Information card for entry 1100871

Structure parameters

• Formula: C35 H51 F12 N O2 P2 W
• Calculated formula: C35 H51 F12 N O2 P2 W
• Title of publication: Double Phosphaalkyne Insertion to a Tungsten Alkylidene: Formation of a Diphosphametallabicyclobutane
• Authors of publication: Jamison, Gregory M.; Wheeler, David R.; Loy, Douglas A.; Ziller, Joseph W.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 10
• Pages of publication: 2245 - 2247
• a: 42.11 ± 0.005 Å
• b: 10.6323 ± 0.0009 Å
• c: 20.577 ± 0.002 Å
• α: 90°
• β: 117.67 ± 0.006°
• γ: 90°
• Cell volume: 8159.4 ± 1.4 ų
• Cell temperature: 163 K
• Ambient diffraction temperature: 163 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for all reflections: 0.0714
• Weighted residual factors for significantly intense reflections: 0.065
• Goodness-of-fit parameter for all reflections: 1.06
• Goodness-of-fit parameter for significantly intense reflections: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No