Information card for entry 1100260

Structure parameters

• Chemical name: Iodo-tris(triphenylphosphineimine)-sodium tetrahydrofuran solvate
• Formula: C56 H52 I N3 Na O0.5 P3
• Calculated formula: C182 H180 I N9 Na O4.5 P9
• Title of publication: Die Kristallstrukturen der Phosphanimin-Komplexe [NaI(HNPPh~3~)~3~] und [SrI~2~(HNPPh~3~)~2~(THF)~2~] sowie des Natrium-triphenylphosphaniminats [NaNPPh~3~]~6~
• Authors of publication: Gröb, Thorsten; Müller, Christoph; Massa, W.; Miekisch, Thomas; Seybert, Gert; Harms, Klaus; Dehnicke, Kurt
• Journal of publication: Zeitschrift fuer Anorganische und Allgemeine Chemie
• Year of publication: 2001
• Journal volume: 627
• Journal issue: 9
• Pages of publication: 2191 - 2197
• a: 15.3323 ± 0.0004 Å
• b: 15.3323 ± 0.0004 Å
• c: 25.4556 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5182.37 ų
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 7
• Space group number: 165
• Hermann-Mauguin space group symbol: P -3 c 1
• Hall space group symbol: -P 3 2"c
• Residual factor for significantly intense reflections: 4.17
• Weighted residual factors for significantly intense reflections: 4.17
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No