#------------------------------------------------------------------------------
#$Date: 2025-08-21 00:01:10 +0200 (Thu 21 de Aug de 2025) $
#$Revision: 301838 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/03/4320349.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4320349
loop_
_publ_author_name
'Svilen Bobev'
'Slavi C. Sevov'
_publ_contact_author
;
Slavi C. Sevov
Department of Chemistry and Biochemistry
251 Nieuwland Science Hall
University of Notre Dame
Notre Dame, IN 46556-5670
USA
;
_publ_contact_author_email       ssevov@nd.edu
_publ_contact_author_fax         'Intl. Code + (219)631-6652'
_publ_contact_author_phone       'Intl. Code + (219)631-5891'
_publ_section_title
;
 Synthesis and Characterization of the Largest Isolated Clusters of Tin,
 [Sn12]12-, in (AE)Na10Sn12 (AE = Ca or Sr)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5361
_journal_page_last               5364
_journal_paper_doi               10.1021/ic0103953
_journal_volume                  40
_journal_year                    2001
_chemical_formula_moiety         CaNa10Sn12
_chemical_formula_sum            'Ca Na10 Sn12'
_chemical_formula_weight         1694.26
_chemical_melting_point          ?
_chemical_name_common            CaNa10Sn12
_space_group_IT_number           217
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  'I -4 2 3'
_symmetry_space_group_name_H-M   'I -4 3 m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   11.1847(6)
_cell_length_b                   11.1847(6)
_cell_length_c                   11.1847(6)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      13.48
_cell_measurement_theta_min      12.69
_cell_volume                     1399.18(13)
_computing_cell_refinement       CAD4_(Enraf-Nonius,_1977)
_computing_data_collection       CAD4_(Enraf-Nonius,_1977)
_computing_data_reduction        SDS_Package_(Enraf-Nonius,_1985)
_computing_molecular_graphics    'SHELXTL (Siemens, 1994)'
_computing_publication_material  'SHELXTL (Siemens, 1994)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  Enraf_Nonius_CAD4
_diffrn_measurement_method       omega-2theta
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0330
_diffrn_reflns_av_sigmaI/netI    0.0196
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            1168
_diffrn_reflns_theta_full        29.89
_diffrn_reflns_theta_max         29.89
_diffrn_reflns_theta_min         2.58
_diffrn_standards_interval_count 200
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    10.831
_exptl_absorpt_correction_T_max  0.3124
_exptl_absorpt_correction_T_min  0.2459
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   'average of 6 psi-scan reflections'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    4.021
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       bar
_exptl_crystal_F_000             1460
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_refine_diff_density_max         0.326
_refine_diff_density_min         -0.391
_refine_diff_density_rms         0.091
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.00(11)
_refine_ls_extinction_coef       0.0049(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.247
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     15
_refine_ls_number_reflns         235
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.247
_refine_ls_R_factor_all          0.0136
_refine_ls_R_factor_gt           0.0131
_refine_ls_shift/su_max          0.071
_refine_ls_shift/su_mean         0.065
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0083P)²+0.1566P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0293
_refine_ls_wR_factor_ref         0.0295
_reflns_number_gt                233
_reflns_number_total             235
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0103953_1.cif
_cod_data_source_block           CaNa10Sn12
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value 'not measured' was changed to '?' -
the value is undefined or not given.

'_symmetry_cell_setting' value
'Cubic' changed to 'cubic' according to the built-in table from CIF
Core dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        1399.2(1)
_cod_database_code               4320349
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'z, x, y'
'z, -x, -y'
'-z, -x, y'
'-z, x, -y'
'y, z, x'
'-y, z, -x'
'y, -z, -x'
'-y, -z, x'
'y, x, z'
'-y, -x, z'
'y, -x, -z'
'-y, x, -z'
'x, z, y'
'-x, z, -y'
'-x, -z, y'
'x, -z, -y'
'z, y, x'
'z, -y, -x'
'-z, y, -x'
'-z, -y, x'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'z+1/2, x+1/2, y+1/2'
'z+1/2, -x+1/2, -y+1/2'
'-z+1/2, -x+1/2, y+1/2'
'-z+1/2, x+1/2, -y+1/2'
'y+1/2, z+1/2, x+1/2'
'-y+1/2, z+1/2, -x+1/2'
'y+1/2, -z+1/2, -x+1/2'
'-y+1/2, -z+1/2, x+1/2'
'y+1/2, x+1/2, z+1/2'
'-y+1/2, -x+1/2, z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'-y+1/2, x+1/2, -z+1/2'
'x+1/2, z+1/2, y+1/2'
'-x+1/2, z+1/2, -y+1/2'
'-x+1/2, -z+1/2, y+1/2'
'x+1/2, -z+1/2, -y+1/2'
'z+1/2, y+1/2, x+1/2'
'z+1/2, -y+1/2, -x+1/2'
'-z+1/2, y+1/2, -x+1/2'
'-z+1/2, -y+1/2, x+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn Sn 0.09068(2) 0.09068(2) 0.27800(3) 0.02674(13) Uani 1 2 d S . .
Na2 Na 0.2500 0.5000 0.0000 0.0404(7) Uani 1 4 d S . .
Na1 Na 0.30613(17) 0.30613(17) 0.30613(17) 0.0347(9) Uani 1 6 d S . .
Ca Ca 0.0000 0.0000 0.0000 0.0151(5) Uani 1 24 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Sn Sn Sn 120.0 2 9 ?
Sn Sn Sn 120.0 2 5 ?
Sn Sn Sn 60.0 9 5 ?
Sn Sn Na2 99.706(6) 2 5 ?
Sn Sn Na2 98.854(5) 9 5 ?
Sn Sn Na2 140.170(6) 5 5 ?
Sn Sn Na2 99.706(6) 2 26 ?
Sn Sn Na2 140.170(6) 9 26 ?
Sn Sn Na2 98.854(5) 5 26 ?
Na2 Sn Na2 75.761(7) 5 26 ?
Sn Sn Na1 174.72(3) 2 . ?
Sn Sn Na1 64.35(2) 9 . ?
Sn Sn Na1 64.35(2) 5 . ?
Na2 Sn Na1 76.19(2) 5 . ?
Na2 Sn Na1 76.19(2) 26 . ?
Sn Sn Ca 65.238(6) 2 . ?
Sn Sn Ca 64.364(5) 9 . ?
Sn Sn Ca 64.364(5) 5 . ?
Na2 Sn Ca 140.425(4) 5 . ?
Na2 Sn Ca 140.425(4) 26 . ?
Na1 Sn Ca 120.04(3) . . ?
Sn Sn Na1 65.908(14) 2 28_455 ?
Sn Sn Na1 65.061(15) 9 28_455 ?
Sn Sn Na1 116.81(3) 5 28_455 ?
Na2 Sn Na1 74.90(5) 5 28_455 ?
Na2 Sn Na1 144.21(4) 26 28_455 ?
Na1 Sn Na1 115.54(3) . 28_455 ?
Ca Sn Na1 65.53(5) . 28_455 ?
Sn Sn Na1 65.908(14) 2 27_545 ?
Sn Sn Na1 116.81(3) 9 27_545 ?
Sn Sn Na1 65.061(15) 5 27_545 ?
