#------------------------------------------------------------------------------
#$Date: 2026-04-05 13:34:49 +0200 (Sun 05 de Apr de 2026) $
#$Revision: 305283 $
#$URL: svn://www.crystallography.net/cod/cif/7/13/55/7135571.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7135571
loop_
_publ_author_name
'Meduri, Rahul'
'Wilkinson, Grant R.'
'Idrees, Muhammad Z.'
'Wei, Kaya'
'Stoian, Sebastian A.'
'La Pierre, Henry S.'
'McCandless, Gregory T.'
'Chan, Julia Y.'
_publ_section_title
;
 Zn-flux-enabled synthesis of orthorhombic kagome
 YbFe₆Ge₆: Yb reduction and magnetic behavior.
;
_journal_issue                   24
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              6617
_journal_page_last               6621
_journal_paper_doi               10.1039/d6cc00958a
_journal_volume                  62
_journal_year                    2026
_chemical_formula_sum            'Fe5.52 Ge6 Yb Zn0.48'
_chemical_formula_weight         948.25
_space_group_crystal_system      orthorhombic
_space_group_IT_number           63
_space_group_name_Hall           '-C 2c 2'
_space_group_name_H-M_alt        'C m c m'
_audit_creation_method           SHELXL-2019/3
_audit_update_record
;
2026-02-03 deposited with the CCDC.	2026-03-04 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.1799(12)
_cell_length_b                   17.541(2)
_cell_length_c                   5.0739(6)
_cell_measurement_reflns_used    2607
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      29.67
_cell_measurement_theta_min      6.82
_cell_volume                     728.02(16)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX5'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'CrystalMaker (CrystalMaker, 2024)'
_computing_publication_material  'publCIF (Westrip, 2012)'
_computing_structure_refinement  'SHELXL-2019/3 (Sheldrick, 2019)'
_computing_structure_solution
'SHELXT Intrinsic Phasing 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Kappa D8 Quest CPAD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  'HELIOS optics'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0761
_diffrn_reflns_av_unetI/netI     0.0231
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       -7
_diffrn_reflns_number            15627
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.540
_diffrn_reflns_theta_min         2.322
_diffrn_source                   'I\mS microfocus tube'
_exptl_absorpt_coefficient_mu    49.151
_exptl_absorpt_correction_T_max  0.7461
_exptl_absorpt_correction_T_min  0.4682
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
SADABS(Krause,Herbst-Irmer,Sheldrick,&Stalke;J.Appl.Cryst.2015,48,3-10)
_exptl_crystal_colour            Grey
_exptl_crystal_density_diffrn    8.651
_exptl_crystal_description       Fragment
_exptl_crystal_F_000             1680
_exptl_crystal_size_max          0.050
_exptl_crystal_size_mid          0.038
_exptl_crystal_size_min          0.010
_refine_diff_density_max         2.512
_refine_diff_density_min         -2.704
_refine_diff_density_rms         0.390
_refine_ls_extinction_coef       0.00115(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2019/2 (Sheldrick 2019)'
_refine_ls_goodness_of_fit_ref   1.188
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     50
_refine_ls_number_reflns         653
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.187
_refine_ls_R_factor_all          0.0355
_refine_ls_R_factor_gt           0.0262
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0269P)²+10.2293P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0612
_refine_ls_wR_factor_ref         0.0713
_reflns_Friedel_coverage         0.000
_reflns_number_gt                522
_reflns_number_total             653
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d6cc00958a2.cif
_cod_data_source_block           shelx
_cod_depositor_comments          'Adding full bibliography for 7135571.cif.'
_cod_original_cell_volume        728.03(16)
_cod_database_code               7135571
_shelx_shelxl_version_number     2019/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.192
_shelx_estimated_absorpt_t_max   0.639
_publcif_funding_html
;
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Yb1 Yb 0.000000 0.12740(3) 0.250000 0.00766(17) Uani 0.8945(13) 4 d S T P A 1
Ge5 Ge 0.34659(11) 0.12380(5) 0.250000 0.0078(2) Uani 0.8945(13) 2 d S T P A 1
Yb2 Yb 0.500000 0.1213(2) 0.250000 0.00766(17) Uani 0.1055(13) 4 d S T P A 2
Ge6 Ge 0.8474(9) 0.1243(4) 0.250000 0.0078(2) Uani 0.1055(13) 2 d S T P A 2
Fe1 Fe 0.250000 0.250000 0.000000 0.0078(3) Uani 0.92 2 d S . P . .
Zn1 Zn 0.250000 0.250000 0.000000 0.0078(3) Uani 0.08 2 d S . P . .
Fe2 Fe 0.24711(12) 0.000000 0.000000 0.0078(3) Uani 0.92 2 d S T P . .
Zn2 Zn 0.24711(12) 0.000000 0.000000 0.0078(3) Uani 0.08 2 d S T P . .
Fe3 Fe 0.24821(12) 0.12505(6) 0.750000 0.0078(3) Uani 0.92 2 d S T P . .
Zn3 Zn 0.24821(12) 0.12505(6) 0.750000 0.0078(3) Uani 0.08 2 d S T P . .
Ge1 Ge 0.000000 0.04210(6) 0.750000 0.0069(3) Uani 1 4 d S T P A .
Ge2 Ge 0.500000 0.04038(6) 0.750000 0.0107(3) Uani 1 4 d S T P A .
Ge3 Ge 0.000000 0.21099(6) 0.750000 0.0081(3) Uani 1 4 d S T P A .
Ge4 Ge 0.500000 0.20467(6) 0.750000 0.0096(3) Uani 1 4 d S T P A .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ge5 Yb1 Ge5 177.45(4) . 3 ?
Ge5 Yb1 Ge3 90.638(10) . . ?
Ge5 Yb1 Ge3 90.638(10) 3 . ?
Ge5 Yb1 Ge3 90.638(10) . 1_554 ?
Ge5 Yb1 Ge3 90.638(10) 3 1_554 ?
Ge3 Yb1 Ge3 119.95(4) . 1_554 ?
Ge5 Yb1 Ge1 89.352(10) . . ?
Ge5 Yb1 Ge1 89.352(10) 3 . ?
Ge3 Yb1 Ge1 60.56(3) . . ?
Ge3 Yb1 Ge1 179.50(3) 1_554 . ?
Ge5 Yb1 Ge1 89.352(10) . 1_554 ?
Ge5 Yb1 Ge1 89.352(10) 3 1_554 ?
Ge3 Yb1 Ge1 179.49(3) . 1_554 ?
