Information card for entry 1100395

Structure parameters

• Formula: C68 H160 Li8 N18 O7 Si10
• Calculated formula: C336 H928 Li24 N52 O24 Si64
• Title of publication: {6 Lithio(trimethylsilyl)diazomethane · 2 Lithio[4,5-bis(trimethylsilyl)triazene] · 7 Diethyl Ether}: The First X-Ray Structure Analysis of a Lithiated Diazoalkane
• Authors of publication: Boche, Gernot; Harms, Klaus; Marsch, Michael; Schubert, Frank
• Journal of publication: Chemische Berichte
• Year of publication: 1994
• Journal volume: 127
• Journal issue: 11
• Pages of publication: 2193 - 2195
• a: 23.356 ± 0.005 Å
• b: 16.078 ± 0.003 Å
• c: 15.402 ± 0.003 Å
• α: 90°
• β: 101.92 ± 0.03°
• γ: 90°
• Cell volume: 5659.01 ų
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No