Na2 Sn Na1 144.21(4) 5 27_545 ?
Na2 Sn Na1 74.90(5) 26 27_545 ?
Na1 Sn Na1 115.54(3) . 27_545 ?
Ca Sn Na1 65.53(5) . 27_545 ?
Na1 Sn Na1 121.55(7) 28_455 27_545 ?
Sn Sn Na2 42.934(3) 2 6_556 ?
Sn Sn Na2 162.749(3) 9 6_556 ?
Sn Sn Na2 122.052(2) 5 6_556 ?
Na2 Sn Na2 88.458(8) 5 6_556 ?
Na2 Sn Na2 56.771(5) 26 6_556 ?
Na1 Sn Na2 132.85(2) . 6_556 ?
Ca Sn Na2 100.207(7) . 6_556 ?
Na1 Sn Na2 102.367(9) 28_455 6_556 ?
Na1 Sn Na2 58.23(2) 27_545 6_556 ?
Sn Sn Na2 42.934(3) 2 25_445 ?
Sn Sn Na2 122.052(2) 9 25_445 ?
Sn Sn Na2 162.749(3) 5 25_445 ?
Na2 Sn Na2 56.771(5) 5 25_445 ?
Na2 Sn Na2 88.458(8) 26 25_445 ?
Na1 Sn Na2 132.85(2) . 25_445 ?
Ca Sn Na2 100.207(7) . 25_445 ?
Na1 Sn Na2 58.23(2) 28_455 25_445 ?
Na1 Sn Na2 102.367(9) 27_545 25_445 ?
Na2 Sn Na2 50.215(4) 6_556 25_445 ?
Sn Sn Na2 122.428(3) 2 34 ?
Sn Sn Na2 42.611(4) 9 34 ?
Sn Sn Na2 96.055(4) 5 34 ?
Na2 Sn Na2 56.243(2) 5 34 ?
Na2 Sn Na2 118.531(7) 26 34 ?
Na1 Sn Na2 58.140(5) . 34 ?
Ca Sn Na2 99.444(5) . 34 ?
Na1 Sn Na2 57.77(2) 28_455 34 ?
Na1 Sn Na2 159.29(3) 27_545 34 ?
Na2 Sn Na2 141.734(6) 6_556 34 ?
Na2 Sn Na2 94.076(2) 25_445 34 ?
Sn Sn Na2 122.428(3) 2 9 ?
Sn Sn Na2 96.055(4) 9 9 ?
Sn Sn Na2 42.611(4) 5 9 ?
Na2 Sn Na2 118.531(7) 5 9 ?
Na2 Sn Na2 56.243(2) 26 9 ?
Na1 Sn Na2 58.140(5) . 9 ?
Ca Sn Na2 99.444(5) . 9 ?
Na1 Sn Na2 159.29(3) 28_455 9 ?
Na1 Sn Na2 57.77(2) 27_545 9 ?
Na2 Sn Na2 94.076(2) 6_556 9 ?
Na2 Sn Na2 141.734(6) 25_445 9 ?
Na2 Sn Na2 114.583(7) 34 9 ?
Sn Sn Sn 90.537(7) 2 10 ?
Sn Sn Sn 29.464(7) 9 10 ?
Sn Sn Sn 72.942(4) 5 10 ?
Na2 Sn Sn 105.872(5) 5 10 ?
Na2 Sn Sn 169.254(13) 26 10 ?
Na1 Sn Sn 93.77(3) . 10 ?
Ca Sn Sn 42.484(1) . 10 ?
Na1 Sn Sn 44.05(3) 28_455 10 ?
Na1 Sn Sn 106.80(4) 27_545 10 ?
Na2 Sn Sn 133.384(9) 6_556 10 ?
Na2 Sn Sn 101.358(5) 25_445 10 ?
Na2 Sn Sn 56.961(6) 34 10 ?
Na2 Sn Sn 115.236(8) 9 10 ?
Sn Sn Sn 90.537(7) 2 6 ?
Sn Sn Sn 72.942(4) 9 6 ?
Sn Sn Sn 29.464(7) 5 6 ?
Na2 Sn Sn 169.254(13) 5 6 ?
Na2 Sn Sn 105.872(5) 26 6 ?
Na1 Sn Sn 93.77(3) . 6 ?
Ca Sn Sn 42.484(1) . 6 ?
Na1 Sn Sn 106.80(4) 28_455 6 ?
Na1 Sn Sn 44.05(3) 27_545 6 ?
Na2 Sn Sn 101.358(5) 6_556 6 ?
Na2 Sn Sn 133.384(9) 25_445 6 ?
Na2 Sn Sn 115.236(8) 34 6 ?
Na2 Sn Sn 56.961(6) 9 6 ?
Sn Sn Sn 70.5 10 6 ?
Sn Sn Sn 30.537(7) 2 12 ?
Sn Sn Sn 106.498(4) 9 12 ?
Sn Sn Sn 89.464(7) 5 12 ?
Na2 Sn Sn 130.181(13) 5 12 ?
Na2 Sn Sn 106.557(6) 26 12 ?
Na1 Sn Sn 153.61(2) . 12 ?
Ca Sn Sn 42.484(1) . 12 ?
Na1 Sn Sn 78.07(3) 28_455 12 ?
Na1 Sn Sn 44.05(3) 27_545 12 ?
Na2 Sn Sn 57.723(6) 6_556 12 ?
Na2 Sn Sn 73.437(9) 25_445 12 ?
Na2 Sn Sn 132.925(4) 34 12 ?
Na2 Sn Sn 100.800(4) 9 12 ?
Sn Sn Sn 80.718(4) 10 12 ?
Sn Sn Sn 60.0 6 12 ?
Sn Sn Sn 30.537(7) 2 7 ?
Sn Sn Sn 89.464(7) 9 7 ?
Sn Sn Sn 106.498(4) 5 7 ?
Na2 Sn Sn 106.557(6) 5 7 ?
Na2 Sn Sn 130.181(13) 26 7 ?
Na1 Sn Sn 153.61(2) . 7 ?
Ca Sn Sn 42.484(1) . 7 ?
Na1 Sn Sn 44.05(3) 28_455 7 ?
Na1 Sn Sn 78.07(3) 27_545 7 ?
Na2 Sn Sn 73.437(9) 6_556 7 ?
Na2 Sn Sn 57.723(6) 25_445 7 ?
Na2 Sn Sn 100.800(4) 34 7 ?
Na2 Sn Sn 132.925(4) 9 7 ?
Sn Sn Sn 60.0 10 7 ?
Sn Sn Sn 80.718(4) 6 7 ?
Sn Sn Sn 34.117(7) 12 7 ?
Sn Sn Sn 133.136(5) 2 36 ?
Sn Sn Sn 105.997(4) 9 36 ?
Sn Sn Sn 89.480(7) 5 36 ?
Na2 Sn Sn 62.704(5) 5 36 ?
Na2 Sn Sn 36.083(3) 26 36 ?
Na1 Sn Sn 42.05(3) . 36 ?
Ca Sn Sn 153.705(11) . 36 ?
Na1 Sn Sn 135.03(4) 28_455 36 ?
Na1 Sn Sn 102.16(4) 27_545 36 ?
