Information card for entry 1100893

Structure parameters

• Formula: C34 H10 B F24 N P2 Pd
• Calculated formula: C34 H10 B F24 N P2 Pd
• Title of publication: Electron-Poor Pentafluorophenyl-Substituted PCP‒Palladium Pincer Complexes
• Authors of publication: Chase, Preston A.; Gagliardo, Marcella; Lutz, Martin; Spek, Anthony L.; van Klink, Gerard P. M.; van Koten, Gerard
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 9
• Pages of publication: 2016 - 2019
• a: 10.1565 ± 0.0002 Å
• b: 25.6619 ± 0.0005 Å
• c: 16.1795 ± 0.0003 Å
• α: 90°
• β: 110.544 ± 0.0008°
• γ: 90°
• Cell volume: 3948.77 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.0931
• Weighted residual factors for all reflections included in the refinement: 0.1001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No