#------------------------------------------------------------------------------
#$Date: 2016-03-26 15:49:15 +0100 (Sat 26 de Mar de 2016) $
#$Revision: 180357 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/26/7202642.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7202642
loop_
_publ_author_name
'Song, Yu-Fei'
'Abbas, Hamera'
'Ritchie, Chris'
'McMillian, Nicola'
'Long, De-Liang'
'Gadegaard, Nikolaj'
'Cronin, Leroy'
_publ_section_title
;
 From polyoxometalate building blocks to polymers and materials: the
 silver connection
;
_journal_issue                   19
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              1903
_journal_paper_doi               10.1039/b617830h
_journal_volume                  17
_journal_year                    2007
_chemical_formula_moiety         'C16 H48 Ag4 Mo8 O34 S8'
_chemical_formula_sum            'C16 H48 Ag4 Mo8 O34 S8'
_chemical_formula_weight         2240.02
_chemical_name_common            'Compound ha003'
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.200(2)
_cell_angle_beta                 113.487(1)
_cell_angle_gamma                108.774(1)
_cell_formula_units_Z            1
_cell_length_a                   10.8053(3)
_cell_length_b                   11.1381(3)
_cell_length_c                   13.3396(3)
_cell_measurement_reflns_used    10970
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      1.51
_cell_volume                     1333.30(6)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor 1997)'
_computing_data_collection       'Collect (Nonius BV, 1997-2000)'
_computing_data_reduction
'HKL Denzo and Scalepack (Otwinowski & Minor 1997)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Nonius Kappa CCD'
_diffrn_measurement_method       'ω & π scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0483
_diffrn_reflns_av_sigmaI/netI    0.0352
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            18453
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.74
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    3.646
_exptl_absorpt_correction_T_max  0.7844
_exptl_absorpt_correction_T_min  0.6293
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.790
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1068
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.07
_refine_diff_density_max         0.86
_refine_diff_density_min         -1.08
_refine_diff_density_rms         0.14
_refine_ls_extinction_coef       0.00233(13)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.068
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     317
_refine_ls_number_reflns         5233
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.068
_refine_ls_R_factor_all          0.0307
_refine_ls_R_factor_gt           0.0249
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0234P)²+2.1287P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0575
_refine_ls_wR_factor_ref         0.0600
_reflns_number_gt                4664
_reflns_number_total             5233
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b617830h.txt
_cod_data_source_block           ha003
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7202642
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.98486(3) 0.79882(3) 0.16926(3) 0.02222(9) Uani 1 1 d . . .
Ag2 Ag 0.52705(3) 0.51263(3) -0.33500(2) 0.01967(9) Uani 1 1 d . . .
Mo1 Mo 0.82422(3) 0.85203(3) 0.59062(3) 0.01184(8) Uani 1 1 d . . .
Mo2 Mo 0.83182(3) 1.06038(3) 0.22507(3) 0.01290(8) Uani 1 1 d . . .
Mo3 Mo 0.74076(3) 0.80200(3) 0.31101(3) 0.01145(8) Uani 1 1 d . . .
Mo4 Mo 1.08147(3) 0.88646(3) 0.49002(2) 0.01014(8) Uani 1 1 d . . .
S1 S 1.31977(10) 0.82175(10) 0.16463(8) 0.0228(2) Uani 1 1 d . . .
S2 S 0.40768(10) 0.57128(9) -0.13840(8) 0.0186(2) Uani 1 1 d . . .
S3 S 0.78457(11) 0.62499(11) -0.12346(8) 0.0233(2) Uani 1 1 d . . .
S4 S 0.35011(10) 0.58795(9) -0.48890(8) 0.01478(19) Uani 1 1 d . . .
O1 O 1.1537(3) 0.7617(3) 0.1207(2) 0.0327(8) Uani 1 1 d . . .
O2 O 0.4433(3) 0.6304(3) -0.2256(2) 0.0258(6) Uani 1 1 d . . .
O3 O 0.7872(3) 0.6132(3) -0.0117(2) 0.0279(7) Uani 1 1 d . . .
