Information card for entry 1502347

Structure parameters

• Formula: C18 H31 Br O Si
• Calculated formula: C18 H31 Br O Si
• SMILES: Brc1ccccc1O[Si](C(C)(C)C)(C(C)(C)C)CC(C)C
• Title of publication: Di-tert-butylisobutylsilyl, another useful protecting group.
• Authors of publication: Liang, Huan; Hu, Lin; Corey, E. J.
• Journal of publication: Organic letters
• Year of publication: 2011
• Journal volume: 13
• Journal issue: 15
• Pages of publication: 4120 - 4123
• a: 7.9868 ± 0.0014 Å
• b: 16.291 ± 0.003 Å
• c: 15.104 ± 0.003 Å
• α: 90°
• β: 100.77 ± 0.002°
• γ: 90°
• Cell volume: 1930.6 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0355
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0589
• Weighted residual factors for all reflections included in the refinement: 0.0624
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No