Information card for entry 1503754

Structure parameters

• Formula: C22 H21 Cl O
• Calculated formula: C22 H21 Cl O
• Title of publication: Enantioselective reactions of donor/acceptor carbenoids derived from alpha-aryl-alpha-diazoketones.
• Authors of publication: Denton, Justin R.; Davies, Huw M. L.
• Journal of publication: Organic letters
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 4
• Pages of publication: 787 - 790
• a: 16.428 ± 0.002 Å
• b: 6.3139 ± 0.0008 Å
• c: 18.813 ± 0.002 Å
• α: 90°
• β: 106.092 ± 0.002°
• γ: 90°
• Cell volume: 1874.9 ± 0.4 ų
• Cell temperature: 90 ± 1 K
• Ambient diffraction temperature: 90 ± 1 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0816
• Weighted residual factors for all reflections included in the refinement: 0.0899
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No