Information card for entry 1504189
Formula
C19 H24 O4
Calculated formula
C19 H24 O4
SMILES
O=C1O[C@H]2[C@H]3[C@]1(C)CCC[C@@]3(C1=CC(=O)O[C@@H](C1=C2)C(C)C)C
Title of publication
Total synthesis of oidiodendrolides and related norditerpene dilactones from a common precursor: metabolites CJ-14,445, LL-Z1271gamma, oidiolactones A, B, C, and D, and nagilactone F.
Authors of publication
Hanessian, Stephen; Boyer, Nicolas; Reddy, Gone Jayapal; Deschênes-Simard, Benoît
Journal of publication
Organic letters
Year of publication
2009
Journal volume
11
Journal issue
20
Pages of publication
4640 - 4643
a
7.7249 ± 0.0001 Å
b
9.6338 ± 0.0002 Å
c
22.5067 ± 0.0004 Å
α
90°
β
90°
γ
90°
Cell volume
1674.95 ± 0.05 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
3
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0369
Residual factor for significantly intense reflections
0.0333
Weighted residual factors for significantly intense reflections
0.0854
Weighted residual factors for all reflections included in the refinement
0.0881
Goodness-of-fit parameter for all reflections included in the refinement
1.038
Diffraction radiation wavelength
1.54178 Å
Diffraction radiation type
CuKα
Has coordinates
Yes
Has disorder
No
Has Fobs
No
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/1504189.html