#------------------------------------------------------------------------------
#$Date: 2025-08-22 23:12:46 +0200 (Fri 22 de Aug de 2025) $
#$Revision: 301866 $
#$URL: svn://www.crystallography.net/cod/cif/7/23/68/7236865.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7236865
loop_
_publ_author_name
'Sun, Lin'
'Wei, Shilong'
'Zhang, Jun'
'Wang, Wenyuan'
'Chen, Sanping'
'Zhang, Yiquan'
'Wei, Qing'
'Xie, Gang'
'Gao, Shengli'
_publ_section_title
;
 Isomeric ligands enhance the anisotropy barrier within nine-coordinated
 {Dy2} compounds
;
_journal_issue                   36
_journal_name_full               'Journal of Materials Chemistry C'
_journal_page_first              9488
_journal_paper_doi               10.1039/C7TC02786A
_journal_volume                  5
_journal_year                    2017
_chemical_formula_moiety         'C32 H36 Dy2 N10 O12, 4(H2 O)'
_chemical_formula_sum            'C32 H44 Dy2 N10 O16'
_chemical_formula_weight         1149.77
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2017-08-21 deposited with the CCDC.
2017-08-23 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 97.960(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.6569(7)
_cell_length_b                   13.0716(5)
_cell_length_c                   18.0859(7)
_cell_measurement_reflns_used    4230
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.8310
_cell_measurement_theta_min      3.8410
_cell_volume                     4134.1(3)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.848
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0374
_diffrn_reflns_av_unetI/netI     0.0561
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.848
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            11114
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.848
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.323
_diffrn_reflns_theta_min         3.318
_exptl_absorpt_coefficient_mu    3.668
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.82314
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
'SADABS 2015/2 (Bruker,2015) was used for absorption correction. R(int) was  0.07741 before and 0.05435 after correction. The Ratio of minimum to maximum transmission is 0.8231. The λ/2 correction factor is 0.0015.'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.847
_exptl_crystal_description       block
_exptl_crystal_F_000             2264
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.19
_refine_diff_density_max         1.059
_refine_diff_density_min         -0.742
_refine_diff_density_rms         0.144
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.946
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     261
_refine_ls_number_reflns         4803
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.946
_refine_ls_R_factor_all          0.0634
_refine_ls_R_factor_gt           0.0418
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0840P)²+1.2560P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1129
_refine_ls_wR_factor_ref         0.1290
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3688
_reflns_number_total             4803
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c7tc02786a2.cif
_cod_data_source_block           exp_0803_2-1
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7236865
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.18874(2) 0.83873(2) 0.56712(2) 0.02625(12) Uani 1 1 d . . . .
O6 O 0.2633(3) 0.8418(3) 0.4683(2) 0.0314(10) Uani 1 1 d . . . .
O5 O 0.3183(2) 0.8284(3) 0.6188(2) 0.0339(10) Uani 1 1 d . . . .
H5A H 0.3450 0.7878 0.5923 0.051 Uiso 1 1 d R U . .
H5B H 0.3227 0.8029 0.6650 0.051 Uiso 1 1 d R U . .
O1 O 0.0934(2) 0.7738(3) 0.4755(2) 0.0331(10) Uani 1 1 d . . . .
O2 O 0.0841(3) 0.8700(5) 0.6389(3) 0.0550(14) Uani 1 1 d . . . .
O3 O 0.1972(3) 0.8662(4) 0.7021(3) 0.0518(13) Uani 1 1 d . . . .
C1 C -0.1070(5) 0.8217(9) 0.2710(5) 0.062(3) Uani 1 1 d . . . .
H1 H -0.1381 0.8669 0.2409 0.074 Uiso 1 1 calc R U . .
N4 N 0.0786(4) 1.1332(5) 0.4546(3) 0.0440(14) Uani 1 1 d . . . .
H4A H 0.0959 1.1389 0.4109 0.053 Uiso 1 1 d R U . .
H4B H 0.0307 1.1107 0.4472 0.053 Uiso 1 1 d R U . .
