Information card for entry 1504192
Formula
C16 H18 O6
Calculated formula
C16 H18 O6
SMILES
O=C1O[C@H]2[C@H]3[C@]1(C)CCC[C@@]3(C1=CC(=O)O[C@@H](O)[C@@]31O[C@H]23)C
Title of publication
Total synthesis of oidiodendrolides and related norditerpene dilactones from a common precursor: metabolites CJ-14,445, LL-Z1271gamma, oidiolactones A, B, C, and D, and nagilactone F.
Authors of publication
Hanessian, Stephen; Boyer, Nicolas; Reddy, Gone Jayapal; Deschênes-Simard, Benoît
Journal of publication
Organic letters
Year of publication
2009
Journal volume
11
Journal issue
20
Pages of publication
4640 - 4643
a
8.2864 ± 0.0002 Å
b
10.0771 ± 0.0002 Å
c
17.1744 ± 0.0003 Å
α
90°
β
90°
γ
90°
Cell volume
1434.11 ± 0.05 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
3
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0373
Residual factor for significantly intense reflections
0.037
Weighted residual factors for significantly intense reflections
0.0903
Weighted residual factors for all reflections included in the refinement
0.0907
Goodness-of-fit parameter for all reflections included in the refinement
1.091
Diffraction radiation wavelength
1.54178 Å
Diffraction radiation type
CuKα
Has coordinates
Yes
Has disorder
No
Has Fobs
No
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The link is:
https://www.crystallography.net/1504192.html