O4 O 0.3264(3) 0.5670(3) -0.6099(2) 0.0193(6) Uani 1 1 d . . .
O5 O 0.7890(3) 0.7287(2) 0.2208(2) 0.0160(5) Uani 1 1 d . . .
O6 O 0.5764(3) 0.6861(3) 0.2881(2) 0.0180(6) Uani 1 1 d . . .
O7 O 0.8791(3) 0.7758(2) 0.4525(2) 0.0125(5) Uani 1 1 d . . .
O8 O 0.7615(2) 0.9377(2) 0.4658(2) 0.0125(5) Uani 1 1 d . . .
O9 O 0.6703(3) 0.7077(3) 0.5377(2) 0.0189(6) Uani 1 1 d . . .
O10 O 1.0292(3) 1.1976(2) 0.3121(2) 0.0137(5) Uani 1 1 d . . .
O11 O 0.8084(3) 0.9529(3) 0.6883(2) 0.0180(6) Uani 1 1 d . . .
O12 O 0.9624(2) 0.9858(2) 0.3868(2) 0.0116(5) Uani 1 1 d . . .
O13 O 1.1019(3) 0.8009(2) 0.3875(2) 0.0148(5) Uani 1 1 d . . .
O14 O 0.8319(3) 1.1566(2) 0.3871(2) 0.0132(5) Uani 1 1 d . . .
O15 O 0.7347(3) 1.1356(3) 0.1430(2) 0.0214(6) Uani 1 1 d . . .
O16 O 0.8638(3) 0.9652(3) 0.1348(2) 0.0183(6) Uani 1 1 d . . .
O17 O 0.6801(3) 0.9210(2) 0.2356(2) 0.0143(5) Uani 1 1 d . . .
C1 C 1.3647(5) 0.9834(5) 0.1452(4) 0.0317(10) Uani 1 1 d . . .
H1A H 1.3282 0.9753 0.0635 0.048 Uiso 1 1 calc R . .
H1B H 1.4722 1.0337 0.1857 0.048 Uiso 1 1 calc R . .
H1C H 1.3182 1.0297 0.1757 0.048 Uiso 1 1 calc R . .
C2 C 1.3983(4) 0.8676(4) 0.3165(3) 0.0231(9) Uani 1 1 d . . .
H2A H 1.3827 0.7876 0.3418 0.035 Uiso 1 1 calc R . .
H2B H 1.3509 0.9183 0.3409 0.035 Uiso 1 1 calc R . .
H2C H 1.5046 0.9222 0.3504 0.035 Uiso 1 1 calc R . .
C3 C 0.4958(5) 0.7075(4) -0.0122(3) 0.0263(9) Uani 1 1 d . . .
H3A H 0.6031 0.7349 0.0227 0.039 Uiso 1 1 calc R . .
H3B H 0.4606 0.6805 0.0421 0.039 Uiso 1 1 calc R . .
H3C H 0.4720 0.7819 -0.0323 0.039 Uiso 1 1 calc R . .
C4 C 0.2205(4) 0.5480(4) -0.1785(4) 0.0258(9) Uani 1 1 d . . .
H4A H 0.1537 0.4741 -0.2487 0.039 Uiso 1 1 calc R . .
H4B H 0.2084 0.6290 -0.1917 0.039 Uiso 1 1 calc R . .
H4C H 0.1970 0.5280 -0.1171 0.039 Uiso 1 1 calc R . .
C5 C 0.9229(5) 0.5786(5) -0.1356(4) 0.0317(10) Uani 1 1 d . . .
H5A H 0.8919 0.4827 -0.1482 0.048 Uiso 1 1 calc R . .
H5B H 1.0165 0.6255 -0.0650 0.048 Uiso 1 1 calc R . .
H5C H 0.9359 0.6021 -0.2002 0.048 Uiso 1 1 calc R . .
C6 C 0.8699(5) 0.7990(5) -0.1019(4) 0.0331(11) Uani 1 1 d . . .
H6A H 0.8059 0.8407 -0.0937 0.050 Uiso 1 1 calc R . .
H6B H 0.8852 0.8141 -0.1676 0.050 Uiso 1 1 calc R . .
