Information card for entry 1100574

Structure parameters

• Formula: C28 H64 N4 O2 Si2 Ti2
• Calculated formula: C62 H146 N8 O4 Si4 Ti4
• Title of publication: Synthese eines Titana-Oxacyclohexanringes durch kontrollierte Ringöffnung von Tetrahydrofuran. Kristallstrukturen von [Ti(CH~2~)~4~O{Me~2~Si(NBut)~2~}]~2~, [TiCl{Me~2~Si(NBut)~2~}]~3~(μ~3~-O)(μ~3~-Cl) und [Li~2~(THF)~3~{Me~2~Si(NBut)~2~}]
• Authors of publication: Mommertz, Andreas; Leo, Roland; Massa, Werner; Harms, Klaus; Dehnicke, Kurt
• Journal of publication: Zeitschrift fuer Anorganische und Allgemeine Chemie
• Year of publication: 1998
• Journal volume: 624
• Journal issue: 10
• Pages of publication: 1647 - 1652
• a: 8.6362 ± 0.0015 Å
• b: 8.957 ± 0.002 Å
• c: 13.116 ± 0.002 Å
• α: 73.365 ± 0.019°
• β: 73.53 ± 0.02°
• γ: 76.594 ± 0.017°
• Cell volume: 919.61 ų
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No