Na2 Sn Sn 91.247(3) 6_556 36 ?
Na2 Sn Sn 105.268(7) 25_445 36 ?
Na2 Sn Sn 85.277(6) 34 36 ?
Na2 Sn Sn 55.849(6) 9 36 ?
Sn Sn Sn 134.954(10) 10 36 ?
Sn Sn Sn 112.201(11) 6 36 ?
Sn Sn Sn 141.642(3) 12 36 ?
Sn Sn Sn 162.018(12) 7 36 ?
Sn Sn Sn 133.136(5) 2 31 ?
Sn Sn Sn 89.480(7) 9 31 ?
Sn Sn Sn 105.997(5) 5 31 ?
Na2 Sn Sn 36.083(3) 5 31 ?
Na2 Sn Sn 62.704(5) 26 31 ?
Na1 Sn Sn 42.05(3) . 31 ?
Ca Sn Sn 153.705(11) . 31 ?
Na1 Sn Sn 102.16(4) 28_455 31 ?
Na1 Sn Sn 135.03(4) 27_545 31 ?
Na2 Sn Sn 105.268(7) 6_556 31 ?
Na2 Sn Sn 91.247(3) 25_445 31 ?
Na2 Sn Sn 55.849(6) 34 31 ?
Na2 Sn Sn 85.277(6) 9 31 ?
Sn Sn Sn 112.201(11) 10 31 ?
Sn Sn Sn 134.954(10) 6 31 ?
Sn Sn Sn 162.018(12) 12 31 ?
Sn Sn Sn 141.642(3) 7 31 ?
Sn Sn Sn 33.077(8) 36 31 ?
Sn Sn Sn 90.520(7) 2 34_545 ?
Sn Sn Sn 132.428(5) 9 34_545 ?
Sn Sn Sn 73.462(4) 5 34_545 ?
Na2 Sn Sn 111.710(6) 5 34_545 ?
Na2 Sn Sn 36.083(3) 26 34_545 ?
Na1 Sn Sn 87.995(10) . 34_545 ?
Ca Sn Sn 105.073(5) . 34_545 ?
Na1 Sn Sn 156.419(18) 28_455 34_545 ?
Na1 Sn Sn 40.72(4) 27_545 34_545 ?
Na2 Sn Sn 56.580(4) 6_556 34_545 ?
Na2 Sn Sn 105.268(7) 25_445 34_545 ?
Na2 Sn Sn 145.198(9) 34 34_545 ?
Na2 Sn Sn 37.509(2) 9 34_545 ?
Sn Sn Sn 141.643(3) 10 34_545 ?
Sn Sn Sn 71.124(3) 6 34_545 ?
Sn Sn Sn 80.995(4) 12 34_545 ?
Sn Sn Sn 113.973(11) 7 34_545 ?
Sn Sn Sn 62.037(7) 36 34_545 ?
Sn Sn Sn 94.431(4) 31 34_545 ?
Sn Na2 Sn 107.833(6) 27 9 ?
Sn Na2 Sn 112.799(12) 27 26_554 ?
Sn Na2 Sn 107.833(6) 9 26_554 ?
Sn Na2 Sn 107.833(6) 27 11_565 ?
Sn Na2 Sn 112.799(12) 9 11_565 ?
Sn Na2 Sn 107.833(6) 26_554 11_565 ?
Sn Na2 Na2 159.479(6) 27 33_454 ?
Sn Na2 Na2 80.293(6) 9 33_454 ?
Sn Na2 Na2 81.146(5) 26_554 33_454 ?
Sn Na2 Na2 52.119(3) 11_565 33_454 ?
Sn Na2 Na2 52.119(3) 27 29_554 ?
Sn Na2 Na2 159.479(6) 9 29_554 ?
Sn Na2 Na2 80.293(6) 26_554 29_554 ?
Sn Na2 Na2 81.146(5) 11_565 29_554 ?
Na2 Na2 Na2 120.0 33_454 29_554 ?
Sn Na2 Na2 81.146(5) 27 34 ?
Sn Na2 Na2 52.119(3) 9 34 ?
Sn Na2 Na2 159.479(6) 26_554 34 ?
Sn Na2 Na2 80.293(6) 11_565 34 ?
Na2 Na2 Na2 90.0 33_454 34 ?
Na2 Na2 Na2 120.0 29_554 34 ?
Sn Na2 Na2 80.293(6) 27 30 ?
Sn Na2 Na2 81.146(5) 9 30 ?
Sn Na2 Na2 52.119(3) 26_554 30 ?
Sn Na2 Na2 159.479(6) 11_565 30 ?
Na2 Na2 Na2 120.0 33_454 30 ?
Na2 Na2 Na2 90.0 29_554 30 ?
Na2 Na2 Na2 120.0 34 30 ?
Sn Na2 Na1 55.81(5) 27 . ?
Sn Na2 Na1 54.13(4) 9 . ?
Sn Na2 Na1 113.111(11) 26_554 . ?
Sn Na2 Na1 139.055(12) 11_565 . ?
Na2 Na2 Na1 134.32(4) 33_454 . ?
Na2 Na2 Na1 105.40(4) 29_554 . ?
Na2 Na2 Na1 61.177(7) 34 . ?
Na2 Na2 Na1 61.177(7) 30 . ?
Sn Na2 Na1 139.055(12) 27 26_554 ?
Sn Na2 Na1 55.81(5) 9 26_554 ?
Sn Na2 Na1 54.13(4) 26_554 26_554 ?
Sn Na2 Na1 113.111(11) 11_565 26_554 ?
Na2 Na2 Na1 61.177(7) 33_454 26_554 ?
Na2 Na2 Na1 134.32(4) 29_554 26_554 ?
Na2 Na2 Na1 105.40(4) 34 26_554 ?
Na2 Na2 Na1 61.177(7) 30 26_554 ?
Na1 Na2 Na1 91.343(8) . 26_554 ?
Sn Na2 Na1 54.13(4) 27 27 ?
Sn Na2 Na1 113.111(11) 9 27 ?
Sn Na2 Na1 139.055(12) 26_554 27 ?
Sn Na2 Na1 55.81(5) 11_565 27 ?
Na2 Na2 Na1 105.40(4) 33_454 27 ?
Na2 Na2 Na1 61.177(7) 29_554 27 ?
Na2 Na2 Na1 61.177(7) 34 27 ?
Na2 Na2 Na1 134.32(4) 30 27 ?
Na1 Na2 Na1 91.343(8) . 27 ?
Na1 Na2 Na1 162.39(5) 26_554 27 ?
Sn Na2 Na1 113.111(11) 27 4_565 ?
Sn Na2 Na1 139.055(12) 9 4_565 ?
Sn Na2 Na1 55.81(5) 26_554 4_565 ?
Sn Na2 Na1 54.13(4) 11_565 4_565 ?
Na2 Na2 Na1 61.177(7) 33_454 4_565 ?
Na2 Na2 Na1 61.177(7) 29_554 4_565 ?
Na2 Na2 Na1 134.32(4) 34 4_565 ?
Na2 Na2 Na1 105.40(4) 30 4_565 ?
Na1 Na2 Na1 162.39(5) . 4_565 ?
Na1 Na2 Na1 91.343(8) 26_554 4_565 ?