Ge3 Yb1 Ge1 60.56(3) 1_554 1_554 ?
Ge1 Yb1 Ge1 118.94(4) . 1_554 ?
Ge5 Yb1 Ge4 91.276(19) . 13_556 ?
Ge5 Yb1 Ge4 91.275(19) 3 13_556 ?
Ge3 Yb1 Ge4 59.97(2) . 13_556 ?
Ge3 Yb1 Ge4 59.97(2) 1_554 13_556 ?
Ge1 Yb1 Ge4 120.532(19) . 13_556 ?
Ge1 Yb1 Ge4 120.532(19) 1_554 13_556 ?
Ge5 Yb1 Ge1 88.724(19) . 9_556 ?
Ge5 Yb1 Ge1 88.725(19) 3 9_556 ?
Ge3 Yb1 Ge1 120.03(2) . 9_556 ?
Ge3 Yb1 Ge1 120.03(2) 1_554 9_556 ?
Ge1 Yb1 Ge1 59.468(19) . 9_556 ?
Ge1 Yb1 Ge1 59.468(19) 1_554 9_556 ?
Ge4 Yb1 Ge1 180.0 13_556 9_556 ?
Ge5 Yb1 Fe1 51.783(17) . 6 ?
Ge5 Yb1 Fe1 130.414(19) 3 6 ?
Ge3 Yb1 Fe1 47.644(11) . 6 ?
Ge3 Yb1 Fe1 90.392(18) 1_554 6 ?
Ge1 Yb1 Fe1 89.998(15) . 6 ?
Ge1 Yb1 Fe1 132.614(10) 1_554 6 ?
Ge4 Yb1 Fe1 48.214(8) 13_556 6 ?
Ge1 Yb1 Fe1 131.786(8) 9_556 6 ?
Ge5 Yb1 Fe1 51.783(17) . . ?
Ge5 Yb1 Fe1 130.414(19) 3 . ?
Ge3 Yb1 Fe1 90.392(18) . . ?
Ge3 Yb1 Fe1 47.644(11) 1_554 . ?
Ge1 Yb1 Fe1 132.614(10) . . ?
Ge1 Yb1 Fe1 89.999(15) 1_554 . ?
Ge4 Yb1 Fe1 48.214(8) 13_556 . ?
Ge1 Yb1 Fe1 131.786(8) 9_556 . ?
Fe1 Yb1 Fe1 46.287(9) 6 . ?
Ge5 Yb1 Fe1 130.415(19) . 8_455 ?
Ge5 Yb1 Fe1 51.782(17) 3 8_455 ?
Ge3 Yb1 Fe1 90.392(18) . 8_455 ?
Ge3 Yb1 Fe1 47.644(11) 1_554 8_455 ?
Ge1 Yb1 Fe1 132.614(10) . 8_455 ?
Ge1 Yb1 Fe1 89.999(15) 1_554 8_455 ?
Ge4 Yb1 Fe1 48.214(8) 13_556 8_455 ?
Ge1 Yb1 Fe1 131.786(8) 9_556 8_455 ?
Fe1 Yb1 Fe1 96.428(16) 6 8_455 ?
Fe1 Yb1 Fe1 78.638(14) . 8_455 ?
Ge5 Ge5 Fe2 107.93(3) 3_655 10_556 ?
Ge5 Ge5 Fe2 107.93(3) 3_655 . ?
Fe2 Ge5 Fe2 57.36(2) 10_556 . ?
Ge5 Ge5 Fe3 107.60(3) 3_655 1_554 ?
Fe2 Ge5 Fe3 111.78(4) 10_556 1_554 ?
Fe2 Ge5 Fe3 57.06(2) . 1_554 ?
Ge5 Ge5 Fe3 107.60(3) 3_655 . ?
Fe2 Ge5 Fe3 57.06(2) 10_556 . ?
Fe2 Ge5 Fe3 111.78(4) . . ?
Fe3 Ge5 Fe3 144.79(6) 1_554 . ?
Ge5 Ge5 Fe1 107.21(2) 3_655 6 ?
Fe2 Ge5 Fe1 111.22(2) 10_556 6 ?
Fe2 Ge5 Fe1 144.86(4) . 6 ?
Fe3 Ge5 Fe1 110.88(4) 1_554 6 ?
Fe3 Ge5 Fe1 56.71(2) . 6 ?
Ge5 Ge5 Fe1 107.21(2) 3_655 . ?
Fe2 Ge5 Fe1 144.86(4) 10_556 . ?
Fe2 Ge5 Fe1 111.22(2) . . ?
Fe3 Ge5 Fe1 56.71(2) 1_554 . ?
Fe3 Ge5 Fe1 110.88(4) . . ?
Fe1 Ge5 Fe1 56.71(2) 6 . ?
Ge5 Ge5 Yb1 178.724(19) 3_655 . ?
Fe2 Ge5 Yb1 73.17(3) 10_556 . ?
Fe2 Ge5 Yb1 73.17(3) . . ?
Fe3 Ge5 Yb1 72.39(3) 1_554 . ?
Fe3 Ge5 Yb1 72.39(3) . . ?
Fe1 Ge5 Yb1 71.69(2) 6 . ?
Fe1 Ge5 Yb1 71.69(2) . . ?
Ge2 Yb2 Ge6 91.08(16) 9_656 3_655 ?
Ge2 Yb2 Ge6 91.08(16) 9_656 . ?
Ge6 Yb2 Ge6 177.8(3) 3_655 . ?
Ge2 Yb2 Ge2 60.78(7) 9_656 . ?
Ge6 Yb2 Ge2 90.53(8) 3_655 . ?
Ge6 Yb2 Ge2 90.53(8) . . ?
Ge2 Yb2 Ge2 60.77(7) 9_656 1_554 ?
Ge2 Yb2 Ge2 121.55(15) . 1_554 ?
Ge2 Yb2 Ge4 119.97(7) 9_656 . ?
Ge6 Yb2 Ge4 89.46(8) 3_655 . ?
Ge6 Yb2 Ge4 89.46(8) . . ?
Ge2 Yb2 Ge4 59.19(3) . . ?
Ge2 Yb2 Ge4 179.26(14) 1_554 . ?
Ge2 Yb2 Ge4 119.97(7) 9_656 1_554 ?
Ge2 Yb2 Ge4 179.26(14) . 1_554 ?
Ge2 Yb2 Ge4 59.19(3) 1_554 1_554 ?
Ge4 Yb2 Ge4 120.07(14) . 1_554 ?
