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Information card for entry 1502080
Preview
Coordinates | 1502080.cif |
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Original paper (by DOI) | HTML |
Formula | C32 H29 N O Si |
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Calculated formula | C32 H29 N O Si |
SMILES | c1cccc2c3ccccc3n(c12)/C=C/C#CC(c1ccccc1)(c1ccccc1)O[Si](C)(C)C |
Title of publication | (E)-9-(2-iodovinyl)-9H-carbazole: a new coupling reagent for the synthesis of π-conjugated carbazoles. |
Authors of publication | Pawluć, Piotr; Franczyk, Adrian; Walkowiak, Jędrzej; Hreczycho, Grzegorz; Kubicki, Maciej; Marciniec, Bogdan |
Journal of publication | Organic letters |
Year of publication | 2011 |
Journal volume | 13 |
Journal issue | 8 |
Pages of publication | 1976 - 1979 |
a | 8.497 ± 0.002 Å |
b | 17.41 ± 0.003 Å |
c | 17.576 ± 0.003 Å |
α | 90.96 ± 0.02° |
β | 96.2 ± 0.02° |
γ | 100.08 ± 0.02° |
Cell volume | 2543.3 ± 0.9 Å3 |
Cell temperature | 100 ± 1 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.196 |
Residual factor for significantly intense reflections | 0.0889 |
Weighted residual factors for significantly intense reflections | 0.1833 |
Weighted residual factors for all reflections included in the refinement | 0.2314 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.971 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1502080.html
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