Na1 Na2 Na1 91.343(8) 27 4_565 ?
Sn Na2 Sn 142.016(4) 27 10 ?
Sn Na2 Sn 37.359(8) 9 10 ?
Sn Na2 Sn 96.712(8) 26_554 10 ?
Sn Na2 Sn 83.672(7) 11_565 10 ?
Na2 Na2 Sn 42.935(3) 33_454 10 ?
Na2 Na2 Sn 162.749(3) 29_554 10 ?
Na2 Na2 Sn 64.892(2) 34 10 ?
Na2 Na2 Sn 101.621(3) 30 10 ?
Na1 Na2 Sn 91.44(4) . 10 ?
Na1 Na2 Sn 46.75(3) 26_554 10 ?
Na1 Na2 Sn 115.77(2) 27 10 ?
Na1 Na2 Sn 103.014(3) 4_565 10 ?
Sn Na2 Sn 37.359(8) 27 28 ?
Sn Na2 Sn 96.712(8) 9 28 ?
Sn Na2 Sn 83.672(7) 26_554 28 ?
Sn Na2 Sn 142.016(4) 11_565 28 ?
Na2 Na2 Sn 162.749(3) 33_454 28 ?
Na2 Na2 Sn 64.892(2) 29_554 28 ?
Na2 Na2 Sn 101.621(3) 34 28 ?
Na2 Na2 Sn 42.935(3) 30 28 ?
Na1 Na2 Sn 46.75(3) . 28 ?
Na1 Na2 Sn 103.014(3) 26_554 28 ?
Na1 Na2 Sn 91.44(4) 27 28 ?
Na1 Na2 Sn 115.77(2) 4_565 28 ?
Sn Na2 Sn 131.966(4) 10 28 ?
Sn Na2 Sn 83.672(7) 27 25_554 ?
Sn Na2 Sn 142.016(4) 9 25_554 ?
Sn Na2 Sn 37.359(9) 26_554 25_554 ?
Sn Na2 Sn 96.712(8) 11_565 25_554 ?
Na2 Na2 Sn 101.621(3) 33_454 25_554 ?
Na2 Na2 Sn 42.935(3) 29_554 25_554 ?
Na2 Na2 Sn 162.749(3) 34 25_554 ?
Na2 Na2 Sn 64.892(2) 30 25_554 ?
Na1 Na2 Sn 115.77(2) . 25_554 ?
Na1 Na2 Sn 91.44(4) 26_554 25_554 ?
Na1 Na2 Sn 103.014(3) 27 25_554 ?
Na1 Na2 Sn 46.75(3) 4_565 25_554 ?
Sn Na2 Sn 131.966(4) 10 25_554 ?
Sn Na2 Sn 70.282(6) 28 25_554 ?
Sn Na2 Sn 96.712(8) 27 12_565 ?
Sn Na2 Sn 83.672(7) 9 12_565 ?
Sn Na2 Sn 142.016(4) 26_554 12_565 ?
Sn Na2 Sn 37.359(9) 11_565 12_565 ?
Na2 Na2 Sn 64.892(2) 33_454 12_565 ?
Na2 Na2 Sn 101.621(3) 29_554 12_565 ?
Na2 Na2 Sn 42.935(3) 34 12_565 ?
Na2 Na2 Sn 162.749(3) 30 12_565 ?
Na1 Na2 Sn 103.014(3) . 12_565 ?
Na1 Na2 Sn 115.77(2) 26_554 12_565 ?
Na1 Na2 Sn 46.75(3) 27 12_565 ?
Na1 Na2 Sn 91.44(4) 4_565 12_565 ?
Sn Na2 Sn 70.282(6) 10 12_565 ?
Sn Na2 Sn 131.966(4) 28 12_565 ?
Sn Na2 Sn 131.966(4) 25_554 12_565 ?
Sn Na2 Sn 148.871(4) 27 31_554 ?
Sn Na2 Sn 95.943(2) 9 31_554 ?
Sn Na2 Sn 38.535(9) 26_554 31_554 ?
Sn Na2 Sn 79.787(4) 11_565 31_554 ?
Na2 Na2 Sn 42.611(4) 33_454 31_554 ?
Na2 Na2 Sn 101.521(3) 29_554 31_554 ?
Na2 Na2 Sn 129.919(4) 34 31_554 ?
Na2 Na2 Sn 83.946(4) 30 31_554 ?
Na1 Na2 Sn 135.19(4) . 31_554 ?
Na1 Na2 Sn 45.14(4) 26_554 31_554 ?
Na1 Na2 Sn 133.24(4) 27 31_554 ?
Na1 Na2 Sn 46.45(3) 4_565 31_554 ?
Sn Na2 Sn 67.572(4) 10 31_554 ?
Sn Na2 Sn 121.778(4) 28 31_554 ?
Sn Na2 Sn 65.316(7) 25_554 31_554 ?
Sn Na2 Sn 105.814(6) 12_565 31_554 ?
Sn Na2 Sn 38.535(9) 27 32 ?
Sn Na2 Sn 79.787(4) 9 32 ?
Sn Na2 Sn 148.871(4) 26_554 32 ?
Sn Na2 Sn 95.943(2) 11_565 32 ?
Na2 Na2 Sn 129.919(4) 33_454 32 ?
Na2 Na2 Sn 83.946(4) 29_554 32 ?
Na2 Na2 Sn 42.611(4) 34 32 ?
Na2 Na2 Sn 101.521(3) 30 32 ?
Na1 Na2 Sn 46.45(3) . 32 ?
Na1 Na2 Sn 133.24(4) 26_554 32 ?
Na1 Na2 Sn 45.14(4) 27 32 ?
Na1 Na2 Sn 135.19(4) 4_565 32 ?
Sn Na2 Sn 105.814(6) 10 32 ?
Sn Na2 Sn 65.316(7) 28 32 ?
Sn Na2 Sn 121.778(4) 25_554 32 ?
Sn Na2 Sn 67.572(4) 12_565 32 ?
Sn Na2 Sn 172.356(8) 31_554 32 ?
Sn Na2 Sn 79.787(4) 27 6_565 ?
Sn Na2 Sn 148.871(4) 9 6_565 ?
Sn Na2 Sn 95.943(2) 26_554 6_565 ?
Sn Na2 Sn 38.535(9) 11_565 6_565 ?
Na2 Na2 Sn 83.946(4) 33_454 6_565 ?
Na2 Na2 Sn 42.611(4) 29_554 6_565 ?
Na2 Na2 Sn 101.521(3) 34 6_565 ?
Na2 Na2 Sn 129.919(4) 30 6_565 ?
Na1 Na2 Sn 133.24(4) . 6_565 ?
Na1 Na2 Sn 135.19(4) 26_554 6_565 ?
Na1 Na2 Sn 46.45(3) 27 6_565 ?
Na1 Na2 Sn 45.14(4) 4_565 6_565 ?
Sn Na2 Sn 121.778(4) 10 6_565 ?
Sn Na2 Sn 105.814(6) 28 6_565 ?
Sn Na2 Sn 67.572(4) 25_554 6_565 ?
Sn Na2 Sn 65.316(7) 12_565 6_565 ?