Ge2 Yb2 Ge3 180.0 9_656 13_556 ?
Ge2 Yb2 Ge3 119.22(7) . 13_556 ?
Ge2 Yb2 Ge3 119.23(7) 1_554 13_556 ?
Ge4 Yb2 Ge3 60.03(7) . 13_556 ?
Ge4 Yb2 Ge3 60.03(7) 1_554 13_556 ?
Ge2 Yb2 Fe2 48.76(6) 9_656 10_556 ?
Ge2 Yb2 Fe2 48.32(4) . 10_556 ?
Ge2 Yb2 Fe2 91.21(9) 1_554 10_556 ?
Ge4 Yb2 Fe2 89.36(2) . 10_556 ?
Ge4 Yb2 Fe2 132.05(3) 1_554 10_556 ?
Ge3 Yb2 Fe2 131.24(6) 13_556 10_556 ?
Ge2 Yb2 Fe2 48.76(6) 9_656 2_655 ?
Ge2 Yb2 Fe2 48.32(4) . 2_655 ?
Ge2 Yb2 Fe2 91.21(9) 1_554 2_655 ?
Ge4 Yb2 Fe2 89.36(2) . 2_655 ?
Ge4 Yb2 Fe2 132.05(3) 1_554 2_655 ?
Ge3 Yb2 Fe2 131.24(6) 13_556 2_655 ?
Fe2 Yb2 Fe2 79.73(9) 10_556 2_655 ?
Ge2 Yb2 Fe2 48.76(6) 9_656 9_655 ?
Ge2 Yb2 Fe2 91.21(9) . 9_655 ?
Ge2 Yb2 Fe2 48.32(4) 1_554 9_655 ?
Ge4 Yb2 Fe2 132.05(3) . 9_655 ?
Ge4 Yb2 Fe2 89.36(2) 1_554 9_655 ?
Ge3 Yb2 Fe2 131.24(6) 13_556 9_655 ?
Fe2 Yb2 Fe2 97.51(12) 10_556 9_655 ?
Fe2 Yb2 Fe2 46.29(4) 2_655 9_655 ?
Ge2 Yb2 Fe2 48.76(6) 9_656 . ?
Ge6 Yb2 Fe2 51.06(13) 3_655 . ?
Ge6 Yb2 Fe2 130.79(16) . . ?
Ge2 Yb2 Fe2 91.21(9) . . ?
Ge2 Yb2 Fe2 48.32(4) 1_554 . ?
Ge4 Yb2 Fe2 132.05(3) . . ?
Ge4 Yb2 Fe2 89.36(2) 1_554 . ?
Ge3 Yb2 Fe2 131.24(6) 13_556 . ?
Fe2 Yb2 Fe2 46.29(4) 10_556 . ?
Fe2 Yb2 Fe2 97.51(12) 2_655 . ?
Fe2 Yb2 Fe2 79.73(9) 9_655 . ?
Fe2 Ge6 Fe2 57.46(17) 9_655 2_655 ?
Fe2 Ge6 Fe3 57.19(10) 9_655 3_655 ?
Fe2 Ge6 Fe3 112.1(3) 2_655 3_655 ?
Fe2 Ge6 Fe3 112.1(3) 9_655 3_656 ?
Fe2 Ge6 Fe3 57.19(10) 2_655 3_656 ?
Fe3 Ge6 Fe3 145.7(3) 3_655 3_656 ?
Fe2 Ge6 Fe1 145.6(3) 9_655 3_655 ?
Fe2 Ge6 Fe1 111.54(15) 2_655 3_655 ?
Fe3 Ge6 Fe1 111.3(3) 3_655 3_655 ?
Fe3 Ge6 Fe1 56.85(10) 3_656 3_655 ?
Fe2 Ge6 Fe1 111.54(15) 9_655 8 ?
Fe2 Ge6 Fe1 145.6(3) 2_655 8 ?
Fe3 Ge6 Fe1 56.85(10) 3_655 8 ?
Fe3 Ge6 Fe1 111.3(3) 3_656 8 ?
Fe1 Ge6 Fe1 56.84(16) 3_655 8 ?
Ge6 Ge6 Yb2 178.92(16) 3_755 . ?
Fe2 Ge6 Yb2 72.02(19) 9_655 . ?
Fe2 Ge6 Yb2 72.02(19) 2_655 . ?
Fe3 Ge6 Yb2 72.87(16) 3_655 . ?
Fe3 Ge6 Yb2 72.87(16) 3_656 . ?
Fe1 Ge6 Yb2 73.53(19) 3_655 . ?
Fe1 Ge6 Yb2 73.53(19) 8 . ?
Ge3 Fe1 Ge3 180.00(5) 13_556 1_554 ?
Ge3 Fe1 Fe3 60.30(3) 13_556 13_556 ?
Ge3 Fe1 Fe3 119.70(3) 1_554 13_556 ?
Ge3 Fe1 Fe3 119.70(3) 13_556 1_554 ?
Ge3 Fe1 Fe3 60.30(3) 1_554 1_554 ?
Fe3 Fe1 Fe3 180.00(2) 13_556 1_554 ?
Ge3 Fe1 Ge4 108.662(17) 13_556 13_556 ?
Ge3 Fe1 Ge4 71.338(17) 1_554 13_556 ?
Fe3 Fe1 Ge4 58.83(3) 13_556 13_556 ?
Fe3 Fe1 Ge4 121.17(3) 1_554 13_556 ?
Ge3 Fe1 Ge4 71.338(17) 13_556 1_554 ?
Ge3 Fe1 Ge4 108.662(17) 1_554 1_554 ?
Fe3 Fe1 Ge4 121.17(3) 13_556 1_554 ?
Fe3 Fe1 Ge4 58.83(3) 1_554 1_554 ?
Ge4 Fe1 Ge4 180.0 13_556 1_554 ?
Ge3 Fe1 Fe1 59.535(6) 13_556 6 ?
Ge3 Fe1 Fe1 120.465(6) 1_554 6 ?
Fe3 Fe1 Fe1 59.941(12) 13_556 6 ?
Fe3 Fe1 Fe1 120.059(12) 1_554 6 ?
Ge4 Fe1 Fe1 59.966(6) 13_556 6 ?
Ge4 Fe1 Fe1 120.034(6) 1_554 6 ?
Ge3 Fe1 Fe1 120.465(6) 13_556 6_554 ?
Ge3 Fe1 Fe1 59.535(6) 1_554 6_554 ?
Fe3 Fe1 Fe1 120.059(12) 13_556 6_554 ?
