#------------------------------------------------------------------------------
#$Date: 2016-02-19 15:29:56 +0100 (Fri, 19 Feb 2016) $
#$Revision: 176759 $
#$URL: svn://saulius.grazulis.lt/cod-secondary/cif/2/00/02/2000212.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000212
loop_
_publ_author_name
'Davies, J. A.'
'Pinkerton, A. A.'
'Vilmer, M.'
_publ_section_title
<i>cis</i>,<i>cis</i>-[Bis(dimethylphosphino)methane]tetrachlorodipalladium(II)
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              2092
_journal_page_last               2094
_journal_paper_doi               10.1107/S0108270191004869
_journal_volume                  47
_journal_year                    1991
_chemical_formula_sum            'C10 H28 Cl4 P4 Pd2'
_chemical_formula_weight         626.84
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.380(10)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   8.8930(10)
_cell_length_b                   9.712
_cell_length_c                   12.745(3)
_cell_volume                     1070.9(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    2.45
_exptl_crystal_density_diffrn    1.94
_exptl_crystal_F_000             616
_cod_data_source_file            cr0322.cif
_cod_data_source_block           cr0322a
_cod_original_cell_volume        1071.00(6)
_cod_database_code               2000212
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Pd(1) .57415(4) .43823(4) .36202(2)
Cl(1) .4911(2) .59280(10) .21736(9)
Cl(2) .8294(2) .4702(2) .34450(10)
P(1) .67650(10) .31000(10) .50957(9)
P(2) .31870(10) .41710(10) .35613(9)
C(1) .7698(5) .4184(5) .6226(4)
C(2) .5656(6) .1915(5) .5698(4)
C(3) .8323(6) .1977(6) .4920(5)
C(4) .2380(6) .2985(6) .4372(4)
C(5) .2122(6) .3661(6) .2230(4)
H(1) .871 .438 .614
H(2) .777 .365 .686
H(3) .631 .149 .631
H(4) .486 .240 .592
H(5) .522 .123 .519
H(6) .870 .147 .556
H(7) .795 .136 .434
H(8) .913 .252 .476
H(9) .129 .308 .421
H(10) .264 .207 .422
H(11) .279 .318 .511
H(12) .106 .358 .223
H(13) .225 .434 .172
H(14) .250 .280 .205
