Information card for entry 1503786

Structure parameters

• Formula: C39 H36 O11
• Calculated formula: C39 H36 O11
• Title of publication: Sn-free Ni-catalyzed reductive coupling of glycosyl bromides with activated alkenes.
• Authors of publication: Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagné, Michel R
• Journal of publication: Organic letters
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 4
• Pages of publication: 879 - 882
• a: 17.0749 ± 0.0005 Å
• b: 24.0641 ± 0.0006 Å
• c: 24.8996 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10231 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1268
• Residual factor for significantly intense reflections: 0.0661
• Weighted residual factors for significantly intense reflections: 0.1615
• Weighted residual factors for all reflections included in the refinement: 0.2006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No