Fe3 Fe1 Fe1 59.941(12) 1_554 6_554 ?
Ge4 Fe1 Fe1 120.034(6) 13_556 6_554 ?
Ge4 Fe1 Fe1 59.966(6) 1_554 6_554 ?
Fe1 Fe1 Fe1 180.0 6 6_554 ?
Ge3 Fe1 Ge6 103.26(13) 13_556 3_655 ?
Ge3 Fe1 Ge6 76.74(13) 1_554 3_655 ?
Fe3 Fe1 Ge6 118.63(10) 13_556 3_655 ?
Fe3 Fe1 Ge6 61.37(10) 1_554 3_655 ?
Ge4 Fe1 Ge6 77.29(16) 13_556 3_655 ?
Ge4 Fe1 Ge6 102.71(16) 1_554 3_655 ?
Fe1 Fe1 Ge6 61.58(8) 6 3_655 ?
Fe1 Fe1 Ge6 118.42(8) 6_554 3_655 ?
Ge3 Fe1 Ge6 76.74(13) 13_556 15_455 ?
Ge3 Fe1 Ge6 103.26(13) 1_554 15_455 ?
Fe3 Fe1 Ge6 61.37(10) 13_556 15_455 ?
Fe3 Fe1 Ge6 118.63(10) 1_554 15_455 ?
Ge4 Fe1 Ge6 102.71(16) 13_556 15_455 ?
Ge4 Fe1 Ge6 77.29(16) 1_554 15_455 ?
Fe1 Fe1 Ge6 118.42(8) 6 15_455 ?
Fe1 Fe1 Ge6 61.58(8) 6_554 15_455 ?
Ge3 Fe1 Ge5 104.83(3) 13_556 13 ?
Ge3 Fe1 Ge5 75.17(3) 1_554 13 ?
Fe3 Fe1 Ge5 61.462(19) 13_556 13 ?
Fe3 Fe1 Ge5 118.538(19) 1_554 13 ?
Ge4 Fe1 Ge5 74.87(3) 13_556 13 ?
Ge4 Fe1 Ge5 105.13(3) 1_554 13 ?
Fe1 Fe1 Ge5 118.355(10) 6 13 ?
Fe1 Fe1 Ge5 61.645(10) 6_554 13 ?
Ge3 Fe1 Ge5 75.17(3) 13_556 . ?
Ge3 Fe1 Ge5 104.83(3) 1_554 . ?
Fe3 Fe1 Ge5 118.538(19) 13_556 . ?
Fe3 Fe1 Ge5 61.462(19) 1_554 . ?
Ge4 Fe1 Ge5 105.13(3) 13_556 . ?
Ge4 Fe1 Ge5 74.87(3) 1_554 . ?
Fe1 Fe1 Ge5 61.646(10) 6 . ?
Fe1 Fe1 Ge5 118.354(10) 6_554 . ?
Ge5 Fe1 Ge5 180.0 13 . ?
Ge1 Fe2 Ge1 71.97(3) 1_554 9_556 ?
Ge1 Fe2 Ge2 178.92(4) 1_554 9_656 ?
Ge1 Fe2 Ge2 108.938(17) 9_556 9_656 ?
Ge1 Fe2 Ge2 108.938(17) 1_554 1_554 ?
Ge1 Fe2 Ge2 178.92(4) 9_556 1_554 ?
Ge2 Fe2 Ge2 70.16(3) 9_656 1_554 ?
Ge1 Fe2 Fe3 120.86(4) 1_554 11 ?
Ge1 Fe2 Fe3 59.52(3) 9_556 11 ?
Ge2 Fe2 Fe3 60.22(3) 9_656 11 ?
Ge2 Fe2 Fe3 119.40(4) 1_554 11 ?
Ge1 Fe2 Fe3 59.52(3) 1_554 1_554 ?
Ge1 Fe2 Fe3 120.86(4) 9_556 1_554 ?
Ge2 Fe2 Fe3 119.40(4) 9_656 1_554 ?
Ge2 Fe2 Fe3 60.22(3) 1_554 1_554 ?
Fe3 Fe2 Fe3 179.60(6) 11 1_554 ?
Ge1 Fe2 Fe2 120.517(12) 1_554 10_556 ?
Ge1 Fe2 Fe2 59.484(13) 9_556 10_556 ?
Ge2 Fe2 Fe2 59.880(12) 9_656 10_556 ?
Ge2 Fe2 Fe2 120.120(12) 1_554 10_556 ?
Fe3 Fe2 Fe2 59.959(12) 11 10_556 ?
Fe3 Fe2 Fe2 120.041(12) 1_554 10_556 ?
Ge1 Fe2 Fe2 59.484(12) 1_554 10 ?
Ge1 Fe2 Fe2 120.517(12) 9_556 10 ?
Ge2 Fe2 Fe2 120.120(12) 9_656 10 ?
Ge2 Fe2 Fe2 59.880(12) 1_554 10 ?
Fe3 Fe2 Fe2 120.041(12) 11 10 ?
Fe3 Fe2 Fe2 59.959(12) 1_554 10 ?
Fe2 Fe2 Fe2 180.0 10_556 10 ?
Ge1 Fe2 Ge6 76.30(16) 1_554 9_655 ?
Ge1 Fe2 Ge6 76.27(13) 9_556 9_655 ?
Ge2 Fe2 Ge6 104.45(16) 9_656 9_655 ?
Ge2 Fe2 Ge6 103.31(13) 1_554 9_655 ?
Fe3 Fe2 Ge6 61.72(10) 11 9_655 ?
Fe3 Fe2 Ge6 118.42(10) 1_554 9_655 ?
Fe2 Fe2 Ge6 118.73(8) 10_556 9_655 ?
Fe2 Fe2 Ge6 61.27(8) 10 9_655 ?
Ge1 Fe2 Ge6 76.27(13) 1_554 3_655 ?
Ge1 Fe2 Ge6 76.30(16) 9_556 3_655 ?
Ge2 Fe2 Ge6 103.31(13) 9_656 3_655 ?
Ge2 Fe2 Ge6 104.45(16) 1_554 3_655 ?
Fe3 Fe2 Ge6 118.42(10) 11 3_655 ?
Fe3 Fe2 Ge6 61.72(10) 1_554 3_655 ?
Fe2 Fe2 Ge6 61.27(8) 10_556 3_655 ?
Fe2 Fe2 Ge6 118.73(8) 10 3_655 ?
Ge1 Fe2 Ge5 104.47(3) 1_554 . ?
Ge1 Fe2 Ge5 104.38(3) 9_556 . ?