Sn Na2 Sn 90.255(1) 31_554 6_565 ?
Sn Na2 Sn 90.255(1) 32 6_565 ?
Sn Na2 Sn 95.943(2) 27 5 ?
Sn Na2 Sn 38.535(9) 9 5 ?
Sn Na2 Sn 79.787(4) 26_554 5 ?
Sn Na2 Sn 148.871(4) 11_565 5 ?
Na2 Na2 Sn 101.521(3) 33_454 5 ?
Na2 Na2 Sn 129.919(4) 29_554 5 ?
Na2 Na2 Sn 83.946(4) 34 5 ?
Na2 Na2 Sn 42.611(4) 30 5 ?
Na1 Na2 Sn 45.14(4) . 5 ?
Na1 Na2 Sn 46.45(3) 26_554 5 ?
Na1 Na2 Sn 135.19(4) 27 5 ?
Na1 Na2 Sn 133.24(4) 4_565 5 ?
Sn Na2 Sn 65.316(7) 10 5 ?
Sn Na2 Sn 67.572(4) 28 5 ?
Sn Na2 Sn 105.814(6) 25_554 5 ?
Sn Na2 Sn 121.778(4) 12_565 5 ?
Sn Na2 Sn 90.255(1) 31_554 5 ?
Sn Na2 Sn 90.255(1) 32 5 ?
Sn Na2 Sn 172.356(8) 6_565 5 ?
Sn Na1 Sn 51.30(5) . 9 ?
Sn Na1 Sn 51.30(5) . 5 ?
Sn Na1 Sn 51.30(5) 9 5 ?
Sn Na1 Sn 97.236(19) . 36 ?
Sn Na1 Sn 147.61(6) 9 36 ?
Sn Na1 Sn 118.64(3) 5 36 ?
Sn Na1 Sn 118.64(3) . 35 ?
Sn Na1 Sn 147.61(6) 9 35 ?
Sn Na1 Sn 97.235(19) 5 35 ?
Sn Na1 Sn 48.18(3) 36 35 ?
Sn Na1 Sn 118.64(3) . 32 ?
Sn Na1 Sn 97.235(19) 9 32 ?
Sn Na1 Sn 147.61(6) 5 32 ?
Sn Na1 Sn 91.89(6) 36 32 ?
Sn Na1 Sn 112.17(9) 35 32 ?
Sn Na1 Sn 97.236(19) . 31 ?
Sn Na1 Sn 118.64(3) 9 31 ?
Sn Na1 Sn 147.61(6) 5 31 ?
Sn Na1 Sn 49.88(3) 36 31 ?
Sn Na1 Sn 91.89(6) 35 31 ?
Sn Na1 Sn 48.18(3) 32 31 ?
Sn Na1 Sn 147.61(6) . 28 ?
Sn Na1 Sn 118.64(3) 9 28 ?
Sn Na1 Sn 97.235(19) 5 28 ?
Sn Na1 Sn 91.89(6) 36 28 ?
Sn Na1 Sn 49.88(3) 35 28 ?
Sn Na1 Sn 91.89(6) 32 28 ?
Sn Na1 Sn 112.17(9) 31 28 ?
Sn Na1 Sn 147.61(6) . 27 ?
Sn Na1 Sn 97.235(19) 9 27 ?
Sn Na1 Sn 118.64(3) 5 27 ?
Sn Na1 Sn 112.17(9) 36 27 ?
Sn Na1 Sn 91.89(6) 35 27 ?
Sn Na1 Sn 49.88(3) 32 27 ?
Sn Na1 Sn 91.89(6) 31 27 ?
Sn Na1 Sn 48.18(3) 28 27 ?
Sn Na1 Ca 150.01(3) . 25 ?
Sn Na1 Ca 150.01(3) 9 25 ?
Sn Na1 Ca 150.01(3) 5 25 ?
Sn Na1 Ca 56.09(5) 36 25 ?
Sn Na1 Ca 56.09(5) 35 25 ?
Sn Na1 Ca 56.09(5) 32 25 ?
Sn Na1 Ca 56.09(5) 31 25 ?
Sn Na1 Ca 56.09(5) 28 25 ?
Sn Na1 Ca 56.09(5) 27 25 ?
Sn Na1 Na2 76.72(4) . 34 ?
Sn Na1 Na2 49.68(2) 9 34 ?
Sn Na1 Na2 100.82(7) 5 34 ?
Sn Na1 Na2 123.68(3) 36 34 ?
Sn Na1 Na2 161.46(9) 35 34 ?
Sn Na1 Na2 49.292(4) 32 34 ?
Sn Na1 Na2 75.012(10) 31 34 ?
Sn Na1 Na2 122.79(3) 28 34 ?
Sn Na1 Na2 75.780(9) 27 34 ?
Ca Na1 Na2 105.38(5) 25 34 ?
Sn Na1 Na2 76.72(4) . 9 ?
Sn Na1 Na2 100.82(7) 9 9 ?
Sn Na1 Na2 49.68(2) 5 9 ?
Sn Na1 Na2 75.012(10) 36 9 ?
Sn Na1 Na2 49.292(4) 35 9 ?
Sn Na1 Na2 161.46(9) 32 9 ?
Sn Na1 Na2 123.68(3) 31 9 ?
Sn Na1 Na2 75.780(9) 28 9 ?
Sn Na1 Na2 122.79(3) 27 9 ?
Ca Na1 Na2 105.38(5) 25 9 ?
Na2 Na1 Na2 149.25(9) 34 9 ?
Sn Na1 Na2 100.82(7) . 30 ?
Sn Na1 Na2 76.72(4) 9 30 ?
Sn Na1 Na2 49.68(2) 5 30 ?
Sn Na1 Na2 122.79(3) 36 30 ?
Sn Na1 Na2 75.780(9) 35 30 ?
Sn Na1 Na2 123.68(3) 32 30 ?
Sn Na1 Na2 161.46(9) 31 30 ?
Sn Na1 Na2 49.292(4) 28 30 ?
Sn Na1 Na2 75.012(9) 27 30 ?
Ca Na1 Na2 105.38(5) 25 30 ?
Na2 Na1 Na2 113.24(4) 34 30 ?
Na2 Na1 Na2 57.646(14) 9 30 ?
Sn Na1 Na2 49.68(2) . 5 ?
Sn Na1 Na2 76.72(4) 9 5 ?
Sn Na1 Na2 100.82(7) 5 5 ?
Sn Na1 Na2 75.780(9) 36 5 ?
Sn Na1 Na2 122.79(3) 35 5 ?
Sn Na1 Na2 75.012(10) 32 5 ?
Sn Na1 Na2 49.292(4) 31 5 ?
Sn Na1 Na2 161.46(9) 28 5 ?
Sn Na1 Na2 123.68(3) 27 5 ?
Ca Na1 Na2 105.38(5) 25 5 ?
Na2 Na1 Na2 57.646(14) 34 5 ?
Na2 Na1 Na2 113.24(4) 9 5 ?
Na2 Na1 Na2 149.25(9) 30 5 ?
Sn Na1 Na2 49.68(2) . 26 ?
Sn Na1 Na2 100.82(7) 9 26 ?
Sn Na1 Na2 76.72(4) 5 26 ?
