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Information card for entry 1503769
Preview
Coordinates | 1503769.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H25 F Si |
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Calculated formula | C19 H25 F Si |
SMILES | [Si](C(=C(\F)C(C)(C)C)/c1cccc2ccccc12)(C)(C)C |
Title of publication | Stereocontrolled approach to bromofluoroalkenes and their use for the synthesis of tri- and tetrasubstituted fluoroalkenes. |
Authors of publication | Landelle, Grégory; Champagne, Pier Alexandre; Barbeau, Xavier; Paquin, Jean-François |
Journal of publication | Organic letters |
Year of publication | 2009 |
Journal volume | 11 |
Journal issue | 3 |
Pages of publication | 681 - 684 |
a | 8.5973 ± 0.001 Å |
b | 13.7008 ± 0.0016 Å |
c | 15.9798 ± 0.0019 Å |
α | 90° |
β | 105.287 ± 0.002° |
γ | 90° |
Cell volume | 1815.7 ± 0.4 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1305 |
Residual factor for significantly intense reflections | 0.0621 |
Weighted residual factors for significantly intense reflections | 0.1385 |
Weighted residual factors for all reflections included in the refinement | 0.1635 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.197 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1503769.html
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