Ge2 Fe2 Ge5 74.78(4) 9_656 . ?
Ge2 Fe2 Ge5 76.04(3) 1_554 . ?
Fe3 Fe2 Ge5 118.03(2) 11 . ?
Fe3 Fe2 Ge5 61.833(19) 1_554 . ?
Fe2 Fe2 Ge5 61.322(11) 10_556 . ?
Fe2 Fe2 Ge5 118.677(11) 10 . ?
Ge1 Fe2 Ge5 104.38(3) 1_554 11 ?
Ge1 Fe2 Ge5 104.47(3) 9_556 11 ?
Ge2 Fe2 Ge5 76.04(3) 9_656 11 ?
Ge2 Fe2 Ge5 74.78(4) 1_554 11 ?
Fe3 Fe2 Ge5 61.833(19) 11 11 ?
Fe3 Fe2 Ge5 118.03(2) 1_554 11 ?
Fe2 Fe2 Ge5 118.677(11) 10_556 11 ?
Fe2 Fe2 Ge5 61.323(11) 10 11 ?
Ge5 Fe2 Ge5 144.14(6) . 11 ?
Ge4 Fe3 Ge1 178.52(5) . . ?
Ge4 Fe3 Ge3 109.26(5) . . ?
Ge1 Fe3 Ge3 72.22(4) . . ?
Ge4 Fe3 Fe1 60.62(3) . 1_556 ?
Ge1 Fe3 Fe1 120.59(4) . 1_556 ?
Ge3 Fe3 Fe1 59.25(3) . 1_556 ?
Ge4 Fe3 Fe1 60.62(3) . 6 ?
Ge1 Fe3 Fe1 120.59(4) . 6 ?
Ge3 Fe3 Fe1 59.25(3) . 6 ?
Fe1 Fe3 Fe1 60.12(2) 1_556 6 ?
Ge4 Fe3 Fe2 119.26(4) . 10_556 ?
Ge1 Fe3 Fe2 59.53(3) . 10_556 ?
Ge3 Fe3 Fe2 120.88(4) . 10_556 ?
Fe1 Fe3 Fe2 179.87(5) 1_556 10_556 ?
Fe1 Fe3 Fe2 119.901(8) 6 10_556 ?
Ge4 Fe3 Fe2 119.26(4) . 1_556 ?
Ge1 Fe3 Fe2 59.53(3) . 1_556 ?
Ge3 Fe3 Fe2 120.88(4) . 1_556 ?
Fe1 Fe3 Fe2 119.901(8) 1_556 1_556 ?
Fe1 Fe3 Fe2 179.87(5) 6 1_556 ?
Fe2 Fe3 Fe2 60.08(2) 10_556 1_556 ?
Ge4 Fe3 Ge2 69.94(4) . . ?
Ge1 Fe3 Ge2 108.58(5) . . ?
Ge3 Fe3 Ge2 179.20(5) . . ?
Fe1 Fe3 Ge2 120.10(4) 1_556 . ?
Fe1 Fe3 Ge2 120.10(4) 6 . ?
Fe2 Fe3 Ge2 59.77(3) 10_556 . ?
Fe2 Fe3 Ge2 59.77(3) 1_556 . ?
Ge4 Fe3 Ge6 104.27(16) . 3_655 ?
Ge1 Fe3 Ge6 75.98(16) . 3_655 ?
Ge3 Fe3 Ge6 76.48(17) . 3_655 ?
Fe1 Fe3 Ge6 118.97(17) 1_556 3_655 ?
Fe1 Fe3 Ge6 61.78(17) 6 3_655 ?
Fe2 Fe3 Ge6 61.09(17) 10_556 3_655 ?
Fe2 Fe3 Ge6 118.25(17) 1_556 3_655 ?
Ge2 Fe3 Ge6 103.67(17) . 3_655 ?
Ge4 Fe3 Ge6 104.27(16) . 3_656 ?
Ge1 Fe3 Ge6 75.98(16) . 3_656 ?
Ge3 Fe3 Ge6 76.48(17) . 3_656 ?
Fe1 Fe3 Ge6 61.78(17) 1_556 3_656 ?
Fe1 Fe3 Ge6 118.97(17) 6 3_656 ?
Fe2 Fe3 Ge6 118.25(17) 10_556 3_656 ?
Fe2 Fe3 Ge6 61.09(17) 1_556 3_656 ?
Ge2 Fe3 Ge6 103.67(17) . 3_656 ?
Ge4 Fe3 Ge5 75.78(3) . . ?
Ge1 Fe3 Ge5 103.95(3) . . ?
Ge3 Fe3 Ge5 104.34(3) . . ?
Fe1 Fe3 Ge5 118.87(4) 1_556 . ?
Fe1 Fe3 Ge5 61.83(2) 6 . ?
Fe2 Fe3 Ge5 61.11(2) 10_556 . ?
Fe2 Fe3 Ge5 118.11(4) 1_556 . ?
Ge2 Fe3 Ge5 75.52(3) . . ?
Ge4 Fe3 Ge5 75.78(3) . 1_556 ?
Ge1 Fe3 Ge5 103.95(3) . 1_556 ?
Ge3 Fe3 Ge5 104.34(3) . 1_556 ?
Fe1 Fe3 Ge5 61.83(2) 1_556 1_556 ?
Fe1 Fe3 Ge5 118.87(4) 6 1_556 ?
Fe2 Fe3 Ge5 118.11(4) 10_556 1_556 ?
Fe2 Fe3 Ge5 61.11(2) 1_556 1_556 ?
Ge2 Fe3 Ge5 75.52(3) . 1_556 ?
Ge5 Fe3 Ge5 144.79(6) . 1_556 ?
Fe3 Ge1 Fe3 108.75(6) . 3_556 ?
Fe3 Ge1 Fe2 146.09(3) . 2 ?
Fe3 Ge1 Fe2 60.95(2) 3_556 2 ?
Fe3 Ge1 Fe2 60.95(2) . 1_556 ?
Fe3 Ge1 Fe2 146.09(3) 3_556 1_556 ?
Fe2 Ge1 Fe2 145.61(5) 2 1_556 ?
Fe3 Ge1 Fe2 146.09(3) . 9_556 ?
Fe3 Ge1 Fe2 60.95(2) 3_556 9_556 ?
Fe2 Ge1 Fe2 61.03(3) 2 9_556 ?
Fe2 Ge1 Fe2 108.03(3) 1_556 9_556 ?
Fe3 Ge1 Fe2 60.95(2) . 10_556 ?
