Information card for entry 1502140

Structure parameters

• Formula: C23 H22 O2
• Calculated formula: C23 H22 O2
• Title of publication: Diasteroselective preparation of cyclopropanols using methylene bis(iodozinc).
• Authors of publication: Cheng, Kevin; Carroll, Patrick J.; Walsh, Patrick J.
• Journal of publication: Organic letters
• Year of publication: 2011
• Journal volume: 13
• Journal issue: 9
• Pages of publication: 2346 - 2349
• a: 8.8401 ± 0.0013 Å
• b: 13.1944 ± 0.0019 Å
• c: 15.906 ± 0.002 Å
• α: 95.193 ± 0.007°
• β: 98.155 ± 0.007°
• γ: 96.746 ± 0.007°
• Cell volume: 1812.9 ± 0.4 ų
• Cell temperature: 143 ± 1 K
• Ambient diffraction temperature: 143 ± 1 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.0993
• Weighted residual factors for all reflections included in the refinement: 0.1047
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No