H6C H 0.9654 0.8377 -0.0324 0.050 Uiso 1 1 calc R . .
C7 C 0.4087(4) 0.7610(4) -0.4287(3) 0.0201(8) Uani 1 1 d . . .
H7A H 0.5096 0.8090 -0.4163 0.030 Uiso 1 1 calc R . .
H7B H 0.4066 0.7761 -0.3555 0.030 Uiso 1 1 calc R . .
H7C H 0.3421 0.7930 -0.4811 0.030 Uiso 1 1 calc R . .
C8 C 0.1686(4) 0.5314(4) -0.5004(3) 0.0224(9) Uani 1 1 d . . .
H8A H 0.1187 0.4348 -0.5330 0.034 Uiso 1 1 calc R . .
H8B H 0.1116 0.5725 -0.5501 0.034 Uiso 1 1 calc R . .
H8C H 0.1761 0.5559 -0.4243 0.034 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Ag1 O5 151.95(10) . . ?
O1 Ag1 O3 86.46(9) . . ?
O5 Ag1 O3 80.38(8) . . ?
O1 Ag1 O16 132.38(10) . . ?
O5 Ag1 O16 74.07(8) . . ?
O3 Ag1 O16 96.40(9) . . ?
O4 Ag2 O6 93.16(9) 2_664 2_665 ?
O4 Ag2 O2 163.03(9) 2_664 . ?
O6 Ag2 O2 89.76(9) 2_665 . ?
O4 Ag2 S4 115.48(7) 2_664 . ?
O6 Ag2 S4 119.58(6) 2_665 . ?
O2 Ag2 S4 77.07(7) . . ?
O4 Ag2 S3 82.65(6) 2_664 . ?
O6 Ag2 S3 93.66(6) 2_665 . ?
O2 Ag2 S3 80.48(7) . . ?
S4 Ag2 S3 139.25(3) . . ?
O9 Mo1 O11 104.94(12) . . ?
O9 Mo1 O10 101.03(12) . 2_776 ?
O11 Mo1 O10 101.21(11) . 2_776 ?
O9 Mo1 O8 100.36(11) . . ?
O11 Mo1 O8 96.11(11) . . ?
O10 Mo1 O8 147.86(10) 2_776 . ?
O9 Mo1 O7 89.54(10) . . ?
O11 Mo1 O7 162.94(11) . . ?
O10 Mo1 O7 84.43(9) 2_776 . ?
O8 Mo1 O7 72.03(9) . . ?
O9 Mo1 O12 161.51(11) . 2_776 ?
O11 Mo1 O12 93.20(10) . 2_776 ?
O10 Mo1 O12 78.41(9) 2_776 2_776 ?
O8 Mo1 O12 73.74(9) . 2_776 ?
O7 Mo1 O12 71.99(8) . 2_776 ?
O15 Mo2 O16 105.04(13) . . ?
O15 Mo2 O10 103.83(12) . . ?
O16 Mo2 O10 98.28(11) . . ?
O15 Mo2 O17 102.36(12) . . ?
O16 Mo2 O17 98.69(11) . . ?
O10 Mo2 O17 143.71(10) . . ?
O15 Mo2 O14 94.17(11) . . ?
O16 Mo2 O14 160.80(11) . . ?
O10 Mo2 O14 76.84(9) . . ?
O17 Mo2 O14 76.63(9) . . ?
O15 Mo2 O12 163.38(11) . . ?
O16 Mo2 O12 91.57(10) . . ?
O10 Mo2 O12 73.67(9) . . ?
O17 Mo2 O12 74.03(9) . . ?
O14 Mo2 O12 69.22(8) . . ?
O6 Mo3 O5 105.31(12) . . ?
O6 Mo3 O17 101.76(12) . . ?
O5 Mo3 O17 101.06(11) . . ?
O6 Mo3 O7 99.88(11) . . ?
O5 Mo3 O7 95.65(11) . . ?
O17 Mo3 O7 147.96(10) . . ?
O6 Mo3 O8 92.09(10) . . ?
O5 Mo3 O8 160.46(10) . . ?