Fe3 Ge1 Fe2 146.09(3) 3_556 10_556 ?
Fe2 Ge1 Fe2 108.03(3) 2 10_556 ?
Fe2 Ge1 Fe2 61.03(3) 1_556 10_556 ?
Fe2 Ge1 Fe2 145.61(5) 9_556 10_556 ?
Fe3 Ge1 Ge1 107.042(15) . 9_556 ?
Fe3 Ge1 Ge1 107.042(15) 3_556 9_556 ?
Fe2 Ge1 Ge1 54.016(17) 2 9_556 ?
Fe2 Ge1 Ge1 106.86(3) 1_556 9_556 ?
Fe2 Ge1 Ge1 106.86(3) 9_556 9_556 ?
Fe2 Ge1 Ge1 54.016(17) 10_556 9_556 ?
Fe3 Ge1 Ge1 107.042(15) . 9_557 ?
Fe3 Ge1 Ge1 107.042(15) 3_556 9_557 ?
Fe2 Ge1 Ge1 106.86(3) 2 9_557 ?
Fe2 Ge1 Ge1 54.016(17) 1_556 9_557 ?
Fe2 Ge1 Ge1 54.016(17) 9_556 9_557 ?
Fe2 Ge1 Ge1 106.86(3) 10_556 9_557 ?
Ge1 Ge1 Ge1 119.59(7) 9_556 9_557 ?
Fe3 Ge1 Yb1 72.79(2) . . ?
Fe3 Ge1 Yb1 72.79(2) 3_556 . ?
Fe2 Ge1 Yb1 73.310(11) 2 . ?
Fe2 Ge1 Yb1 125.984(18) 1_556 . ?
Fe2 Ge1 Yb1 125.984(18) 9_556 . ?
Fe2 Ge1 Yb1 73.310(11) 10_556 . ?
Ge1 Ge1 Yb1 60.74(2) 9_556 . ?
Ge1 Ge1 Yb1 179.68(5) 9_557 . ?
Fe3 Ge1 Yb1 72.79(2) . 1_556 ?
Fe3 Ge1 Yb1 72.79(2) 3_556 1_556 ?
Fe2 Ge1 Yb1 125.984(18) 2 1_556 ?
Fe2 Ge1 Yb1 73.310(10) 1_556 1_556 ?
Fe2 Ge1 Yb1 73.310(11) 9_556 1_556 ?
Fe2 Ge1 Yb1 125.984(18) 10_556 1_556 ?
Ge1 Ge1 Yb1 179.67(5) 9_556 1_556 ?
Ge1 Ge1 Yb1 60.74(2) 9_557 1_556 ?
Yb1 Ge1 Yb1 118.94(4) . 1_556 ?
Fe3 Ge1 Ge3 54.37(3) . . ?
Fe3 Ge1 Ge3 54.37(3) 3_556 . ?
Fe2 Ge1 Ge3 107.20(2) 2 . ?
Fe2 Ge1 Ge3 107.19(2) 1_556 . ?
Fe2 Ge1 Ge3 107.19(2) 9_556 . ?
Fe2 Ge1 Ge3 107.19(2) 10_556 . ?
Ge1 Ge1 Ge3 120.21(3) 9_556 . ?
Ge1 Ge1 Ge3 120.21(3) 9_557 . ?
Yb1 Ge1 Ge3 59.468(19) . . ?
Yb1 Ge1 Ge3 59.467(19) 1_556 . ?
Fe2 Ge2 Fe2 147.46(5) 10_556 9_656 ?
Fe2 Ge2 Fe2 60.24(2) 10_556 1_556 ?
Fe2 Ge2 Fe2 109.84(3) 9_656 1_556 ?
Fe2 Ge2 Fe2 109.84(3) 10_556 2_655 ?
Fe2 Ge2 Fe2 60.24(2) 9_656 2_655 ?
Fe2 Ge2 Fe2 147.46(5) 1_556 2_655 ?
Fe2 Ge2 Fe3 60.01(2) 10_556 . ?
Fe2 Ge2 Fe3 145.86(3) 9_656 . ?
Fe2 Ge2 Fe3 60.01(2) 1_556 . ?
Fe2 Ge2 Fe3 145.86(3) 2_655 . ?
Fe2 Ge2 Fe3 145.86(3) 10_556 3_656 ?
Fe2 Ge2 Fe3 60.01(2) 9_656 3_656 ?
Fe2 Ge2 Fe3 145.86(3) 1_556 3_656 ?
Fe2 Ge2 Fe3 60.01(2) 2_655 3_656 ?
Fe3 Ge2 Fe3 108.41(6) . 3_656 ?
Fe2 Ge2 Yb2 73.73(3) 10_556 9_656 ?
Fe2 Ge2 Yb2 73.73(3) 9_656 9_656 ?
Fe2 Ge2 Yb2 73.73(3) 1_556 9_656 ?
Fe2 Ge2 Yb2 73.73(3) 2_655 9_656 ?
Fe3 Ge2 Yb2 125.80(3) . 9_656 ?
Fe3 Ge2 Yb2 125.80(3) 3_656 9_656 ?
Fe2 Ge2 Ge4 106.27(3) 10_556 . ?
Fe2 Ge2 Ge4 106.27(3) 9_656 . ?
Fe2 Ge2 Ge4 106.27(3) 1_556 . ?
Fe2 Ge2 Ge4 106.27(3) 2_655 . ?
Fe3 Ge2 Ge4 54.20(3) . . ?
Fe3 Ge2 Ge4 54.20(3) 3_656 . ?
Yb2 Ge2 Ge4 180.0 9_656 . ?
Fe2 Ge2 Ge2 54.919(17) 10_556 9_656 ?
Fe2 Ge2 Ge2 107.55(4) 9_656 9_656 ?
Fe2 Ge2 Ge2 107.55(4) 1_556 9_656 ?
Fe2 Ge2 Ge2 54.919(17) 2_655 9_656 ?
Fe3 Ge2 Ge2 106.567(16) . 9_656 ?
Fe3 Ge2 Ge2 106.567(16) 3_656 9_656 ?
Ge4 Ge2 Ge2 119.18(4) . 9_656 ?
Fe2 Ge2 Ge2 107.55(4) 10_556 9_657 ?
Fe2 Ge2 Ge2 54.919(17) 9_656 9_657 ?
Fe2 Ge2 Ge2 54.919(17) 1_556 9_657 ?
Fe2 Ge2 Ge2 107.55(4) 2_655 9_657 ?
