Information card for entry 1100272

Structure parameters

• Chemical name: (N-(2',4',6'-tris-t-butylphenyl)-E-pent-1-enamide)-tris(tetrahydrofuran)-lithium
• Formula: C35 H62 Li N O3
• Calculated formula: C38 H71 Li N O3
• Title of publication: Crystal structure of (3THF)-N-lithiium-N-(2',4',6'-tris-t-butyl-phenyl)-E'pentene(1)-amide, C~35~H~62~LiNO~3~
• Authors of publication: Bosold, F.; Marsch, M.; Harms, K.; Boche, G.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2001
• Journal volume: 216
• Journal issue: 1-4
• Pages of publication: 427 - 428
• a: 9.1764 ± 0.0006 Å
• b: 13.1644 ± 0.001 Å
• c: 30.036 ± 0.003 Å
• α: 90°
• β: 95.112 ± 0.008°
• γ: 90°
• Cell volume: 3613.97 ų
• Ambient diffraction temperature: 213 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 7.85
• Weighted residual factors for significantly intense reflections: 7.85
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No