Information card for entry 1100674

Structure parameters

• Formula: C74 H74 N10 O2 P2 Zn2
• Calculated formula: C74 H74 N10 O2 P2 Zn2
• Title of publication: Crystal Structure of a Dinuclear 1,2-Bis(diphenylphosphinooxide)ethane-bridged (6,8,15,17-Tetramethyldibenzo[b,i][1,4,8,11]-tetraazacyclotetradecinato) zinc(II) Complex
• Authors of publication: Shen, Xuan; Sakata, Kazunori; Hashimoto, Mamoru
• Journal of publication: Analytical Sciences: X-ray Structure Analysis Online
• Year of publication: 2003
• Journal volume: 19
• Pages of publication: x49 - x50
• a: 15.456 ± 0.003 Å
• b: 9.993 ± 0.002 Å
• c: 21.691 ± 0.002 Å
• α: 90°
• β: 103.23 ± 0.01°
• γ: 90°
• Cell volume: 3261 ± 1 ų
• Cell temperature: 293.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for all reflections included in the refinement: 0.1567
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No