Information card for entry 1504147

Structure parameters

• Formula: C18 H19 N O5
• Calculated formula: C18 H19 N O5
• SMILES: c1(ccc(cc1)C1=CC[C@@]2(C(=O)[C@@]1(C)CCC2)C(=O)OC)N(=O)=O.c1(ccc(cc1)C1=CC[C@]2(C(=O)[C@]1(C)CCC2)C(=O)OC)N(=O)=O
• Title of publication: Gold-catalyzed synthesis of carbon-bridged medium-sized rings.
• Authors of publication: Barabé, Francis; Bétournay, Geneviève; Bellavance, Gabriel; Barriault, Louis
• Journal of publication: Organic letters
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 18
• Pages of publication: 4236 - 4238
• a: 14.725 ± 0.01 Å
• b: 16.2 ± 0.011 Å
• c: 6.768 ± 0.005 Å
• α: 90°
• β: 91.991 ± 0.007°
• γ: 90°
• Cell volume: 1613 ± 2 ų
• Cell temperature: 202 ± 2 K
• Ambient diffraction temperature: 202 ± 2 K
• Number of distinct elements: 4
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1214
• Weighted residual factors for all reflections included in the refinement: 0.1243
• Goodness-of-fit parameter for all reflections included in the refinement: 1.293
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No