Information card for entry 1100166

Structure parameters

• Formula: C44.75 H32 Ag O2 P2
• Calculated formula: C44.82 H32 Ag O2 P2
• Title of publication: Enantioselective O- and N-Nitroso Aldol Synthesis of Tin Enolates. Isolation of Three BINAP-Silver Complexes and Their Role in Regio- and Enantioselectivity
• Authors of publication: Norie Momiyama; Hisashi Yamamoto
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 5360 - 5361
• a: 17.417 ± 0.003 Å
• b: 21.402 ± 0.004 Å
• c: 11.298 ± 0.002 Å
• α: 90°
• β: 117.15 ± 0.03°
• γ: 90°
• Cell volume: 3747.4 ± 1.2 ų
• Cell temperature: 546 ± 2 K
• Ambient diffraction temperature: 546 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0963
• Residual factor for significantly intense reflections: 0.094
• Weighted residual factors for significantly intense reflections: 0.3306
• Weighted residual factors for all reflections included in the refinement: 0.3336
• Goodness-of-fit parameter for all reflections included in the refinement: 1.587
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No