Sn Na1 Na2 49.292(4) 36 26 ?
Sn Na1 Na2 75.012(9) 35 26 ?
Sn Na1 Na2 122.79(3) 32 26 ?
Sn Na1 Na2 75.780(9) 31 26 ?
Sn Na1 Na2 123.68(3) 28 26 ?
Sn Na1 Na2 161.46(9) 27 26 ?
Ca Na1 Na2 105.38(5) 25 26 ?
Na2 Na1 Na2 113.24(4) 34 26 ?
Na2 Na1 Na2 57.646(14) 9 26 ?
Na2 Na1 Na2 113.24(4) 30 26 ?
Na2 Na1 Na2 57.646(14) 5 26 ?
Sn Na1 Na2 100.82(7) . . ?
Sn Na1 Na2 49.68(2) 9 . ?
Sn Na1 Na2 76.72(4) 5 . ?
Sn Na1 Na2 161.46(9) 36 . ?
Sn Na1 Na2 123.68(3) 35 . ?
Sn Na1 Na2 75.780(9) 32 . ?
Sn Na1 Na2 122.79(3) 31 . ?
Sn Na1 Na2 75.012(9) 28 . ?
Sn Na1 Na2 49.292(4) 27 . ?
Ca Na1 Na2 105.38(5) 25 . ?
Na2 Na1 Na2 57.646(14) 34 . ?
Na2 Na1 Na2 113.24(4) 9 . ?
Na2 Na1 Na2 57.646(14) 30 . ?
Na2 Na1 Na2 113.24(4) 5 . ?
Na2 Na1 Na2 149.25(9) 26 . ?
Sn Na1 Sn 112.459(10) . 26 ?
Sn Na1 Sn 147.033(6) 9 26 ?
Sn Na1 Sn 147.033(6) 5 26 ?
Sn Na1 Sn 28.60(3) 36 26 ?
Sn Na1 Sn 63.44(4) 35 26 ?
Sn Na1 Sn 63.44(4) 32 26 ?
Sn Na1 Sn 28.60(3) 31 26 ?
Sn Na1 Sn 89.89(6) 28 26 ?
Sn Na1 Sn 89.89(6) 27 26 ?
Ca Na1 Sn 37.55(2) 25 26 ?
Na2 Na1 Sn 102.14(3) 34 26 ?
Na2 Na1 Sn 102.14(3) 9 26 ?
Na2 Na1 Sn 135.98(6) 30 26 ?
Na2 Na1 Sn 72.62(3) 5 26 ?
Na2 Na1 Sn 72.62(3) 26 26 ?
Na2 Na1 Sn 135.98(6) . 26 ?
Sn Na1 Sn 147.033(6) . 34 ?
Sn Na1 Sn 112.459(10) 9 34 ?
Sn Na1 Sn 147.033(6) 5 34 ?
Sn Na1 Sn 89.89(6) 36 34 ?
Sn Na1 Sn 89.89(6) 35 34 ?
Sn Na1 Sn 28.60(3) 32 34 ?
Sn Na1 Sn 63.44(4) 31 34 ?
Sn Na1 Sn 63.44(4) 28 34 ?
Sn Na1 Sn 28.60(3) 27 34 ?
Ca Na1 Sn 37.55(2) 25 34 ?
Na2 Na1 Sn 72.62(3) 34 34 ?
Na2 Na1 Sn 135.98(6) 9 34 ?
Na2 Na1 Sn 102.14(3) 30 34 ?
Na2 Na1 Sn 102.14(3) 5 34 ?
Na2 Na1 Sn 135.98(6) 26 34 ?
Na2 Na1 Sn 72.62(3) . 34 ?
Sn Na1 Sn 63.72(3) 26 34 ?
Sn Na1 Sn 147.033(6) . 30 ?
Sn Na1 Sn 147.033(6) 9 30 ?
Sn Na1 Sn 112.459(10) 5 30 ?
Sn Na1 Sn 63.44(4) 36 30 ?
Sn Na1 Sn 28.60(3) 35 30 ?
Sn Na1 Sn 89.89(6) 32 30 ?
Sn Na1 Sn 89.89(6) 31 30 ?
Sn Na1 Sn 28.60(3) 28 30 ?
Sn Na1 Sn 63.44(4) 27 30 ?
Ca Na1 Sn 37.55(2) 25 30 ?
Na2 Na1 Sn 135.98(6) 34 30 ?
Na2 Na1 Sn 72.62(3) 9 30 ?
Na2 Na1 Sn 72.62(3) 30 30 ?
Na2 Na1 Sn 135.98(6) 5 30 ?
Na2 Na1 Sn 102.14(3) 26 30 ?
Na2 Na1 Sn 102.14(3) . 30 ?
Sn Na1 Sn 63.72(3) 26 30 ?
Sn Na1 Sn 63.72(3) 34 30 ?
Sn Na1 Na1 32.71(4) . 28_455 ?
Sn Na1 Na1 32.71(4) 9 28_455 ?
Sn Na1 Na1 67.11(8) 5 28_455 ?
Sn Na1 Na1 116.717(15) 36 28_455 ?
Sn Na1 Na1 151.19(6) 35 28_455 ?
Sn Na1 Na1 90.508(6) 32 28_455 ?
Sn Na1 Na1 90.508(6) 31 28_455 ?
Sn Na1 Na1 151.19(6) 28 28_455 ?
Sn Na1 Na1 116.717(15) 27 28_455 ?
Ca Na1 Na1 142.88(5) 25 28_455 ?
Na2 Na1 Na1 44.329(4) 34 28_455 ?
Na2 Na1 Na1 107.01(9) 9 28_455 ?
Na2 Na1 Na1 107.01(9) 30 28_455 ?
Na2 Na1 Na1 44.329(4) 5 28_455 ?
Na2 Na1 Na1 77.79(4) 26 28_455 ?
Na2 Na1 Na1 77.79(4) . 28_455 ?
Sn Na1 Na1 116.63(2) 26 28_455 ?
Sn Na1 Na1 116.63(2) 34 28_455 ?
Sn Na1 Na1 179.57(7) 30 28_455 ?
Sn Ca Sn 51.273(10) . 9 ?
Sn Ca Sn 51.273(10) . 5 ?
Sn Ca Sn 51.273(10) 9 5 ?
Sn Ca Sn 95.033(2) . 12 ?
Sn Ca Sn 145.544(8) 9 12 ?
Sn Ca Sn 116.754(4) 5 12 ?
Sn Ca Sn 116.754(4) . 11 ?
Sn Ca Sn 145.544(8) 9 11 ?
Sn Ca Sn 95.032(2) 5 11 ?
Sn Ca Sn 49.524(12) 12 11 ?
Sn Ca Sn 116.754(4) . 8 ?
Sn Ca Sn 95.032(2) 9 8 ?
Sn Ca Sn 145.544(8) 5 8 ?
Sn Ca Sn 95.032(2) 12 8 ?
Sn Ca Sn 116.754(4) 11 8 ?
Sn Ca Sn 95.033(2) . 7 ?
Sn Ca Sn 116.754(4) 9 7 ?
Sn Ca Sn 145.544(8) 5 7 ?
Sn Ca Sn 51.274(10) 12 7 ?