N3 N 0.1160(3) 0.9675(4) 0.4905(3) 0.0299(11) Uani 1 1 d . . . .
N2 N 0.0584(3) 0.9364(5) 0.4343(3) 0.0362(12) Uani 1 1 d . . . .
C6 C 0.0512(3) 0.8378(5) 0.4315(3) 0.0321(14) Uani 1 1 d . . . .
C8 C 0.1825(2) 1.1032(3) 0.5529(2) 0.0333(14) Uani 1 1 d G . . .
N5 N 0.2246(2) 1.0274(2) 0.5938(2) 0.0380(13) Uani 1 1 d G . . .
C12 C 0.2815(3) 1.0540(3) 0.6516(3) 0.060(2) Uani 1 1 d G . . .
H12 H 0.3097 1.0032 0.6790 0.071 Uiso 1 1 calc R U . .
C11 C 0.2963(3) 1.1564(3) 0.6685(3) 0.070(3) Uani 1 1 d G . . .
H11 H 0.3344 1.1742 0.7071 0.084 Uiso 1 1 calc R U . .
C10 C 0.2542(3) 1.2323(2) 0.6275(3) 0.063(2) Uani 1 1 d G . . .
H10 H 0.2641 1.3008 0.6388 0.076 Uiso 1 1 calc R U . .
C9 C 0.1973(3) 1.2057(2) 0.5697(3) 0.051(2) Uani 1 1 d G . . .
H9 H 0.1691 1.2564 0.5423 0.062 Uiso 1 1 calc R U . .
C2 C -0.0731(5) 0.6591(7) 0.3026(5) 0.059(2) Uani 1 1 d . . . .
H2 H -0.0793 0.5890 0.2952 0.071 Uiso 1 1 calc R U . .
C5 C -0.0548(4) 0.8617(7) 0.3267(4) 0.0501(19) Uani 1 1 d . . . .
H5 H -0.0507 0.9322 0.3333 0.060 Uiso 1 1 calc R U . .
C7 C 0.1231(3) 1.0657(5) 0.4968(3) 0.0320(13) Uani 1 1 d . . . .
C4 C -0.0088(3) 0.7972(6) 0.3723(3) 0.0397(16) Uani 1 1 d . . . .
C3 C -0.0190(4) 0.6940(7) 0.3612(4) 0.0501(18) Uani 1 1 d . . . .
H3 H 0.0098 0.6476 0.3924 0.060 Uiso 1 1 calc R U . .
C13 C 0.1273(5) 0.8757(7) 0.7008(4) 0.0463(18) Uani 1 1 d . . . .
N1 N -0.1158(3) 0.7227(7) 0.2574(3) 0.059(2) Uani 1 1 d . . . .
C14 C 0.0971(6) 0.8897(10) 0.7659(5) 0.091(4) Uani 1 1 d . . . .
H14A H 0.0632 0.9312 0.7587 0.137 Uiso 1 1 d R U . .
H14B H 0.1358 0.9126 0.8049 0.137 Uiso 1 1 d R U . .
H14C H 0.0760 0.8263 0.7804 0.137 Uiso 1 1 d R U . .
C15 C 0.2954(4) 0.8820(6) 0.4166(4) 0.0426(16) Uani 1 1 d . . A 2
C16 C 0.2858(9) 0.9926(7) 0.4021(8) 0.113(5) Uani 1 1 d . . A 2
H16A H 0.2524 1.0029 0.3561 0.170 Uiso 1 1 calc R U A 2
H16B H 0.3346 1.0229 0.3985 0.170 Uiso 1 1 calc R U A 2
H16C H 0.2640 1.0241 0.4422 0.170 Uiso 1 1 calc R U A 2
O17 O 0.3344(4) 0.8278(4) 0.3780(3) 0.0531(15) Uani 1 1 d . . A 2
O9 O 0.4653(10) 0.1398(10) 0.5356(7) 0.210(7) Uani 1 1 d . . B 2
H9A H 0.5019 0.1825 0.5393 0.314 Uiso 1 1 d R U B 2
H9B H 0.4816 0.0828 0.5538 0.314 Uiso 1 1 d R U B 2
O10 O 0.5264(6) 0.1204(12) 0.6826(6) 0.190(6) Uani 1 1 d . . C -1
H10A H 0.5411 0.1533 0.6594 0.285 Uiso 1 1 d R U C -1
H10B H 0.5564 0.1002 0.7206 0.285 Uiso 1 1 d R U C -1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Dy1 O5 145.22(14) . .
