Crystallography Open Database

Information card for entry 1502581

Preview

Coordinates	1502581.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H20 N2 O2
Calculated formula	C20 H20 N2 O2
Title of publication	Synthesis of azines in solid state: reactivity of solid hydrazine with aldehydes and ketones.
Authors of publication	Lee, Byeongno; Lee, Kyu Hyung; Cho, Jaeheung; Nam, Wonwoo; Hur, Nam Hwi
Journal of publication	Organic letters
Year of publication	2011
Journal volume	13
Journal issue	24
Pages of publication	6386 - 6389
a	19.0367 ± 0.0006 Å
b	4.9902 ± 0.0002 Å
c	19.2908 ± 0.0007 Å
α	90°
β	108.317 ± 0.002°
γ	90°
Cell volume	1739.71 ± 0.11 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0484
Residual factor for significantly intense reflections	0.0387
Weighted residual factors for significantly intense reflections	0.0971
Weighted residual factors for all reflections included in the refinement	0.1075
Goodness-of-fit parameter for all reflections included in the refinement	0.835
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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