24 H24A 109.5 . .
C14 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C14 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
N1 C25 C26 177.9(7) . .
C25 C26 H26A 109.5 . .
C25 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
C25 C26 H26C 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U O1 1.796(2) .
U O1 1.796(2) 2_665
U O3 2.250(2) .
U O3 2.250(2) 2_665
U O2 2.250(2) 2_665
U O2 2.250(2) .
O3 C15 1.348(4) .
O2 C1 1.332(4) .
O4 C20 1.406(6) .
O4 H4 0.98(6) .
N8 C16 1.497(4) .
N8 C9 1.504(4) .
N8 C7 1.507(4) .
N8 H8 0.82(4) .
C1 C2 1.399(5) .
C1 C6 1.410(5) .
C2 C3 1.396(5) .
C2 C21 1.515(5) .
C3 C4 1.395(6) .
C3 H3 0.9500 .
C4 C5 1.393(6) .
C4 C22 1.512(5) .
C5 C6 1.386(5) .
C5 H5 0.9500 .
C6 C7 1.499(5) .
C7 H7A 0.9900 .
C7 H7B 0.9900 .
C9 C10 1.498(5) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
C10 C11 1.402(5) .
C10 C15 1.407(5) .
C11 C12 1.385(5) .
C11 H11 0.9500 .
C12 C13 1.393(6) .
C12 C23 1.513(6) .
C13 C14 1.398(6) .
C13 H13 0.9500 .
C14 C15 1.398(5) .
C14 C24 1.509(5) .
C16 C17 1.516(5) .
C16 H16A 0.9900 .
C16 H16B 0.9900 .
C17 C18 1.527(5) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 C19 1.522(5) .
C18 H18A 0.9900 .
C18 H18B 0.9900 .
C19 C20 1.509(5) .
C19 H19A 0.9900 .
C19 H19B 0.9900 .
C20 H20A 0.9900 .
C20 H20B 0.9900 .
C21 H21A 0.9800 .
C21 H21B 0.9800 .
C21 H21C 0.9800 .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
C23 H23A 0.9800 .
C23 H23B 0.9800 .
C23 H23C 0.9800 .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
N1 C25 1.156(8) .
C25 C26 1.449(9) .
C26 H26A 0.9800 .
C26 H26B 0.9800 .
C26 H26C 0.9800 .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O4 H4 O2 0.98(6) 2.09(6) 3.048(5) 164(5) 2_766
N8 H8 O3 0.82(4) 2.13(4) 2.790(4) 137(3) .
N8 H8 O2 0.82(4) 2.21(4) 2.841(4) 134(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
O1 U O3 C15 139.4(4) .
O1 U O3 C15 -40.6(4) 2_665
O3 U O3 C15 -48(95) 2_665
O2 U O3 C15 47.7(4) 2_665
O2 U O3 C15 -132.3(4) .
O1 U O2 C1 -129.1(10) .
O1 U O2 C1 50.9(10) 2_665
O3 U O2 C1 140.2(10) .
O3 U O2 C1 -39.8(10) 2_665
O2 U O2 C1 163(100) 2_665
U O2 C1 C2 90.0(11) .
U O2 C1 C6 -92.3(10) .
O2 C1 C2 C3 178.8(3) .
C6 C1 C2 C3 1.1(5) .
O2 C1 C2 C21 -0.9(5) .
C6 C1 C2 C21 -178.7(3) .
C1 C2 C3 C4 -0.8(6) .
C21 C2 C3 C4 178.9(4) .
C2 C3 C4 C5 -0.8(6) .
C2 C3 C4 C22 177.2(4) .
C3 C4 C5 C6 2.3(6) .
C22 C4 C5 C6 -175.7(4) .
C4 C5 C6 C1 -2.1(6) .
C4 C5 C6 C7 174.8(4) .
O2 C1 C6 C5 -177.4(3) .
C2 C1 C6 C5 0.3(5) .
O2 C1 C6 C7 5.7(5) .
C2 C1 C6 C7 -176.5(3) .
C5 C6 C7 N8 125.0(3) .
C1 C6 C7 N8 -58.1(4) .
C16 N8 C7 C6 -60.9(4) .
C9 N8 C7 C6 166.6(3) .
C16 N8 C9 C10 59.5(4) .
C7 N8 C9 C10 -168.1(3) .
N8 C9 C10 C11 -134.8(3) .
N8 C9 C10 C15 52.8(4) .
C15 C10 C11 C12 0.7(5) .
C9 C10 C11 C12 -171.6(3) .
C10 C11 C12 C13 -1.8(5) .
C10 C11 C12 C23 177.1(4) .
C11 C12 C13 C14 1.2(6) .
C23 C12 C13 C14 -177.7(4) .
C12 C13 C14 C15 0.5(6) .
C12 C13 C14 C24 179.2(4) .
U O3 C15 C14 -91.9(5) .
U O3 C15 C10 89.5(5) .
C13 C14 C15 O3 179.8(3) .
C24 C14 C15 O3 1.1(5) .
C13 C14 C15 C10 -1.6(5) .
C24 C14 C15 C10 179.7(3) .
C11 C10 C15 O3 179.6(3) .
C9 C10 C15 O3 -8.1(5) .
C11 C10 C15 C14 1.0(5) .
C9 C10 C15 C14 173.3(3) .
C9 N8 C16 C17 64.6(4) .
C7 N8 C16 C17 -65.4(4) .
N8 C16 C17 C18 -179.1(3) .
C16 C17 C18 C19 178.5(3) .
C17 C18 C19 C20 -177.6(3) .
C18 C19 C20 O4 63.6(5) .
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1 PubChem 139041527