O1 Dy1 O6 83.81(15) . .
O5 Dy1 O6 71.86(16) . .
O1 Dy1 N3 65.02(15) . .
O5 Dy1 N3 132.40(16) . .
O6 Dy1 N3 82.08(16) . .
O1 Dy1 O2 85.09(17) . .
O5 Dy1 O2 124.45(17) . .
O6 Dy1 O2 160.70(17) . .
N3 Dy1 O2 78.93(18) . .
O1 Dy1 O3 133.96(17) . .
O5 Dy1 O3 71.97(17) . .
O6 Dy1 O3 141.93(17) . .
N3 Dy1 O3 114.91(18) . .
O2 Dy1 O3 52.48(18) . .
O1 Dy1 O17 79.73(18) . 7_566
O5 Dy1 O17 89.75(19) . 7_566
O6 Dy1 O17 117.62(15) . 7_566
N3 Dy1 O17 137.9(2) . 7_566
O2 Dy1 O17 75.61(19) . 7_566
O3 Dy1 O17 73.58(19) . 7_566
O1 Dy1 N5 127.68(13) . .
O5 Dy1 N5 77.30(13) . .
O6 Dy1 N5 88.70(14) . .
N3 Dy1 N5 62.66(14) . .
O2 Dy1 N5 85.66(19) . .
O3 Dy1 N5 72.14(17) . .
O17 Dy1 N5 145.61(16) 7_566 .
O1 Dy1 O6 74.11(14) . 7_566
O5 Dy1 O6 73.48(14) . 7_566
O6 Dy1 O6 66.25(15) . 7_566
N3 Dy1 O6 130.40(15) . 7_566
O2 Dy1 O6 125.22(18) . 7_566
O3 Dy1 O6 113.48(16) . 7_566
O17 Dy1 O6 51.37(16) 7_566 7_566
N5 Dy1 O6 146.13(14) . 7_566
O1 Dy1 C13 110.0(2) . .
O5 Dy1 C13 97.90(19) . .
O6 Dy1 C13 164.8(2) . .
N3 Dy1 C13 97.73(19) . .
O2 Dy1 C13 26.55(19) . .
O3 Dy1 C13 25.9(2) . .
O17 Dy1 C13 72.5(2) 7_566 .
N5 Dy1 C13 77.8(2) . .
O6 Dy1 C13 122.62(19) 7_566 .
O1 Dy1 C15 76.28(19) . 7_566
O5 Dy1 C15 80.10(18) . 7_566
O6 Dy1 C15 92.15(17) . 7_566
N3 Dy1 C15 141.2(2) . 7_566
O2 Dy1 C15 100.5(2) . 7_566
O3 Dy1 C15 93.04(19) . 7_566
O17 Dy1 C15 25.49(18) 7_566 7_566
N5 Dy1 C15 155.92(17) . 7_566
O6 Dy1 C15 25.90(16) 7_566 7_566
C13 Dy1 C15 97.2(2) . 7_566
C15 O6 Dy1 156.2(4) . .
C15 O6 Dy1 90.0(4) . 7_566
Dy1 O6 Dy1 113.74(15) . 7_566
Dy1 O5 H5A 112.2 . .
Dy1 O5 H5B 110.4 . .
H5A O5 H5B 107.2 . .
C6 O1 Dy1 119.3(4) . .
C13 O2 Dy1 94.2(4) . .
C13 O3 Dy1 94.1(4) . .
N1 C1 C5 124.0(8) . .
N1 C1 H1 118.0 . .