Sn Ca Sn 95.032(2) 11 7 ?
Sn Ca Sn 49.524(12) 8 7 ?
Sn Ca Sn 145.544(8) . 4 ?
Sn Ca Sn 116.754(4) 9 4 ?
Sn Ca Sn 95.032(2) 5 4 ?
Sn Ca Sn 95.032(2) 12 4 ?
Sn Ca Sn 51.274(10) 11 4 ?
Sn Ca Sn 95.032(2) 8 4 ?
Sn Ca Sn 116.754(4) 7 4 ?
Sn Ca Sn 145.544(8) . 3 ?
Sn Ca Sn 95.032(2) 9 3 ?
Sn Ca Sn 116.754(4) 5 3 ?
Sn Ca Sn 116.754(4) 12 3 ?
Sn Ca Sn 95.032(2) 11 3 ?
Sn Ca Sn 51.274(10) 8 3 ?
Sn Ca Sn 95.032(2) 7 3 ?
Sn Ca Sn 49.524(12) 4 3 ?
Sn Ca Sn 95.032(2) . 10 ?
Sn Ca Sn 49.524(12) 9 10 ?
Sn Ca Sn 95.032(2) 5 10 ?
Sn Ca Sn 145.544(8) 12 10 ?
Sn Ca Sn 145.544(8) 11 10 ?
Sn Ca Sn 51.274(10) 8 10 ?
Sn Ca Sn 95.032(2) 7 10 ?
Sn Ca Sn 95.032(2) 4 10 ?
Sn Ca Sn 51.274(10) 3 10 ?
Sn Ca Sn 95.032(2) . 6 ?
Sn Ca Sn 95.032(2) 9 6 ?
Sn Ca Sn 49.524(12) 5 6 ?
Sn Ca Sn 95.032(2) 12 6 ?
Sn Ca Sn 51.274(10) 11 6 ?
Sn Ca Sn 145.544(8) 8 6 ?
Sn Ca Sn 145.544(8) 7 6 ?
Sn Ca Sn 51.274(10) 4 6 ?
Sn Ca Sn 95.032(2) 3 6 ?
Sn Ca Sn 116.754(4) 10 6 ?
Sn Ca Sn 49.525(12) . 2 ?
Sn Ca Sn 95.032(2) 9 2 ?
Sn Ca Sn 95.032(2) 5 2 ?
Sn Ca Sn 51.274(10) 12 2 ?
Sn Ca Sn 95.032(2) 11 2 ?
Sn Ca Sn 95.032(2) 8 2 ?
Sn Ca Sn 51.274(10) 7 2 ?
Sn Ca Sn 145.544(8) 4 2 ?
Sn Ca Sn 145.544(8) 3 2 ?
Sn Ca Sn 116.754(4) 10 2 ?
Sn Ca Sn 116.754(4) 6 2 ?
Sn Ca Na1 150.027(6) . 25_444 ?
Sn Ca Na1 150.027(6) 9 25_444 ?
Sn Ca Na1 150.027(6) 5 25_444 ?
Sn Ca Na1 58.381(2) 12 25_444 ?
Sn Ca Na1 58.381(2) 11 25_444 ?
Sn Ca Na1 58.381(2) 8 25_444 ?
Sn Ca Na1 58.381(2) 7 25_444 ?
Sn Ca Na1 58.381(2) 4 25_444 ?
Sn Ca Na1 58.381(2) 3 25_444 ?
Sn Ca Na1 100.502(6) 10 25_444 ?
Sn Ca Na1 100.502(6) 6 25_444 ?
Sn Ca Na1 100.502(6) 2 25_444 ?
Sn Ca Na1 58.381(2) . 28_455 ?
Sn Ca Na1 58.381(2) 9 28_455 ?
Sn Ca Na1 100.502(6) 5 28_455 ?
Sn Ca Na1 100.502(6) 12 28_455 ?
Sn Ca Na1 150.027(6) 11 28_455 ?
Sn Ca Na1 58.381(2) 8 28_455 ?
Sn Ca Na1 58.381(2) 7 28_455 ?
Sn Ca Na1 150.027(6) 4 28_455 ?
Sn Ca Na1 100.502(6) 3 28_455 ?
Sn Ca Na1 58.381(2) 10 28_455 ?
Sn Ca Na1 150.027(6) 6 28_455 ?
Sn Ca Na1 58.381(2) 2 28_455 ?
Na1 Ca Na1 109.5 25_444 28_455 ?
Sn Ca Na1 58.381(2) . 27_545 ?
Sn Ca Na1 100.502(6) 9 27_545 ?
Sn Ca Na1 58.381(2) 5 27_545 ?
Sn Ca Na1 58.381(2) 12 27_545 ?
Sn Ca Na1 58.381(2) 11 27_545 ?
Sn Ca Na1 150.027(6) 8 27_545 ?
Sn Ca Na1 100.502(6) 7 27_545 ?
Sn Ca Na1 100.502(6) 4 27_545 ?
Sn Ca Na1 150.027(6) 3 27_545 ?
Sn Ca Na1 150.027(6) 10 27_545 ?
Sn Ca Na1 58.381(2) 6 27_545 ?
Sn Ca Na1 58.381(2) 2 27_545 ?
Na1 Ca Na1 109.5 25_444 27_545 ?
Na1 Ca Na1 109.5 28_455 27_545 ?
Sn Ca Na1 100.502(6) . 26_554 ?
Sn Ca Na1 58.381(2) 9 26_554 ?
Sn Ca Na1 58.381(2) 5 26_554 ?
Sn Ca Na1 150.027(6) 12 26_554 ?
Sn Ca Na1 100.502(6) 11 26_554 ?
Sn Ca Na1 100.502(6) 8 26_554 ?
Sn Ca Na1 150.027(6) 7 26_554 ?
Sn Ca Na1 58.381(2) 4 26_554 ?
Sn Ca Na1 58.381(2) 3 26_554 ?
Sn Ca Na1 58.381(2) 10 26_554 ?
Sn Ca Na1 58.381(2) 6 26_554 ?
Sn Ca Na1 150.027(6) 2 26_554 ?
Na1 Ca Na1 109.5 25_444 26_554 ?
Na1 Ca Na1 109.5 28_455 26_554 ?
Na1 Ca Na1 109.5 27_545 26_554 ?
Sn Ca Na1 29.973(6) . . ?
Sn Ca Na1 29.973(6) 9 . ?
Sn Ca Na1 29.973(6) 5 . ?
Sn Ca Na1 121.619(2) 12 . ?
Sn Ca Na1 121.619(2) 11 . ?
Sn Ca Na1 121.619(2) 8 . ?
Sn Ca Na1 121.619(2) 7 . ?
Sn Ca Na1 121.619(2) 4 . ?
Sn Ca Na1 121.619(2) 3 . ?
Sn Ca Na1 79.498(6) 10 . ?
Sn Ca Na1 79.498(6) 6 . ?
Sn Ca Na1 79.498(6) 2 . ?
Na1 Ca Na1 180.00(2) 25_444 . ?
Na1 Ca Na1 70.5 28_455 . ?
Na1 Ca Na1 70.5 27_545 . ?
Na1 Ca Na1 70.5 26_554 . ?
Sn Ca Na1 121.619(2) . 4 ?
