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Information card for entry 1503870
Preview
Coordinates | 1503870.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H35 N O2 |
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Calculated formula | C23 H35 N O2 |
SMILES | O([C@H]([C@@H](/C=C\C)C1CCCCC1)C(C)C)C(=O)N[C@H](C)c1ccccc1 |
Title of publication | Alkylidenesilacyclopropanes derived from allenes: applications to the selective synthesis of triols and homoallylic alcohols. |
Authors of publication | Buchner, Kay M.; Clark, Timothy B.; Loy, Janice M. N.; Nguyen, Thong X.; Woerpel, K. A. |
Journal of publication | Organic letters |
Year of publication | 2009 |
Journal volume | 11 |
Journal issue | 10 |
Pages of publication | 2173 - 2175 |
a | 5.2823 ± 0.0002 Å |
b | 15.4651 ± 0.0006 Å |
c | 13.0625 ± 0.0005 Å |
α | 90° |
β | 100.723 ± 0.0004° |
γ | 90° |
Cell volume | 1048.46 ± 0.07 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0319 |
Residual factor for significantly intense reflections | 0.0303 |
Weighted residual factors for significantly intense reflections | 0.0786 |
Weighted residual factors for all reflections included in the refinement | 0.0798 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1503870.html
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