C5 C1 H1 118.0 . .
C7 N4 H4A 108.3 . .
C7 N4 H4B 109.7 . .
H4A N4 H4B 109.3 . .
C7 N3 N2 113.9(5) . .
C7 N3 Dy1 126.9(4) . .
N2 N3 Dy1 119.2(4) . .
C6 N2 N3 112.1(5) . .
O1 C6 N2 124.4(6) . .
O1 C6 C4 119.6(6) . .
N2 C6 C4 115.9(6) . .
N5 C8 C9 120.0 . .
N5 C8 C7 114.6(3) . .
C9 C8 C7 125.4(3) . .
C8 N5 C12 120.0 . .
C8 N5 Dy1 118.93(18) . .
C12 N5 Dy1 120.92(18) . .
C11 C12 N5 120.0 . .
C11 C12 H12 120.0 . .
N5 C12 H12 120.0 . .
C12 C11 C10 120.0 . .
C12 C11 H11 120.0 . .
C10 C11 H11 120.0 . .
C9 C10 C11 120.0 . .
C9 C10 H10 120.0 . .
C11 C10 H10 120.0 . .
C10 C9 C8 120.0 . .
C10 C9 H9 120.0 . .
C8 C9 H9 120.0 . .
N1 C2 C3 122.1(8) . .
N1 C2 H2 118.9 . .
C3 C2 H2 118.9 . .
C1 C5 C4 119.4(9) . .
C1 C5 H5 120.3 . .
C4 C5 H5 120.3 . .
N3 C7 N4 124.0(6) . .
N3 C7 C8 116.9(5) . .
N4 C7 C8 119.1(6) . .
C5 C4 C3 117.6(7) . .
C5 C4 C6 121.1(7) . .
C3 C4 C6 121.3(7) . .
C4 C3 C2 119.6(8) . .
C4 C3 H3 120.2 . .
C2 C3 H3 120.2 . .
O3 C13 O2 119.2(6) . .
O3 C13 C14 120.1(8) . .
O2 C13 C14 120.7(8) . .
O3 C13 Dy1 60.0(4) . .
O2 C13 Dy1 59.2(4) . .
C14 C13 Dy1 177.8(8) . .
C2 N1 C1 117.2(7) . .
C13 C14 H14A 108.6 . .
C13 C14 H14B 110.6 . .
H14A C14 H14B 110.3 . .
C13 C14 H14C 109.3 . .
H14A C14 H14C 108.6 . .
H14B C14 H14C 109.5 . .
O6 C15 O17 120.5(7) . .
O6 C15 C16 118.9(7) . .
O17 C15 C16 120.6(7) . .
O6 C15 Dy1 64.1(4) . 7_566
O17 C15 Dy1 56.5(4) . 7_566
C16 C15 Dy1 175.5(7) . 7_566
C15 C16 H16A 109.5 . .
C15 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C15 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C15 O17 Dy1 98.0(4) . 7_566
H9A O9 H9B 109.4 . .
H10A O10 H10B 116.6 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O1 2.350(4) .
Dy1 O5 2.352(4) .
Dy1 O6 2.363(4) .
Dy1 N3 2.431(5) .
Dy1 O2 2.434(5) .
Dy1 O3 2.452(5) .
Dy1 O17 2.450(5) 7_566
Dy1 N5 2.575(3) .
Dy1 O6 2.617(4) 7_566
Dy1 C13 2.825(7) .
Dy1 C15 2.909(8) 7_566
O6 C15 1.271(8) .
O6 Dy1 2.617(4) 7_566
O5 H5A 0.8920 .
O5 H5B 0.8919 .
O1 C6 1.313(7) .
O2 C13 1.266(9) .
O3 C13 1.239(9) .
C1 N1 1.322(12) .
C1 C5 1.372(11) .
C1 H1 0.9300 .
N4 C7 1.346(8) .
N4 H4A 0.8895 .
N4 H4B 0.8889 .
N3 C7 1.294(8) .
N3 N2 1.396(7) .
N2 C6 1.295(8) .
