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Information card for entry 1502851
Preview
Coordinates | 1502851.cif |
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Original paper (by DOI) | HTML |
Formula | C23 H25 N O7 S |
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Calculated formula | C23 H25 N O7 S |
SMILES | S(=O)(=O)(N1c2ccccc2CC(C(=O)OC)(C(=O)OC)[C@H]1CC(=O)C)c1ccc(cc1)C |
Title of publication | Diphosphine-catalyzed mixed double-Michael reaction: a unified synthesis of indolines, dihydropyrrolopyridines, benzimidazolines, tetrahydroquinolines, tetrahydroisoquinolines, dihydrobenzo-1,4-oxazines, and dihydrobenzo-3,1-oxazines. |
Authors of publication | Sriramurthy, Vardhineedi; Kwon, Ohyun |
Journal of publication | Organic letters |
Year of publication | 2010 |
Journal volume | 12 |
Journal issue | 5 |
Pages of publication | 1084 - 1087 |
a | 8.7615 ± 0.0011 Å |
b | 9.7378 ± 0.0012 Å |
c | 26.004 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2218.6 ± 0.5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.039 |
Residual factor for significantly intense reflections | 0.0334 |
Weighted residual factors for significantly intense reflections | 0.0787 |
Weighted residual factors for all reflections included in the refinement | 0.081 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.241 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1502851.html
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