O17 Mo3 O8 83.62(10) . . ?
O7 Mo3 O8 72.21(9) . . ?
O6 Mo3 O12 164.11(10) . . ?
O5 Mo3 O12 90.05(10) . . ?
O17 Mo3 O12 78.75(9) . . ?
O7 Mo3 O12 74.06(9) . . ?
O8 Mo3 O12 72.11(8) . . ?
O6 Mo3 Mo4 134.69(9) . . ?
O5 Mo3 Mo4 82.22(8) . . ?
O17 Mo3 Mo4 120.90(7) . . ?
O7 Mo3 Mo4 35.03(7) . . ?
O8 Mo3 Mo4 79.17(6) . . ?
O12 Mo3 Mo4 42.15(6) . . ?
O13 Mo4 O14 105.20(12) . 2_776 ?
O13 Mo4 O7 100.94(11) . . ?
O14 Mo4 O7 96.82(11) 2_776 . ?
O13 Mo4 O8 101.06(11) . 2_776 ?
O14 Mo4 O8 96.85(11) 2_776 2_776 ?
O7 Mo4 O8 149.98(10) . 2_776 ?
O13 Mo4 O12 97.59(11) . . ?
O14 Mo4 O12 157.21(10) 2_776 . ?
O7 Mo4 O12 78.95(9) . . ?
O8 Mo4 O12 78.12(9) 2_776 . ?
O13 Mo4 O12 172.84(10) . 2_776 ?
O14 Mo4 O12 81.97(10) 2_776 2_776 ?
O7 Mo4 O12 77.83(9) . 2_776 ?
O8 Mo4 O12 77.80(9) 2_776 2_776 ?
O12 Mo4 O12 75.25(10) . 2_776 ?
O13 Mo4 Mo3 89.54(8) . . ?
O14 Mo4 Mo3 133.22(8) 2_776 . ?
O7 Mo4 Mo3 36.41(7) . . ?
O8 Mo4 Mo3 124.04(7) 2_776 . ?
O12 Mo4 Mo3 45.93(6) . . ?
O12 Mo4 Mo3 85.37(6) 2_776 . ?
O1 S1 C2 105.42(18) . . ?
O1 S1 C1 105.8(2) . . ?
C2 S1 C1 99.2(2) . . ?
O2 S2 C3 105.23(19) . . ?
O2 S2 C4 105.18(18) . . ?
C3 S2 C4 97.9(2) . . ?
O3 S3 C6 104.81(18) . . ?
O3 S3 C5 108.6(2) . . ?
C6 S3 C5 99.1(2) . . ?
O3 S3 Ag2 123.91(12) . . ?
C6 S3 Ag2 108.74(16) . . ?
C5 S3 Ag2 108.86(14) . . ?
O4 S4 C7 107.33(18) . . ?
O4 S4 C8 105.32(17) . . ?
C7 S4 C8 98.39(18) . . ?
O4 S4 Ag2 123.87(11) . . ?
C7 S4 Ag2 106.28(14) . . ?
C8 S4 Ag2 112.61(14) . . ?
S1 O1 Ag1 137.90(17) . . ?
S2 O2 Ag2 117.51(16) . . ?
S3 O3 Ag1 118.37(15) . . ?
S4 O4 Ag2 120.21(14) . 2_664 ?
Mo3 O5 Ag1 135.34(13) . . ?
Mo3 O6 Ag2 141.84(14) . 2_665 ?
Mo4 O7 Mo3 108.56(11) . . ?
Mo4 O7 Mo1 109.83(10) . . ?
Mo3 O7 Mo1 103.71(10) . . ?
Mo4 O8 Mo1 108.76(11) 2_776 . ?
Mo4 O8 Mo3 109.87(10) 2_776 . ?
Mo1 O8 Mo3 103.98(10) . . ?
Mo1 O10 Mo2 116.53(12) 2_776 . ?
Mo4 O12 Mo1 92.70(8) . 2_776 ?
Mo4 O12 Mo3 91.92(9) . . ?
Mo1 O12 Mo3 163.05(12) 2_776 . ?