C6 C4 1.495(9) .
C8 N5 1.3900 .
C8 C9 1.3900 .
C8 C7 1.440(7) .
N5 C12 1.3900 .
C12 C11 1.3900 .
C12 H12 0.9300 .
C11 C10 1.3900 .
C11 H11 0.9300 .
C10 C9 1.3900 .
C10 H10 0.9300 .
C9 H9 0.9300 .
C2 N1 1.325(12) .
C2 C3 1.402(11) .
C2 H2 0.9300 .
C5 C4 1.366(11) .
C5 H5 0.9300 .
C4 C3 1.371(11) .
C3 H3 0.9300 .
C13 C14 1.371(11) .
C14 H14A 0.8047 .
C14 H14B 0.9597 .
C14 H14C 0.9601 .
C15 O17 1.264(8) .
C15 C16 1.476(11) .
C15 Dy1 2.909(8) 7_566
C16 H16A 0.9600 .
C16 H16B 0.9600 .
C16 H16C 0.9600 .
O17 Dy1 2.450(5) 7_566
O9 H9A 0.8491 .
O9 H9B 0.8493 .
O10 H10A 0.6758 .
O10 H10B 0.8510 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C7 N3 N2 C6 -177.6(6) . .
Dy1 N3 N2 C6 0.6(7) . .
Dy1 O1 C6 N2 0.5(8) . .
Dy1 O1 C6 C4 179.1(4) . .
N3 N2 C6 O1 -0.7(9) . .
N3 N2 C6 C4 -179.4(5) . .
C9 C8 N5 C12 0.0 . .
C7 C8 N5 C12 -177.4(5) . .
C9 C8 N5 Dy1 175.6(3) . .
C7 C8 N5 Dy1 -1.8(4) . .
C8 N5 C12 C11 0.0 . .
Dy1 N5 C12 C11 -175.5(3) . .
N5 C12 C11 C10 0.0 . .
C12 C11 C10 C9 0.0 . .
C11 C10 C9 C8 0.0 . .
N5 C8 C9 C10 0.0 . .
C7 C8 C9 C10 177.1(5) . .
N1 C1 C5 C4 -0.6(14) . .
N2 N3 C7 N4 1.2(9) . .
Dy1 N3 C7 N4 -176.9(5) . .
N2 N3 C7 C8 -178.9(5) . .
Dy1 N3 C7 C8 3.0(8) . .
N5 C8 C7 N3 -0.5(7) . .
C9 C8 C7 N3 -177.8(4) . .
N5 C8 C7 N4 179.4(5) . .
C9 C8 C7 N4 2.1(8) . .
C1 C5 C4 C3 -2.0(12) . .
C1 C5 C4 C6 177.3(7) . .
O1 C6 C4 C5 178.6(6) . .
N2 C6 C4 C5 -2.7(10) . .
O1 C6 C4 C3 -2.2(10) . .
N2 C6 C4 C3 176.5(7) . .
C5 C4 C3 C2 2.6(12) . .
C6 C4 C3 C2 -176.7(7) . .
N1 C2 C3 C4 -0.7(13) . .
Dy1 O3 C13 O2 -1.0(9) . .
Dy1 O3 C13 C14 177.5(9) . .
Dy1 O2 C13 O3 1.0(9) . .
Dy1 O2 C13 C14 -177.5(9) . .
C3 C2 N1 C1 -1.9(13) . .
C5 C1 N1 C2 2.5(13) . .
Dy1 O6 C15 O17 180.0(7) . .
Dy1 O6 C15 O17 -3.2(8) 7_566 .
Dy1 O6 C15 C16 -0.6(18) . .
Dy1 O6 C15 C16 176.3(10) 7_566 .
Dy1 O6 C15 Dy1 -176.8(12) . 7_566
O6 C15 O17 Dy1 3.4(8) . 7_566
C16 C15 O17 Dy1 -176.0(10) . 7_566
loop_
_cod_related_entry_id
_cod_related_entry_database
_cod_related_entry_code
1 PubChem 168339835
