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Information card for entry 1502427
Preview
Coordinates | 1502427.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H19 N O |
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Calculated formula | C24 H19 N O |
SMILES | O=C(c1[nH]c(c2ccccc2)cc1c1ccccc1)c1ccc(cc1)C |
Title of publication | Three-component synthesis of polysubstituted pyrroles from α-diazoketones, nitroalkenes, and amines. |
Authors of publication | Hong, Deng; Zhu, Yuanxun; Li, Yao; Lin, Xufeng; Lu, Ping; Wang, Yanguang |
Journal of publication | Organic letters |
Year of publication | 2011 |
Journal volume | 13 |
Journal issue | 17 |
Pages of publication | 4668 - 4671 |
a | 8.9942 ± 0.0005 Å |
b | 9.2272 ± 0.0006 Å |
c | 12.0198 ± 0.0008 Å |
α | 99.073 ± 0.005° |
β | 104.225 ± 0.005° |
γ | 101.47 ± 0.005° |
Cell volume | 924.97 ± 0.11 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0715 |
Residual factor for significantly intense reflections | 0.0382 |
Weighted residual factors for significantly intense reflections | 0.09 |
Weighted residual factors for all reflections included in the refinement | 0.0989 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.911 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1502427.html
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