Fe3 Ge2 Ge2 106.567(16) . 9_657 ?
Fe3 Ge2 Ge2 106.567(16) 3_656 9_657 ?
Ge4 Ge2 Ge2 119.18(4) . 9_657 ?
Ge2 Ge2 Ge2 121.65(8) 9_656 9_657 ?
Fe2 Ge2 Yb2 72.47(4) 10_556 . ?
Fe2 Ge2 Yb2 125.081(17) 9_656 . ?
Fe2 Ge2 Yb2 125.081(17) 1_556 . ?
Fe2 Ge2 Yb2 72.47(4) 2_655 . ?
Fe3 Ge2 Yb2 73.41(4) . . ?
Fe3 Ge2 Yb2 73.41(4) 3_656 . ?
Yb2 Ge2 Yb2 119.22(7) 9_656 . ?
Ge4 Ge2 Yb2 60.78(7) . . ?
Ge2 Ge2 Yb2 58.40(8) 9_656 . ?
Ge2 Ge2 Yb2 179.95(9) 9_657 . ?
Fe1 Ge3 Fe1 148.25(5) 1_556 3 ?
Fe1 Ge3 Fe1 60.931(12) 1_556 6 ?
Fe1 Ge3 Fe1 109.65(2) 3 6 ?
Fe1 Ge3 Fe1 109.65(2) 1_556 8_456 ?
Fe1 Ge3 Fe1 60.931(12) 3 8_456 ?
Fe1 Ge3 Fe1 148.25(5) 6 8_456 ?
Fe1 Ge3 Fe3 145.02(3) 1_556 3_556 ?
Fe1 Ge3 Fe3 60.45(2) 3 3_556 ?
Fe1 Ge3 Fe3 145.02(3) 6 3_556 ?
Fe1 Ge3 Fe3 60.45(2) 8_456 3_556 ?
Fe1 Ge3 Fe3 60.45(2) 1_556 . ?
Fe1 Ge3 Fe3 145.02(3) 3 . ?
Fe1 Ge3 Fe3 60.45(2) 6 . ?
Fe1 Ge3 Fe3 145.02(3) 8_456 . ?
Fe3 Ge3 Fe3 106.81(6) 3_556 . ?
Fe1 Ge3 Yb1 72.415(9) 1_556 1_556 ?
Fe1 Ge3 Yb1 125.158(12) 3 1_556 ?
Fe1 Ge3 Yb1 125.158(12) 6 1_556 ?
Fe1 Ge3 Yb1 72.415(9) 8_456 1_556 ?
Fe3 Ge3 Yb1 72.64(2) 3_556 1_556 ?
Fe3 Ge3 Yb1 72.64(2) . 1_556 ?
Fe1 Ge3 Yb1 125.158(12) 1_556 . ?
Fe1 Ge3 Yb1 72.416(9) 3 . ?
Fe1 Ge3 Yb1 72.416(9) 6 . ?
Fe1 Ge3 Yb1 125.158(12) 8_456 . ?
Fe3 Ge3 Yb1 72.64(2) 3_556 . ?
Fe3 Ge3 Yb1 72.64(2) . . ?
Yb1 Ge3 Yb1 119.95(4) 1_556 . ?
Fe1 Ge3 Ge4 54.847(11) 1_556 13_557 ?
Fe1 Ge3 Ge4 107.47(3) 3 13_557 ?
Fe1 Ge3 Ge4 107.47(3) 6 13_557 ?
Fe1 Ge3 Ge4 54.847(11) 8_456 13_557 ?
Fe3 Ge3 Ge4 107.476(15) 3_556 13_557 ?
Fe3 Ge3 Ge4 107.476(15) . 13_557 ?
Yb1 Ge3 Ge4 60.27(2) 1_556 13_557 ?
Yb1 Ge3 Ge4 179.78(4) . 13_557 ?
Fe1 Ge3 Ge4 107.47(3) 1_556 13_556 ?
Fe1 Ge3 Ge4 54.847(11) 3 13_556 ?
Fe1 Ge3 Ge4 54.847(11) 6 13_556 ?
Fe1 Ge3 Ge4 107.47(3) 8_456 13_556 ?
Fe3 Ge3 Ge4 107.476(15) 3_556 13_556 ?
Fe3 Ge3 Ge4 107.476(15) . 13_556 ?
Yb1 Ge3 Ge4 179.78(4) 1_556 13_556 ?
Yb1 Ge3 Ge4 60.27(2) . 13_556 ?
Ge4 Ge3 Ge4 119.51(5) 13_557 13_556 ?
Fe1 Ge3 Yb2 74.13(2) 1_556 13_556 ?
Fe1 Ge3 Yb2 74.13(2) 3 13_556 ?
Fe1 Ge3 Yb2 74.13(2) 6 13_556 ?
Fe1 Ge3 Yb2 74.13(2) 8_456 13_556 ?
Fe3 Ge3 Yb2 126.60(3) 3_556 13_556 ?
Fe3 Ge3 Yb2 126.60(3) . 13_556 ?
Yb1 Ge3 Yb2 120.03(2) 1_556 13_556 ?
Yb1 Ge3 Yb2 120.03(2) . 13_556 ?
Ge4 Ge3 Yb2 59.75(3) 13_557 13_556 ?
Ge4 Ge3 Yb2 59.75(3) 13_556 13_556 ?
Fe3 Ge4 Fe3 111.71(6) 3_656 . ?
Fe3 Ge4 Fe1 60.55(2) 3_656 8_556 ?
Fe3 Ge4 Fe1 147.55(2) . 8_556 ?
Fe3 Ge4 Fe1 147.55(2) 3_656 6 ?
Fe3 Ge4 Fe1 60.55(2) . 6 ?
Fe1 Ge4 Fe1 143.43(5) 8_556 6 ?
Fe3 Ge4 Fe1 60.55(2) 3_656 3_655 ?
Fe3 Ge4 Fe1 147.55(2) . 3_655 ?
Fe1 Ge4 Fe1 60.067(13) 8_556 3_655 ?
Fe1 Ge4 Fe1 107.59(2) 6 3_655 ?
Fe3 Ge4 Fe1 147.55(2) 3_656 1_556 ?
Fe3 Ge4 Fe1 60.55(2) . 1_556 ?
Fe1 Ge4 Fe1 107.59(2) 8_556 1_556 ?
Fe1 Ge4 Fe1 60.067(13) 6 1_556 ?
Fe1 Ge4 Fe1 143.43(5) 3_655 1_556 ?
Fe3 Ge4 Ge2 55.86(3) 3_656 . ?