Mo4 O12 Mo4 104.75(10) . 2_776 ?
Mo1 O12 Mo4 97.37(9) 2_776 2_776 ?
Mo3 O12 Mo4 97.20(8) . 2_776 ?
Mo4 O12 Mo2 163.32(12) . . ?
Mo1 O12 Mo2 85.87(8) 2_776 . ?
Mo3 O12 Mo2 85.04(8) . . ?
Mo4 O12 Mo2 91.91(8) 2_776 . ?
Mo4 O14 Mo2 116.90(12) 2_776 . ?
Mo2 O16 Ag1 130.28(13) . . ?
Mo3 O17 Mo2 115.93(12) . . ?
S1 C1 H1A 109.5 . . ?
S1 C1 H1B 109.5 . . ?
H1A C1 H1B 109.5 . . ?
S1 C1 H1C 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
S1 C2 H2A 109.5 . . ?
S1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
S1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
S2 C3 H3A 109.5 . . ?
S2 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
S2 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
S2 C4 H4A 109.5 . . ?
S2 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
S2 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
S3 C5 H5A 109.5 . . ?
S3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
S3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
S3 C6 H6A 109.5 . . ?
S3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
S3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
S4 C7 H7A 109.5 . . ?
S4 C7 H7B 109.5 . . ?
H7A C7 H7B 109.5 . . ?
S4 C7 H7C 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
S4 C8 H8A 109.5 . . ?
S4 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
S4 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O1 2.298(3) . ?
Ag1 O5 2.407(2) . ?
Ag1 O3 2.542(3) . ?
Ag1 O16 2.580(3) . ?
Ag2 O4 2.346(2) 2_664 ?
Ag2 O6 2.420(3) 2_665 ?
Ag2 O2 2.451(3) . ?
Ag2 S4 2.6286(10) . ?
Ag2 S3 2.8083(10) . ?
Mo1 O9 1.705(2) . ?
Mo1 O11 1.710(2) . ?
Mo1 O10 1.899(2) 2_776 ?
Mo1 O8 2.014(2) . ?
Mo1 O7 2.295(2) . ?
Mo1 O12 2.302(2) 2_776 ?
Mo2 O15 1.698(3) . ?
Mo2 O16 1.715(2) . ?
Mo2 O10 1.928(2) . ?
Mo2 O17 1.928(2) . ?
Mo2 O14 2.289(2) . ?
Mo2 O12 2.472(2) . ?
Mo3 O6 1.705(2) . ?
Mo3 O5 1.707(2) . ?
Mo3 O17 1.888(2) . ?
Mo3 O7 2.013(2) . ?
Mo3 O8 2.287(2) . ?
Mo3 O12 2.312(2) . ?
Mo3 Mo4 3.2158(4) . ?
Mo4 O13 1.696(2) . ?
Mo4 O14 1.748(2) 2_776 ?
Mo4 O7 1.947(2) . ?
Mo4 O8 1.959(2) 2_776 ?
Mo4 O12 2.159(2) . ?
Mo4 O12 2.328(2) 2_776 ?
S1 O1 1.517(3) . ?
S1 C2 1.782(4) . ?
S1 C1 1.788(5) . ?
S2 O2 1.523(3) . ?
S2 C3 1.787(4) . ?
S2 C4 1.791(4) . ?
S3 O3 1.503(3) . ?
S3 C6 1.785(5) . ?
S3 C5 1.787(4) . ?
S4 O4 1.505(3) . ?
S4 C7 1.784(4) . ?
S4 C8 1.791(4) . ?
O4 Ag2 2.346(2) 2_664 ?
O6 Ag2 2.420(3) 2_665 ?
O8 Mo4 1.959(2) 2_776 ?
O10 Mo1 1.899(2) 2_776 ?
O12 Mo1 2.302(2) 2_776 ?
O12 Mo4 2.328(2) 2_776 ?
O14 Mo4 1.748(2) 2_776 ?
C1 H1A 0.9800 . ?
C1 H1B 0.9800 . ?
C1 H1C 0.9800 . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C3 H3C 0.9800 . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C7 H7C 0.9800 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