Sn Ca Na1 121.619(2) 9 4 ?
Sn Ca Na1 79.498(6) 5 4 ?
Sn Ca Na1 79.498(6) 12 4 ?
Sn Ca Na1 29.973(6) 11 4 ?
Sn Ca Na1 121.619(2) 8 4 ?
Sn Ca Na1 121.619(2) 7 4 ?
Sn Ca Na1 29.973(6) 4 4 ?
Sn Ca Na1 79.498(6) 3 4 ?
Sn Ca Na1 121.619(2) 10 4 ?
Sn Ca Na1 29.973(6) 6 4 ?
Sn Ca Na1 121.619(2) 2 4 ?
Na1 Ca Na1 70.5 25_444 4 ?
Na1 Ca Na1 180.00(7) 28_455 4 ?
Na1 Ca Na1 70.5 27_545 4 ?
Na1 Ca Na1 70.5 26_554 4 ?
Na1 Ca Na1 109.5 . 4 ?
Sn Ca Na1 121.619(2) . 3 ?
Sn Ca Na1 79.498(6) 9 3 ?
Sn Ca Na1 121.619(2) 5 3 ?
Sn Ca Na1 121.619(2) 12 3 ?
Sn Ca Na1 121.619(2) 11 3 ?
Sn Ca Na1 29.973(6) 8 3 ?
Sn Ca Na1 79.498(6) 7 3 ?
Sn Ca Na1 79.498(6) 4 3 ?
Sn Ca Na1 29.973(6) 3 3 ?
Sn Ca Na1 29.973(6) 10 3 ?
Sn Ca Na1 121.619(2) 6 3 ?
Sn Ca Na1 121.619(2) 2 3 ?
Na1 Ca Na1 70.5 25_444 3 ?
Na1 Ca Na1 70.5 28_455 3 ?
Na1 Ca Na1 180.00(7) 27_545 3 ?
Na1 Ca Na1 70.5 26_554 3 ?
Na1 Ca Na1 109.5 . 3 ?
Na1 Ca Na1 109.5 4 3 ?
Sn Ca Na1 79.498(6) . 2 ?
Sn Ca Na1 121.619(2) 9 2 ?
Sn Ca Na1 121.619(2) 5 2 ?
Sn Ca Na1 29.973(6) 12 2 ?
Sn Ca Na1 79.498(6) 11 2 ?
Sn Ca Na1 79.498(6) 8 2 ?
Sn Ca Na1 29.973(6) 7 2 ?
Sn Ca Na1 121.619(2) 4 2 ?
Sn Ca Na1 121.619(2) 3 2 ?
Sn Ca Na1 121.619(2) 10 2 ?
Sn Ca Na1 121.619(2) 6 2 ?
Sn Ca Na1 29.973(6) 2 2 ?
Na1 Ca Na1 70.5 25_444 2 ?
Na1 Ca Na1 70.5 28_455 2 ?
Na1 Ca Na1 70.5 27_545 2 ?
Na1 Ca Na1 180.00(2) 26_554 2 ?
Na1 Ca Na1 109.5 . 2 ?
Na1 Ca Na1 109.5 4 2 ?
Na1 Ca Na1 109.5 3 2 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sn Sn 2.8686(7) 2 ?
Sn Sn 2.9631(6) 9 ?
Sn Sn 2.9631(6) 5 ?
Sn Na2 3.2201(3) 5 ?
Sn Na2 3.2201(3) 26 ?
Sn Na1 3.422(3) . ?
Sn Ca 3.4243(3) . ?
Sn Na1 3.5137(19) 28_455 ?
Sn Na1 3.5137(19) 27_545 ?
Sn Na2 4.6597(4) 6_556 ?
Sn Na2 4.6597(4) 25_445 ?
Sn Na2 4.6996(3) 34 ?
Sn Na2 4.6996(3) 9 ?
Sn Sn 5.0506(5) 10 ?
Sn Sn 5.0506(5) 6 ?
Sn Sn 5.0506(5) 12 ?
Sn Sn 5.0506(5) 7 ?
Sn Sn 5.2047(4) 36 ?
Sn Sn 5.2047(4) 31 ?
Sn Sn 5.2047(4) 34_545 ?
Na2 Sn 3.2201(3) 27 ?
Na2 Sn 3.2201(3) 9 ?
Na2 Sn 3.2201(3) 26_554 ?
Na2 Sn 3.2201(3) 11_565 ?
Na2 Na2 3.9544(2) 33_454 ?
Na2 Na2 3.9544(2) 29_554 ?
Na2 Na2 3.9544(2) 34 ?
Na2 Na2 3.9544(2) 30 ?
Na2 Na1 4.1012(9) . ?
Na2 Na1 4.1012(9) 26_554 ?
Na2 Na1 4.1012(9) 27 ?
Na2 Na1 4.1012(9) 4_565 ?
Na2 Sn 4.6596(4) 10 ?
Na2 Sn 4.6596(4) 28 ?
Na2 Sn 4.6596(4) 25_554 ?
Na2 Sn 4.6596(4) 12_565 ?
Na2 Sn 4.6996(3) 31_554 ?
Na2 Sn 4.6996(3) 32 ?
Na2 Sn 4.6996(3) 6_565 ?
Na2 Sn 4.6996(3) 5 ?
Na1 Sn 3.423(3) 9 ?
Na1 Sn 3.423(3) 5 ?
Na1 Sn 3.5137(19) 36 ?
Na1 Sn 3.5137(19) 35 ?
Na1 Sn 3.5137(19) 32 ?
Na1 Sn 3.5137(19) 31 ?
Na1 Sn 3.5137(19) 28 ?
Na1 Sn 3.5137(19) 27 ?
Na1 Ca 3.756(3) 25 ?
Na1 Na2 4.1012(9) 34 ?
Na1 Na2 4.1012(9) 9 ?
Na1 Na2 4.1012(9) 30 ?
Na1 Na2 4.1012(9) 5 ?
Na1 Na2 4.1012(9) 26 ?
Na1 Sn 5.524(3) 26 ?
Na1 Sn 5.524(3) 34 ?
Na1 Sn 5.524(3) 30 ?
Na1 Na1 5.8675(17) 28_455 ?
Ca Sn 3.4243(3) 9 ?
Ca Sn 3.4243(3) 5 ?
Ca Sn 3.4243(3) 12 ?
Ca Sn 3.4243(3) 11 ?
Ca Sn 3.4243(3) 8 ?
Ca Sn 3.4243(3) 7 ?
Ca Sn 3.4243(3) 4 ?
Ca Sn 3.4243(3) 3 ?
Ca Sn 3.4243(3) 10 ?
Ca Sn 3.4243(3) 6 ?
Ca Sn 3.4243(3) 2 ?
Ca Na1 3.756(3) 25_444 ?
Ca Na1 3.756(3) 28_455 ?
Ca Na1 3.756(3) 27_545 ?
Ca Na1 3.756(3) 26_554 ?
Ca Na1 5.931(3) 4 ?
Ca Na1 5.931(3) 3 ?
Ca Na1 5.931(3) 2 ?
loop_
_cod_related_entry_id
_cod_related_entry_database
_cod_related_entry_code
1 PubChem 139133874
