Information card for entry 1100253

Structure parameters

• Chemical name: mer-Trichloro-(triphenylphosphineiminato)-bis(triphenylphosphineimine)-zirconi um tetrahydrofuran solvate
• Formula: C58 H55 Cl3 N3 O P3 Zr
• Calculated formula: C54 H47 Cl3 N3 P3 Zr
• Title of publication: Phosphaniminato-Komplexe des Zirconiums: Die Kristallstrukturen von [ZrCl~3~(NPPh~3~)(HNPPh~3~)~2~] und [ZrCl~2~(NPPh~3~)~2~(HNPPh~3~)~2~]
• Authors of publication: Gröb, Thorsten; Geiseler, Gertraud; Harms, Klaus; Greiner, Andreas; Dehnicke, Kurt
• Journal of publication: Zeitschrift fuer Anorganische und Allgemeine Chemie
• Year of publication: 2002
• Journal volume: 628
• Journal issue: 1
• Pages of publication: 217 - 221
• a: 12.0935 ± 0.0015 Å
• b: 14.8079 ± 0.0017 Å
• c: 18.142 ± 0.002 Å
• α: 71.203 ± 0.013°
• β: 71.216 ± 0.013°
• γ: 74.401 ± 0.013°
• Cell volume: 2861.91 ų
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 4.76
• Weighted residual factors for significantly intense reflections: 4.76
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No