Fe3 Ge4 Ge2 55.86(3) . . ?
Fe1 Ge4 Ge2 108.28(2) 8_556 . ?
Fe1 Ge4 Ge2 108.28(2) 6 . ?
Fe1 Ge4 Ge2 108.28(2) 3_655 . ?
Fe1 Ge4 Ge2 108.28(2) 1_556 . ?
Fe3 Ge4 Yb2 73.72(4) 3_656 1_556 ?
Fe3 Ge4 Yb2 73.72(4) . 1_556 ?
Fe1 Ge4 Yb2 73.92(4) 8_556 1_556 ?
Fe1 Ge4 Yb2 126.178(11) 6 1_556 ?
Fe1 Ge4 Yb2 126.178(11) 3_655 1_556 ?
Fe1 Ge4 Yb2 73.92(4) 1_556 1_556 ?
Ge2 Ge4 Yb2 60.04(7) . 1_556 ?
Fe3 Ge4 Yb2 73.72(4) 3_656 . ?
Fe3 Ge4 Yb2 73.72(4) . . ?
Fe1 Ge4 Yb2 126.178(11) 8_556 . ?
Fe1 Ge4 Yb2 73.92(4) 6 . ?
Fe1 Ge4 Yb2 73.92(4) 3_655 . ?
Fe1 Ge4 Yb2 126.178(11) 1_556 . ?
Ge2 Ge4 Yb2 60.03(7) . . ?
Yb2 Ge4 Yb2 120.07(14) 1_556 . ?
Fe3 Ge4 Ge3 106.423(14) 3_656 13_557 ?
Fe3 Ge4 Ge3 106.423(14) . 13_557 ?
Fe1 Ge4 Ge3 53.815(12) 8_556 13_557 ?
Fe1 Ge4 Ge3 105.92(3) 6 13_557 ?
Fe1 Ge4 Ge3 105.92(3) 3_655 13_557 ?
Fe1 Ge4 Ge3 53.815(12) 1_556 13_557 ?
Ge2 Ge4 Ge3 120.25(3) . 13_557 ?
Fe3 Ge4 Ge3 106.423(14) 3_656 13_556 ?
Fe3 Ge4 Ge3 106.423(14) . 13_556 ?
Fe1 Ge4 Ge3 105.92(3) 8_556 13_556 ?
Fe1 Ge4 Ge3 53.815(12) 6 13_556 ?
Fe1 Ge4 Ge3 53.815(12) 3_655 13_556 ?
Fe1 Ge4 Ge3 105.92(3) 1_556 13_556 ?
Ge2 Ge4 Ge3 120.25(3) . 13_556 ?
Ge3 Ge4 Ge3 119.50(5) 13_557 13_556 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Yb1 Ge5 2.8358(10) . ?
Yb1 Ge5 2.8358(10) 3 ?
Yb1 Ge3 2.9302(6) . ?
Yb1 Ge3 2.9302(6) 1_554 ?
Yb1 Ge1 2.9453(6) . ?
Yb1 Ge1 2.9453(6) 1_554 ?
Yb1 Ge4 2.9456(13) 13_556 ?
Yb1 Ge1 2.9732(12) 9_556 ?
Yb1 Fe1 3.2274(4) 6 ?
Yb1 Fe1 3.2274(4) . ?
Yb1 Fe1 3.2274(4) 8_455 ?
Ge5 Ge5 2.5097(19) 3_655 ?
Ge5 Fe2 2.6433(9) 10_556 ?
Ge5 Fe2 2.6433(9) . ?
Ge5 Fe3 2.6616(5) 1_554 ?
Ge5 Fe3 2.6616(5) . ?
Ge5 Fe1 2.6709(9) 6 ?
Ge5 Fe1 2.6709(9) . ?
Yb2 Ge2 2.836(4) 9_656 ?
Yb2 Ge6 2.843(8) 3_655 ?
Yb2 Ge6 2.843(8) . ?
Yb2 Ge2 2.907(2) . ?
Yb2 Ge2 2.907(2) 1_554 ?
Yb2 Ge4 2.928(2) . ?
Yb2 Ge4 2.928(2) 1_554 ?
Yb2 Ge3 2.942(4) 13_556 ?
Yb2 Fe2 3.227(3) 10_556 ?
Yb2 Fe2 3.227(3) 2_655 ?
Yb2 Fe2 3.227(3) 9_655 ?
Yb2 Fe2 3.227(3) . ?
Ge6 Ge6 2.496(15) 3_755 ?
Ge6 Fe2 2.639(7) 9_655 ?
Ge6 Fe2 2.639(7) 2_655 ?
Ge6 Fe3 2.655(2) 3_655 ?
Ge6 Fe3 2.655(2) 3_656 ?
Ge6 Fe1 2.665(7) 3_655 ?
Ge6 Fe1 2.665(7) 8 ?
Fe1 Ge3 2.5018(4) 13_556 ?
Fe1 Ge3 2.5018(4) 1_554 ?
Fe1 Fe3 2.5325(9) 13_556 ?
Fe1 Fe3 2.5325(9) 1_554 ?
Fe1 Ge4 2.5344(4) 13_556 ?
Fe1 Ge4 2.5344(4) 1_554 ?
Fe1 Fe1 2.5369(3) 6 ?
Fe1 Fe1 2.5369(3) 6_554 ?
Fe2 Ge1 2.4981(9) 1_554 ?
Fe2 Ge1 2.4981(9) 9_556 ?
Fe2 Ge2 2.5278(9) 9_656 ?
Fe2 Ge2 2.5278(9) 1_554 ?
Fe2 Fe3 2.5338(9) 11 ?
Fe2 Fe3 2.5338(9) 1_554 ?
Fe2 Fe2 2.5369(3) 10_556 ?
Fe2 Fe2 2.5369(3) 10 ?
Fe3 Ge4 2.4886(12) . ?
Fe3 Ge1 2.4978(12) . ?
Fe3 Ge3 2.5288(12) . ?
Fe3 Ge2 2.5393(12) . ?
Ge1 Ge1 2.9356(11) 9_556 ?
Ge1 Ge1 2.9356(11) 9_557 ?
Ge1 Ge3 2.9625(15) . ?
Ge2 Ge4 2.8819(16) . ?
Ge2 Ge2 2.9056(11) 9_656 ?
Ge2 Ge2 2.9056(11) 9_657 ?
Ge3 Ge4 2.9368(8) 13_557 ?
Ge3 Ge4 2.9368(8) 13_556 ?
