Information card for entry 1503219
| Formula |
C189 H264 N4 O24 |
| Calculated formula |
C188.98 H264 N4 O24 |
| Title of publication |
DIBPillar[n]arenes (n = 5, 6): syntheses, X-ray crystal structures, and complexation with n-octyltriethyl ammonium hexafluorophosphate. |
| Authors of publication |
Han, Chengyou; Ma, Fengying; Zhang, Zibin; Xia, Binyuan; Yu, Yihua; Huang, Feihe |
| Journal of publication |
Organic letters |
| Year of publication |
2010 |
| Journal volume |
12 |
| Journal issue |
19 |
| Pages of publication |
4360 - 4363 |
| a |
13.7506 ± 0.0003 Å |
| b |
18.3037 ± 0.0004 Å |
| c |
19.5207 ± 0.0004 Å |
| α |
78.89 ± 0.002° |
| β |
78.46 ± 0.002° |
| γ |
78.098 ± 0.002° |
| Cell volume |
4651.17 ± 0.18 Å3 |
| Cell temperature |
293 ± 2 K |
| Ambient diffraction temperature |
293 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.111 |
| Residual factor for significantly intense reflections |
0.0999 |
| Weighted residual factors for significantly intense reflections |
0.288 |
| Weighted residual factors for all reflections included in the refinement |
0.3003 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.143 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/1503219.html
